Influence of calcination parameters on physicochemical and structural properties of co-precipitated magnesium silicate

• Autorzy: Ciesielczyk F. , Bartczak P. , Klapiszewski L. , Paukszta D. , Piasecki A. , Jesionowski T.

Identyfikatory

DOI

10.5277/ppmp140111

• Języki publikacji: EN

Abstrakty

EN

Physicochemical properties of different oxide systems depend mostly on the method of their preparation and classification, so the main aim of the study was to obtain the MgO·SiO2 hybrid in an aqueous solution and its calcination under assumed conditions. Research scope included evaluation of the effect of the basic parameters of the calcination process (time and temperature) on the structural properties of the final materials. Products obtained by the proposed method were thoroughly characterized. The chemical composition, crystalline structure, morphology and nature of the dispersion as well as parameters of the porous structure were established. The results of research in a decisive manner confirmed the possibility of designing the properties of inorganic oxide systems such as MgO·SiO2, which will definitively scheduled into potential directions for their use.

Słowa kluczowe

EN

magnesium silicate; precipitation; calcination; WAXS; porous structure

• Wydawca: Oficyna Wydawnicza Politechniki Wrocławskiej
• Czasopismo: Physicochemical Problems of Mineral Processing
• Rocznik: 2014
• Tom: Vol. 50, iss. 1
• Strony: 119--129
• Opis fizyczny: Bibliogr. 22 poz., rys.

Twórcy

autor

Ciesielczyk F.

• Poznan University of Technology, Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, M. Sklodowskiej-Curie 2, PL-60-965, Poznan, Poland

autor

Bartczak P.

• Poznan University of Technology, Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, M. Sklodowskiej-Curie 2, PL-60-965, Poznan, Poland

autor

Klapiszewski L.

• Poznan University of Technology, Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, M. Sklodowskiej-Curie 2, PL-60-965, Poznan, Poland

autor

Paukszta D.

• Poznan University of Technology, Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, M. Sklodowskiej-Curie 2, PL-60-965, Poznan, Poland

autor

Piasecki A.

• Poznan University of Technology, Faculty of Mechanical Engineering and Management, Institute of Materials Science and Engineering, Jana Pawla II 24, PL-60-965, Poznan, Poland

autor

Jesionowski T.

• Poznan University of Technology, Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, M. Sklodowskiej-Curie 2, PL-60-965, Poznan, Poland

