Kompleksowa charakterystyka strukturalna uporządkowanych faz międzymetalicznych

Jezierska, E.

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Tytuł artykułu

Kompleksowa charakterystyka strukturalna uporządkowanych faz międzymetalicznych

Autorzy

Jezierska E.

Identyfikatory

Warianty tytułu

Integrated structural characterization of ordered intermetallics

Języki publikacji

Abstrakty

Badania strukturalne obejmowały kompleksową elektronomikroskopową analizę fazową ze szczególnym uwzględnieniem struktury domen antyfazowych i ich analizy krystalograficznej oraz sposobu rozmieszczenia cząstek i wydzieleń w strukturach wielofazowych. Charakterystyka strukturalna została przeprowadzona zarówno metodami konwencjonalnej mikroskopii i dyfrakcji elektronów, jak też metodami wielokrotnego ciemnego pola, wysokorozdzielczej mikroskopii elektronowej (HRTEM) w jasnym i ciemnym polu (DF HRTEM), krystalografii elektronowej, spektrometrii energodyspersyjnej (EDS) i dyfrakcji w zbieżnej wiązce elektronów przy dużych kątach zbieżności (LACBED). Przedmiotem badań były stopy na bazie uporządkowanych faz międzymetalicznych o różnych nadstrukturach Ni3Al, NiAl, FeAl, Fe3Al, Cu3Au, Al3Ti, Al3Zr. Na podstawie przeprowadzonych badań strukturalnych określono charakter zmian rozkładu wielkości domen antyfazowych oraz ich kształtu w zależności od typu uporządkowania, składu chemicznego i orientacji krystalograficznej. Określono czynniki sprzyjające nadplastyczności w stopach na bazie uporządkowanej fazy międzymetalicznej Fe3Al z uwzględnieniem poślizgu nadstrukturalnego. Uzyskano obrazy HRTEM martenzytu modulowanego, powstającego przez oscylacje płaszczyzn krystalograficznych oraz martenzytycznych struktur wielowarstwowych, typowych dla stopów z pamięcią kształtu, polegających na synchronicznych przesunięciach atomów. Na podstawie komplementarnych badań z różnych technik mikroskopowych określono strukturalne uwarunkowania występowania struktur modulowanych w uporządkowanych fazach międzymetalicznych w stopach Ni-Al, Ni-Al-Cr i Ni-Fe-Ti. Wprowadzono nowatorską koncepcję tensegralności strukturalnej do opisu przemian strukturalnych i samoorganizacji defektów struktury krystalicznej.

Integrated structural characterization of ordered intermetallics and comparison of results for different phases and superstructures were performed by means of transmission electron microscopy. The antiphase domains structure in ordered intermetallics has been examined. Different techniques and methods were used in the study: conventional transmission electron microscopy TEM, electron diffraction, multiple dark field, large angle converged electron diffraction LACBED and high resolution transmission electron microscopy HRTEM. Experimental studies have been carried out in order to evaluate the effect of ordering phenomena for various phases: Ni3Al, NiAl, FeAl, Fe3Al, Cu3Au, Al3Ti, Al3Zr. Nanosized symmetry-related antiphase domains were observed in the studied Ni-Al and Fe-Al alloys after shock-wave deformation and detailed stereological investigation had been performed. Superplastic deformation in Fe3Al alloy was analyzed. Modulated martensite and layered structures were investigated using conventional TEM and HRTEM methods. The methodology of modulated structure recognition was proposed and its application to ordered intermetallics was presented. The concept of structural tensegrity was introduced to describe phase transformation and self-organization of complex defects in crystalline structures.

Słowa kluczowe

uporządkowane fazy międzymetaliczne domeny antyfazowe struktury modulowane tensegralność strukturalna transmisyjna mikroskopia elektronowa dyfrakcja elektronowa dyfrakcja elektronowa przy dużych kątach zbieżności LACBED wysokorozdzielcza transmisyjna mikroskopia elektronowa HRTEM

ordered intermetallics antiphase domains modulated structures structural tensegrity transmission electron microscopy TEM electron diffraction large angle converged electron diffraction LACBED high resolution transmission electron microscopy (HRTEM)

Wydawca

Oficyna Wydawnicza Politechniki Warszawskiej

Czasopismo

Prace Naukowe Politechniki Warszawskiej. Inżynieria Materiałowa

Rocznik

2010

Tom

z. 26

Strony

3--194

Opis fizyczny

Bibliogr. 302 poz., tab., rys., wykr.

Twórcy

autor

Jezierska E.

Wydział Inżynierii Materiałowej, Politechnika Warszawska

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