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Determination of wetting at elevated temperatures using image analysis

Wybrane pełne teksty z tego czasopisma
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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: Wettability of a solid by a liquid is characterized by the contact angle or the wettability parameter which is a function of the contact angle and the surface tension. One well-known method to determine the contact angle and the surface tension experimentally is the sessile-drop method. The accuracy of this method depends on different geometric parameters measured from the image of the liquid drop on the solid captured during the experiments. In this study, software was developed to measure the parameters required for the calculation of the contact angle and the surface tension as well as all other relevant parameters such as spreading and drop volume from the sessile-drop images. Design/methodology/approach: The image analysis program presented in this study was developed to determine the wetting characteristics of a solid/molten metal system at elevated temperatures; hence, it deals mainly with the measurement of the contact angle and the calculation of the surface tension from the images captured during such experiments. Findings: In this study, a robust image analysis program has been developed. It gives not only the contact angle and the surface tension, but also a number of other important parameters of interest in wetting such as the spreading and the change in the surface area and volume of the sessile drop under different lighting conditions. Practical implications: The future work will cover the development of new filters which will eliminate further the interference of components placed outside the "analysis window" with the components to be analyzed. This task will have an impact at the level of filtration in the operation pipeline presented above. Originality/value: The results are validated by comparing them with the measurements conducted using an optical microscope; and the agreement is good.
Rocznik
Strony
213--224
Opis fizyczny
Bibliogr. 24 poz., tab., rys., wykr.
Twórcy
autor
autor
autor
  • Department of Applied Sciences, University of Quebec at Chicoutimi 555 boul. De l'Université Chicoutimi, Québec, G7H 2B1, Canada, dkocaefe@uqac.ca
Bibliografia
  • [1] A.W. Adamson, Physical Chemistry of Surfaces, Wiley, New York, 1982.
  • [2] J.M. Alvarez, A. Amirfazli, A.W. Neumann, Automation of axysymmetric drop shape analysis-diameter for contact angle measurements, Colloids and Surfaces A-Physicochemical and Engineering Aspects 156/1-3 (1999) 163-176.
  • [3] E. Angel, Discrete Techniques in Interactive, Computer Graphics, Addison-Wesley, Reading MA, USA, 1997, 71-414.
  • [4] C. Atae-Allah, M.Cabrerizo-V’ilchez, J.F. G’omez Lopera, J.A. Holgado-Terriza, R. Rom’an-Rold, P.L. Luque-Escamilla, Measurement of surface tension and contact angle using entropic edge detection, Measurement Science and Technology 12/3 (2001) 288-298.
  • [5] F. Bashforth, J.C. Adams, An Attempt to Test the Theory of Capillary Action, Cambridge University Press, London, 1982.
  • [6] O.I. Del Rio, D.Y. Kwok, R. Wu, J.M. Alvarez, A.W. Neumann, Contact angle measurements by axisymmetric drop shape analysis and an automated polynomial fit program, Colloids and Surfaces A-Physicochemical and Engineering Aspects 143/2-3 (1998) 197-210.
  • [7] N.E. Dorsey, A new equation for the determination of surface tension from the form of a sessile drop or bubble, Journal of the Washington Academy of Sciences 18 (1928) 505.
  • [8] N. Eustathopoulos, M.G. Nicholas, B. Drevet, Pergamon Materials Series, Wettability at High Temperatures, Vol. 3, Pergamon, Oxford, 1999.
  • [9] B.M. Gallois, Wetting in nonreactive liquid metal-oxide systems, Journal of the Minerals, Metals and Materials Society 49/6 (1997) 48-51.
  • [10] R.G. Gonzalez, Digital Image Processing, Addison-Wesley, Reading MA, USA, 1992.
  • [11] Yu.A. Koshevnik, I.M. Kusakov, N.M. Lubman, Determination of surface tension of liquids from the dimensions of sessile drop, Russian Journal of Physical Chemistry A 27/12 (1953) 1887-1894 (in Russian).
  • [12] C.G. Levi, G.J. Abbaschian, R. Mehrabian, Interface interactions during fabrication of aluminum alloy-alumina fiber composites, Metallurgical Transactions A-Physical Metallurgy and Materials Science 9/5 (1978) 697-711.
  • [13] V. Leroux, J.C. Labbe, M.E.R. Shanahan, Contact angle and surface tension measurements on a metal drop by image processing and numerical calculations, High Temperature Materials and Processes 19/4 (2000) 351-364.
  • [14] L.E. Murr, Interfacial Phenomena in Metals and Alloys, Addison-Wesley Publishing Company, Reading, MA, 1975.
  • [15] A.W. Neumann, J.K. Spelt, Eds. Surfactant Science Series, Applied surface thermodynamics, Dekker, New York, 63, 1996.
  • [16] S.B.G.M. O’Brian, Wettability and Adhesion, Some Surface Tension and Contact Angle Problems in Industry, in Contact Angle, VSP Publishers, 1993, 937-951.
  • [17] M.E.R. Shanahan, Profile and contact angle of small sessile drops: a more general approximate solution, Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases 80/ 1 (1984) 37-45.
  • [18] A. Sklodowska, M. Wozniak, R. Matlakowska, The method of contact angle measurements and estimation of work of adhesion in bioleaching of metals, Biological Procedures Online 1/3 (1999) 114-121, (Available at: http://www.biologicalprocedures.com).
  • [19] D.N. Stacopolus, Computation of surface tension and of contact angle by the sessile drop method, Journal of Colloid and Interface Science 23/3 (1967) 453-458.
  • [20] K.R. Van Horn, Ed., Aluminum, Properties, Physical Metallurgy and Phase Diagrams, American Society of Metals, Park 1 (1967) 179.
  • [21] H. William, Interpolation and Extrapolation: Cubic Spline Interpolation and Modelling of Data: Fitting Data to a Straight Line in Numerical Recipes in C: The Art of Scientific Computing, Cambridge University Press 113-117 (1992) 661-666.
  • [22] R.P. Woodward, FTA200 Measurement Capabilities, 2007 (http://www.firsttenangstroms.com/pdfdocs/mea.pdf).
  • [23] http://www.omegamultimedia.com/products/media100/cinestream-win.htm
  • [24] The related departments of Stanford University approve the polishing procedures and guarantee the final roughness of the substrates.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-PWA9-0042-0027
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