Bibliografia

• 1. BALDYGA J., JASINSKA M., JODKO K., PETELSKI P., 2012, Precipitation of amorphous colloidal silica from aqueous solutions-aggregation problem, Chem. Eng. Sci., 77, 207–216.
• 2. BHARDWAJ D., SHARMA M., SHARMA P., TOMAR R., 2012, Synthesis and surfactant modification of clinoptilolite and montmorillonite for the removal of nitrate and preparation of slow release nitrogen fertilizer, J. Hazard. Mater., 227–228, 292–300.
• 3. CHOI J., KIM J., YOO K.S., LEE T.G., 2008, Synthesis of mesoporous TiO2/γ-Al2O3 composite granules with different sol composition and calcinations temperature, Powder Technol., 181, 83–88.
• 4. CIESIELCZYK, F., NOWACKA, M., PRZYBYLSKA, A., JESIONOWSKI, T., 2011, Dispersive and electrokinetic evaluations of alkoxysilane-modified MgO-SiO2 oxide composite and pigment hybrids supported on it, Colloids Surf. A: Physicochem. Eng. Asp., 376, 21–30.
• 5. GUO F., PENG Z.G., DAI J.Y., XIU Z.L., 2010, Calcinated sodium silicate as soil base catalyst for biodisel production, Fuel Process. Technol., 91, 322–328.
• 6. IBRAHIM S.S., SELIM A.Q., 2012, Heat treatment of natural diatomite, Physicochem. Probl. Miner. Process., 48, 413–424.
• 7. JOHNSON J.H., MCFARLANE A.J., BORMANN T., MORAES J., 2004, Nano-structured silica and silicates: new materials and their applications in paper, Cur. Appl. Phys., 4, 411–414.
• 8. KIM D.J., HAHN S.H., OH S.H., KIM E.J., 2002, Influence of calcination temperature on structural and optical properties of TiO2 thin films prepared by sol–gel dip coating, Mat. Lett., 57, 355–360.
• 9. LAURENTOWSKA A., JESIONOWSKI T., 2012, ZnO-SiO2 oxide composites synthesis turing precipitation from emulsion system, Physicochem. Probl. Miner. Process., 48, 63–76.
• 10. LEE C.-K., WANG C.-A., LYU M.-D., JUANG L.-C., LIU S.-S., HUNG S.-H., 2007, Effects of sodium content and calcination temperature on the morphology, structure and photocatalytic activity of nanotubular titanates, J. Colloid Interface Sci., 316, 562–569.
• 11. LU B.-Q, ZHU Y.-J., AO H.-Y., QI C., CHEN F., 2012, Synthesis and characterization of magnetic iron oxide/calcium silicate mesoporous nanocomposites as a promising vehicle for drug delivery, Appl. Mater. Interfaces, 4, 6969–6974.
• 12. MODRZEJEWSKA-SIKORSKA A., CIESIELCZYK F., JESIONOWSKI T., 2012, Synthesis and characterisation of precipitated CuO•SiO2 oxide composites, Pigm. Resin Technol., 41, 71–80.
• 13. MOHAMMADI T., PAK A., 2003, Effect of calcinations temperature of kaolin as a support for zeolite membranes, Sep. Purif. Technol., 30, 241–249.
• 14. QIU Z.-Y., NOH I.-S., ZHANG S.-M., 2013, Silicate-doped hydroxyapatite and its promotive effect on bone mineralization (review), Front. Mater. Sci., 7, 40–50.
• 15. REN C., QIU W., CHEN Y., 2013, Physicochemical properties and photocatalytic activity of the TiO2/SiO2 prepared by precipitation method, Sep. Purif. Technol., 107, 264–272.
• 16. SARUCHI, SURBHI, AGHAMKAR, P., KUMAR S., 2013, Neodymia-silica nanocomposites: synthesis and structural properties, Adv. Mater. Lett., 4, 78–81
• 17. SIWINSKA-STEFANSKA K., PAUKSZTA D., JESIONOWSKI T., 2011, Physicochemical properties of TiO2/SiO2 oxide composites produced by nucleation of reaction system, Przem. Chem. 90, 1009–1010.
• 18. TANGCHUPONG N., KHAODEE W., JONGSOMJIT B., LAOSIRIPOJAN N., PRASERTHDAM P., ASSABUMRUNGRAT S., 2010, Effect of calcination temperature on characteristic of sulfated zirconia and it’s application as catalyst for isosynthesis, Fuel Process. Technol., 91, 121–126.
• 19. YAMAGATA C., ELIAS D.R., PAIVA M.R.S., MISSO A.M., CASTANHO S.R.H.M., 2013, Facile preparation of apatite-type lanthanum silicate by a new water-based sol-gel process, Mater. Res. Bull., 48, 2227–2231.
• 20. YAN CH.F., GRACE J.R., LIM C.J., 2010, Effects of rapid calcinations on properties of calcium based sorbents, Fuel Process. Technol., 91, 1678–1686
• 21. YU J., YU H., CHENG B., TRAPALIS C., 2006, Effects of calcinations temperature on the microstructures and photocatalytic activity of titanate nanotubes, J. Mol. Catal., 249, 135–142.
• 22. ZHANG J., GUO Z., ZHI X., TANG H., 2013, Surface modification of ultrafine precipitated silica with 3-methacryloxypropyltrimethoxysilane in carbonization process, Colloids Surf. A: Physicochem. Eng. Asp., 418, 174–179.