Statistical approach to the production of cement composites doped with ZnO and ZnO-based materials

• Autorzy: Klapiszewska Izabela , Balicki Sebastian , Wilk Kazimiera A. , Klapiszewski Łukasz , Ślosarczyk Agnieszka

Identyfikatory

DOI

10.37190/ppmp/168352

• Języki publikacji: EN

Abstrakty

EN

In this study, physical and functional properties of the cement composites containing ZnO, ZnO/lignin and lignin admixtures were investigated using Response Surface Methodology (RSM). The I-optimal design based on RSM was used to assess the influence of ZnO-based doping agent, of either commercial or synthetic origin, on cement composite production in the function of average compressive strength and cost. Polynomial mathematical models were developed by RSM confronting results from the experimental design. The accuracy and precision of the utilized models established by I-optimal design were tested using Analysis of Variance (ANOVA). The first stage of formulation optimization revealed that the use of commercially available ZnO-based admixture no. 4 (ZnO-SA, supplied by Sigma Aldrich) allowed to achieve the desired results, passing all the requirements, i.e., the best microbial purity combined with reasonable cost, followed by satisfactory physical properties. In the second stage of formulation optimization, the influence of implementing the hybrid materials, i.e., ZnO-SA mixed in different proportions with lignin was evaluated. RSM revealed that doping admixture no. 3, i.e., ZnO-SA/lignin (5:1), is the best candidate, which comprised augmented functional and physical properties of the fabricated cement composite. This component exhibited the best microbial purity as well as the lowest total pore volume, followed by satisfactory physical properties. Verification of the model findings indicated considerable agreement between the predicted and experimental values. From the findings, it was confirmed that a reasonable cost-performance balance for cement composites can be achieved using ZnO-SA and ZnO-SA/lignin (5:1).

Słowa kluczowe

EN

cement composite; zinc oxide; hybrid materials; design of experiments

• Wydawca: Oficyna Wydawnicza Politechniki Wrocławskiej
• Czasopismo: Physicochemical Problems of Mineral Processing
• Rocznik: 2023
• Tom: Vol. 59, iss. 4
• Strony: art. no. 168352
• Opis fizyczny: Bibliogr. 40 poz., rys., tab., wykr.

Twórcy

autor

Klapiszewska Izabela

• Institute of Building Engineering, Faculty of Civil and Transport Engineering, Poznan University of Technology, PL-60965 Poznan, Poland

autor

Balicki Sebastian

• Department of Engineering and Technology of Chemical Processes, Faculty of Chemistry, Wroclaw University of Science and Technology, PL-50370 Wroclaw, Poland

autor

Wilk Kazimiera A.

• Department of Engineering and Technology of Chemical Processes, Faculty of Chemistry, Wroclaw University of Science and Technology, PL-50370 Wroclaw, Poland

autor

Klapiszewski Łukasz

• Institute of Chemical Technology and Engineering, Faculty of Chemical Technology, Poznan University of Technology, PL-60965 Poznan, Poland

autor

Ślosarczyk Agnieszka

• Institute of Building Engineering, Faculty of Civil and Transport Engineering, Poznan University of Technology, PL-60965 Poznan, Poland

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Uwagi

Opracowanie rekordu ze środków MNiSW, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2024).