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Warianty tytułu
Ekstrakcja do fazy stałej w analizie żywności
Języki publikacji
Abstrakty
In this study, a Solid Phase Extraction (SPE) as a method of sample preparation has been described. A typical procedure, the mechanisms involved in SPE and factors which affect effectivity have also been discussed. Possible uses of SPE in fragrance and food chemistry have been presented.
Opisano technikę ekstrakcji do fazy stałej (Solid Phase Extraction, SPE), stosowaną jako metoda przygotowania próbek do analizy za pomocą chromatografii gazowej. Omówiono zasadę działania, scharakteryzowano mechanizmy odpowiedzialne za proces rozdziału i czynniki wpływające na efektywność. Przedstawiono możliwe zastosowania SPE w chemii żywności i substancji zapachowych, ze wskazaniem rodzajów wypełnienia i zatrzymywanych związków chemicznych.
Rocznik
Tom
Strony
5--13
Opis fizyczny
Bibliogr. 28 poz.
Twórcy
autor
autor
autor
autor
- Instytut Podstaw Chemii Żywności, Wydział Biotechnologii i Nauk o Żywności, Politechnika Łódzka
Bibliografia
- [1] Guide to Solid Phase Extraction, Supelco Bulletin 910, (1998), http://www.sigmaaldrich.com/Graphics/Supelco/objects/4600/4538.pdf
- [2] Zief M., Kiser R.: Solid Phase Extraction for Sample Preparation, J.T. Baker, (1994).
- [3] Antonelli A., Fabbri C.: Essential Oils: SPE Fractionation, Chromatographia 49, 125-130, (1999).
- [4] Smith R.M.: Extractions with superheated water, J. Chromatogr. A, 975, 31-46, (2002).
- [5] Özel M.Z., Clifford A.A.: Superheated water extraction of fragrance compounds from Rosa canina, Flavour Fragr. J., 19, 354-359, (2004).
- [6] Özel M.Z., Gogus F., Lewis A.C.: Comparison of direct thermal desorption with water distillation and superheated water extraction for the analysis of volatile components of Rosa damascena Mill, using GCxGC-TOF/MS, Anal. Chim. Acta, 556, 172-177, (2006).
- [7] Özel M.Z., Kaymaz H.: Superheated water extraction, steam distillation and Soxhlet extraction of essential oils of Origanum onites, Anal. Bioanal. Chem., 379, 1127-1133, (2004).
- [8] Özel M.Z., Gogus F., Lewis C.: Extraction of essential oils of leaves and flowers of Achillea monocephala by superheated water, Flavour Fragr. J., 21, 122-128, (2006).
- [9] Radulescu V., Chiliment S., Oprea E.: Capillary gas chromatography-mass spectrometry of volatile and semi-volatile compounds of Salvia officinalis, J. Chromatogr. A, 1027, 121-126, (2004).
- [10] Wang Z.H., Dou J., Macura D., Durance T.D., Nakai S.: Solid phase extraction for GC analysis of beany flavours in soymilk, Food Res. Int., 30, 503-511, (1998).
- [11] Adamczyk S., Lazaro R., Perez-Arquillue C., Conchello P., Herrera A.: Evaluation of residues of essential oil components in honey after different anti-varroa treatments, J. Agric. Food Chem., 53, 10085-10090, (2005).
- [12] Özel M.Z., Gogus F., Lewis A.C., Subcritical water extraction of essential oils from Thymbra spicata Food Chem., 82, 381-386, (2003).
- [13] Bertoli A., Pistelli L., Morelli I., Fraternale D., Giamperi L., Ricci D.: Volatile constituents of different parts (roots, stems and leaves) of Smymium olusatrum L., Flavour Fragr. J., 19, 522-525, (2004).
- [14] Pineiro Z., Palma M., Barroso C.G.: Determination of terpenoids in wines by solid phase extraction and gas chromatography, Anal. Chim. Acta, 513, 209-214 (2004).
- [15] Castro Vazquez L., Consuelo Diaz-Maroto M., Guchu E., Soledad Perez-Coello M.: Analysis of volatile compounds of eucalyptus honey by solid phase extraction followed by gas chromatography coupled to mass spectrometry, Eur. Food Res. Technol., 224, 27-31, (2006).
- [16] Brinker A.M., Raskin I.: Determination of triptolide in root extracts of Tripterygium wilfordii by solid-phase extraction and reverse-phase high-performance liquid chromatography, J. Chromatogr. A, 1070, 65-70, (2005).
- [17] Krzyszowska A.J., Vance G.F.: Solid-phase extraction of dicamba and picloram from water and soil samples for HPLC analysis, J. Agric. Food Chem., 42, 1693-1696, (1994).
- [18] Simal-Gándara, Determination of pesticides by solid phase extraction followed by gas chromatography with nitrogen-phosphorous detection in natural water and comparison with solvent drop microextraction, Anal. Bioanal. Chem., 384, 1002-1006, (2006).
- [19] Brandsteterova E., Kubalec P., Bovanova L., Simko P., Bednarikova A.: Machackova L., SPE and MSPD as pre-separation techniques for HPLC of tetracyclines in meat, milk and cheese, Z Lebensm. Unters. F. A, 205, 311-315, (1997).
- [20] Esteve-Turrillas F.A., Pastor A., de la Guardia M.: Determination of pyrethroid insecticide residues in vegetable oils by using combined solid-phases extraction and tandem mass spectrometry detection, Anal. Chim. Acta, 553, 50-57, (2005).
- [21] Barrek S., Paisse O., Grenier-Loustalot M.F.: Analysis of pesticide residues in essential oils of citrus fruit by GC-MS and HPLC-MS after solid-phase extraction, Anal. Bioanal. Chem., 376, 157-161, (2003).
- [22] Kleinhenz S., Jira W., Schwind K.H.: Dioxin and polychlorinated biphenyl analysis: Automation and improvement of clean-up established by example of spices, Mol. Nutr. Food Res., 50, 362-367, (2006).
- [23] Schenck F.J., Howard-King V.: Rapid solid phase extraction cleanup for pesticide residues in fresh fruits and vegetables, Bull. Environ. Contam. Toxicol., 63, 277-281, (1999).
- [24] Jun-Ho Hwang, Kwang-Geun Lee, Reduction of aflatoxin B1 contamination in wheat by various cooking treatments, Food Chem., 98, 71-75, (2006).
- [25] Boselli E., Caboni M.F., Lercker G.: Extraction and purification of free cholesterol from some egg-containing food by on-line supercritical fluid extraction - solid-phase extraction, Eur. Food Res. Technol., 212, 244-246, (2001).
- [26] Lopez-Blanco C., Gomez-Alvarez S., Rey-Garrote M., Cancho-Grande B., Mario Vincenzo Russo J., De Leonardis A., Macciola V.: Solid phase extraction-gas-chromatographic method to determine free cholesterol in animal fats, J. Food Compos. Anal., 18, 617-624, (2005).
- [27] Kyong-Su Kima, Jeong-Min Leeb, Cheul-Hee Hongc, Solid phase extraction (SPE) method for detection of irradiated meats, Lebensm. Wiss. Technol. 37, 559-563, (2004).
- [28] Shimelis O., Auranc C., Trinh A.: Fractionation of cis/trans FAMEs using Discovery AG-Ion SPE, Analytix, 2, 18-19, (2006).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-LOD7-0012-0001