Ultra-High Performance Liquid Chromatography—Tandem Mass Spectrometry for Rapid Analysis of Seven Phenolic Compounds of Sparganii Rhizoma

• Autorzy: Wang X. , Wu Y. , Wu Q. , Qian Y. , Yue W. , Liang Q.
• Języki publikacji: EN

Abstrakty

EN

The rhizome of Sparganium stoloniferum Buch.-Ham has been used as a traditional Chinese folk medicine for thousands of years. Phenolic compounds are the main bioactive ingredients of the plant. In order to determine the content of phenolic compounds from different major cultivations, a reliable method has been developed using ultra-high performance liquid chromatography coupled with a triple quadrupole electrospray tandem mass spectrometry. Seven compounds, including rutin, kaempferol, p-hydroxybenzaldehyde, formononetin, ferulic acid, vanillic acid, and p-coumaric acid, were simultaneously measured in 10 min. The established approach was fully validated in terms of linearity, sensitivity, precision, repeatability as well as recovery, and successfully applied to determine seven phenolic compounds of Rhizoma Sparganii. This study may be helpful in the quality control of Rhizoma Sparganii and can offer technical support for the pharmacological and clinical study of related drugs.

Słowa kluczowe

EN

Sparganium stoloniferum Buch; -Hamphenolic compoundsUPLC—MS/MS; quality control

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2015
• Tom: Vol. 27, no. 4
• Strony: 755--766
• Opis fizyczny: Bibliogr. 23 poz., rys., tab.

Twórcy

autor

Wang X.

• Pharmaceutical School, Nanjing University of Chinese Medicine, 210023 Nanjing, P.R. China
• Chemical Engineering and Pharmaceutical School, Henan University of Science and Technology, 471023 Luoyang, P.R. China

autor

Wu Y.

• Pharmaceutical College, Xinxiang Medical University, Xinxiang 453003, P.R. China

autor

Wu Q.

• Pharmaceutical School, Nanjing University of Chinese Medicine, 210023 Nanjing, P.R. China

autor

Qian Y.

• Pharmaceutical School, Nanjing University of Chinese Medicine, 210023 Nanjing, P.R. China

autor

Yue W.

• Pharmaceutical School, Nanjing University of Chinese Medicine, 210023 Nanjing, P.R. China

autor

Liang Q.

• Pharmaceutical School, Nanjing University of Chinese Medicine, 210023 Nanjing, P.R. China

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