Quality assessment of Moringa seed shells based on fingerprinting using HPLC-DAD

• Autorzy: Zhu Yangin , Du Ping , Huang Shaojun , Yin Qinhong , Yang Yaling

Identyfikatory

DOI

10.1556/1326.2019.00545

• Języki publikacji: EN

Abstrakty

EN

A fingerprint analysis method was established for the quality control of Moringa seed shells by high-performance liquid chromatography with diode array detection (HPLC–DAD). The HPLC–DAD separation was performed on a Thermo Hypersil Gold C18 (4.6 mm × 250 mm, 5 μm) column by gradient elution with acetonitrile–water as mobile phase. The fingerprint of Moringa seed shells was established with good precision, reproducibility, and stability obtaining within 60 min, and 13 common peaks in the fingerprint were designed. Similarity analysis, principal component analysis (PCA), and hierarchical clustering analysis (HCA) were carried out to analyze the obtained fingerprints. The similarity among 11 batches of samples in addition to No. 5 and 6 was no less than 0.92. Eleven samples could be classified into 2 clusters. The HPLC fingerprint technology and application of chemical pattern recognition can provide a more comprehensive reference for the quality control of medicinal plants.

Słowa kluczowe

EN

Moringa seed shells; fingerprint; similarity evaluation; PCA; HCA

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2020
• Tom: Vol. 32, no. 1
• Strony: 28--33
• Opis fizyczny: Bibliogr. 33 poz., rys., tab.

Twórcy

autor

Zhu Yangin

• Kunming University of Science and Technology, Kunming 650500, Yunnan, China
• Kunming University of Science and Technology, Kunming 650093, China

autor

Du Ping

• Kunming University of Science and Technology, Kunming 650093, China

autor

Huang Shaojun

• Kunming University of Science and Technology, Kunming 650093, China

autor

Yin Qinhong

• Kunming 650223, China

autor

Yang Yaling

• Kunming University of Science and Technology, Kunming 650500, Yunnan, China

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Uwagi

PL

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).