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Microstructural and hardness characterisation of sintered low alloyed steel

Wybrane pełne teksty z tego czasopisma
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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: The purpose of the present study is to produce low ally PM steel without any addition and with addition of ferro-boron addition by conventional PM manufacturing route at the different sintering temperature. Design/methodology/approach: Fe-Ni-Cu-Mo-C sintered steel containing 0.5 percent ferro-boron addition was used in this study. The compacts were prepared by powder metallurgy method involving powder mixing, cold pressing at 700 MPa pressure and sintering at temperatures of 1180, 1200 and 1250*C in nitrogen+% 4 H2 atmosphere for 30 minutes. The influence of sintering temperature and boron addition on the hardness and microstructure of P/M steels were investigated. Optical and scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) techniques were used for characterization of the sintered steels. Findings: The results show that increasing sintering temperature resulted in increase in hardness values; however, those values were dropped after sintering temperature higher than 1180*C. On the other hand, Boron addition contributed to hardness values at sintering temperature of 1200oC. Those values were decreased with increasing sintering temperature. Research limitations/implications: The composition of the sintered steels effect on the density values. The composition of the grain boundaries were affected from sintering temperature. Boron, carbon, molybdenum were seen in the grain boundaries of the specimen having the highest hardness values. It is thought that those compositions strongly effects on hardness values of the specimens. Originality/value: Fe-Ni-Cu-Mo-C base powder with and without boron addition low alloy sintered steel were produced. The effects composition and sintering temperature were investigated.
Rocznik
Strony
23--28
Opis fizyczny
Bibliogr. 23 poz., il., tab., wykr.
Twórcy
autor
autor
  • Metal Education Division, Technical Education Faculty, Sakarya University, Esentepe Campus, 54187, Sakarya, Turkey, ryilmaz@sakarya.edu.tr
Bibliografia
  • [1] R. M. German, Powder Metallurgy of Iron and Steel, John Willey and Sons, USA, 1998.
  • [2] K. S. Narasimhan, Sintering of powder mixtures and the Growth of ferrous powder metallurgy, Materials Chemical Physic 67 (2001) 56-65.
  • [3] R. J. Causton, J. J. Fulmer, Sinter hardening low alloy steels, Proceedings of the Advances in Powder Metallurgy and Particulate Materials, San Francisco, California, USA, Volume 5, 1992, 17-52.
  • [4] V. A. Tracey, Nickel sintered steels: development, status and prospects, Proceedings of the Advances in Powder Metallurgy and Particulate Materials, San Francisco, California, USA, Volume 5, 1992, 303-314.
  • [5] G. S. Upadhyaya, Sintered metallic and ceramic materials-sintered low-alloy ferrous materials, John Wiley & Sons LTD, West Sussex, England, 2000.
  • [6] H. Khorsand, S. M. Habii, K. Yoozbasizadea, K. Janghordban, S. M. S. Rihhai, H. R. Serai, M. Ashtai, The role of heat treatment on wear behavior of powder metallurgy low alloy steels, Materials and Design 23 (2002) 667-670.
  • [7] R. Yilmaz, A. Gökçe, Effect of ferro-titanium addition on impact and fracture toughness of low alloyed steel produced by powder metallurgy, Proceedings of the 13th International Metallurgy and Materials Congress, Istanbul, 2006, 903-909 (in Turkish).
  • [8] R. Yilmaz, A. Gökçe, The effect of ferro-titanium addition on mechanical properties of alloyed sintered low alloyed steel, Proceedings of the 11th International Materials Symposium, Denizli, 2006, 760-766 (in Turkish).
  • [9] R. Yilmaz, A. Gökçe, H. Kapdibas, The effect of molybdenum addition on the microstructure and mechanical properties of sintered steel, Advanced Materials Research, Materials and Technologies 22-23 (2007) 71-74.
  • [10] R. Yilmaz, Ö. Özgün, The effect of chemical composition on fracture toughness of sintered alloyed steel produced by powder metallurgy, Proceedings of the 14th International Metallurgy and Materials Congress, Istanbul. Submitted. 2008 (in Turkish).
  • [11] R. M. German, Enhanced Sintering Through 2nd Phase Additions, Powder Metallurgy 28/1 (1985) 7-12.
  • [12] M. Seleckha, A. Salak, H. Danninger, The effect of boron liquid phase sintering on properties of Ni-, Mo-and Cr-alloyed structural steels, Journal of Materials Processing Technology 141 (2003) 379-384.
  • [13] M. Selecka, A. Salak, H. Danninger, The effect of boron liquid phase sintering on properties of Ni-Mo and Cr-alloyed structural steels, Journal of Materials Processing Technology 143-144 (2003) 910-915.
  • [14] M. Sarasola, T. Gomez-Acebo, F. Castro, Liquid generation during sintering of Fe-35% Mo powder compacts with elemental boron additions. Acta Materialia 52 (2004) 4615-4622.
  • [15] J. Nowacki, T. Pieczonka, Dilatometric analysis of sintering of iron-boron-cobalt P/M metal matrix composites, Journal of Materials Processing Technology 157-158 (2004) 749-754.
  • [16] H. O. Gülsoy, S. Salman, S. Özbek, Effect of FeB additions on sintering characteristics of injection molded 17-4PH stainless steel powder, Journal of Materials Science 39 (2004) 4835-4840.
  • [17] H. O. Gülsoy, Enhancing the wear properties of iron based powder metallurgy alloys by boron additions, Materials and Design 28 (2007) 2488-2491.
  • [18] Höganas Datasheet, 69.02.505, Starmix, 2005.
  • [19] Marmara Metal, Datasheet. 2006.
  • [20] J. A. Hamill, R. J. Causton, S. O. Shah, High performance ferrous p/m materials utilizing high temperature sintering, Proceedings of the Advances in Powder Metallurgy and Particulate Materials-1992, San Francisco, California, USA, Volume 5,1992, 193-214.
  • [21] J. Abenojar, D. Esteban, M. A. Martinez, F. Velasco, Sintering stainless steels with boron addition in nitrogen base atmosphere, Materials Science Forum 534-536 (2007) 733-736.
  • [22] U. Engstrom, A. Klekovkin, S. Berg, B. Edwards at al., Efficient low alloy steels for high performance structural applications, webpage of Höganas, 2006.
  • [23] S. M. Lee, S. J. L. Kang, Theoretical analysis of liquid-phase sintering: pore filling theory, Acta Materialia 46/9 (1998) 3191-3202.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BWAN-0003-0038
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