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The Mossbauer spectroscopy studies of retained austenite

Wybrane pełne teksty z tego czasopisma
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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: of this paper: This paper completes the knowledge concerning the mechanisms of destabilization and properties of retained austenite. Investigations were performed on 120MnCrMoV8-6-4-2 steel, which was designed in 1998, in Phase Transformations Research Group of Department of Physical and Powder Metallurgy at the Faculty of Metals Engineering and Industrial Computer Science at AGH University of Science and Technology in Kraków. Design/methodology/approach: The samples of investigated steel were austenitized at the temperature of 900*C and hardened in oil. Next, three from four samples were tempered. Tempering consisted of heating the samples up to chosen temperatures with a heating rate of 0.05*C/s and, after reaching desired temperature, fast cooling. CEMS technique was applied for Mössbauer studies. Findings: Stabilized by heating up to 80oC retained austenite, in the result of mechanical destabilization, transforms into low-temperature tempered martensite, with the structure of low bainite (into the structural constituent in which ε carbide exists). Research limitations/implications: The influence of the temperature, up to which the samples were heated during tempering, on the mechanical stability of retained austenite and on the products of its transformation, was determined. Practical implications: Changes occuring in retained austenite during tempering of steel of high hardenability (hardness), developed for potential applications on tools of enhanced wear resistance, were described. Originality/value: Mössbauer spectroscopy was applied not only for qantitative analysis of retained austenite, but also to analyze the values of quadrupole splitting and isomeric shift, what resulted in significant conclusions concerning the changes in its chemical composition, microstructure, and the level of stresses being present in it.
Rocznik
Strony
633--636
Opis fizyczny
Bibliogr. 17 poz., tab., wykr.
Twórcy
autor
autor
  • Faculty of Metals Engineering and Industrial Computer Science, AGH-University of Science and Technology, ul. Mickiewicza 30, 30-059 Kraków, Poland, jkrawczy@metal.agh.edu.pl
Bibliografia
  • [1] S. Skrzypek, E. Kolawa, J. A. Sawicki, T. Tyliszczak, A study of the retained austenite phase transformation in low alloy steel using conversion electron Mössbauer spectroskopy and X-ray diffraction, Materials Science and Engineering 66 (1984) 145-149.
  • [2] P. Grgac, R. Moravick, M. Kusy, I. Toth, M. Miglierini, E. Illekova, Thermal stability of metastable austenite in rapidly solidified chromium-molybdenum-vanadium tool steel powder, Materials Science and Engineering A 375-377 (2004) 581-584.
  • [3] P. D. Bilmes, M. Solari, C. L. Liorente, Characteristics and effects of austenite resulting from tempering of 13CrNiMo martensitic steel weld metals, Materials Caracterization 46 (2001) 285-296.
  • [4] Soon-Ju Kown, Sei J. Oh, Joo Hag Kim, Sangho Kim, Sunghak Lee, Mössbauer analysis of heat affected zones of an sa 508 steel weld, Scripta Materialia 2, (1999) 131-137.
  • [5] V. G. Gavriljuk, Decomposition of cementite in pearlitic steel due to plastic deformation, Materials Science and Engineering A345 (2003) 81-89.
  • [6] R. Ilola, V. Nadutov, M. Valo, H. Hänninen, On irradiation embrittlement and recovery annealing mechanisms of Cr-Mo-V type pressure vessel steels, Journal of Nuclear Materials 302 (2002) 185-192.
  • [7] V. A. Shabashov, L. G. Korshunov, A. G. Mukoseev, V. V. Sagaradze, A. V. Makarov, V. P. Pilyugin, S. I. Novikov, N. F. Vildanova, Deformation-induced phase transitions in a high-carbon steel. Materials Science and Engineering A346 (2003) 196-207.
  • [8] V. A. Shabashov, A. G. Mukoseev, V. V. Sagaradze, Foration of solid solution of carbon in BCC iron by cold deformation, Material Science and Engineering A307 (2001) 91-97.
  • [9] A. G. Balanyuk, V. G. Gavriljuk, V. N. Shivanyuk, A. I. Tyshchenko, J. C. Rawers, Mössbauer study and thermodynamic modeling of Ee-C-N alloy, Acta Mater. 48 (2000) 3813-3821.
  • [10] E. J. Miola, S. D. De Souza, M. Olzon-Dionysio, D. Spinelli, C. A. Dos Santos, Nitriding of H-12 tool steel by direct-current and pulsed plasmas, Surface and Coatings Technology 116-119 (1999) 347-351.
  • [11] P. Budziński, P. Tarkowski, E. Jartych, A. P. Kobzev, Evolution of mechanical properties in tool steel implanted witch high energy nitrogen ions 63 (2001) 737-742.
  • [12] Y. Jirásková, J. Svoboda, O. Schneeweiss, W. Daves, F. D. Fischer, Microscopic investigation of surface layers on rails, Applied Surface Science 239 (2005) 132-141.
  • [13] P. Bała, The kinetics of phase transformations during tempering and its influence on the mechanical properties, PhD thesis, AGH University of Science and Technology, Cracow 2007. Promotor J. Pacyna (in Polish).
  • [14] P. Bała, J. Pacyna, J. Krawczyk, The kinetics of phase transformations during tempering in the new hot working steel, Journal of Achievements in Materials and Manufacturing Engineering 22 (2007) 15-18.
  • [15] P. Bała, J. Pacyna, J. Krawczyk, The kinetics of phase transformations during the tempering of HS18-0-1 highspeed steel. Journal of Achievements in Materials and Manufacturing Engineering 19 (2006) 19-25.
  • [16] P. Bała, J. Pacyna, J. Krawczyk, The kinetics of phase transformations during the tempering of HS6-5-2 highspeed steel. Journal of Achievements in Materials and Manufacturing Engineering 18 (2006) 47-50.
  • [17] J. Pacyna, P. Bała, T. Skrzypek, The kinetic of phase transformation during continuous heating from quenched state of new high-carbon alloy steel, Proceedings of the 13th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME'2005, Gliwice-Zakopane 2005, 509-512.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BWAN-0002-0014
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