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Mechanical properties of monolayer coatings deposited by PVD techniques

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: This research was done to investigate the mechanical properties of monolayer coatings (Ti/CrN, Ti/TiAlN, Ti/ZrN, CrN, TiAl/TiAlN, Zr/ZrN, TiN) deposited by PVD technique (reactive magnetron sputtering method) onto the substrate from the CuZn40Pb2 brass. A thin metallic layer was deposited prior to deposition of ceramic monolithic coatings to improve adhesion. Design/methodology/approach: The microstructure of the coatings was cross section examined using scanning electron microscope. The residual stress was obtained from the parabolic deflection of the samples, after the coating deposition applying Stoney's equation. The microhardness and Young’s modulus tests were made on the dynamic ultra-microhardness tester. Tests of the coatings' adhesion to the substrate material were made using the scratch test. Findings: Obtained results show that all the coatings are in a state of compressive residual stress. The stiffness of the examined coatings is between 224-330 mN/µm, while Young's modulus is between 258-348 GPa. Concerning the adhesion of the coatings measured by scratch test, it has been stated that the critical load LC2 for coatings, deposited onto the brass ranges from 41 to 57 N. Research limitations/implications: In order to evaluate with more detail the possibility of applying these coatings in tools, further investigations should be concentrated on the determination of the tribological properties of the coatings. Originality/value: The paper contributes to better understanding and recognition the structure of thin coatings deposited by PVD techniques. It should be stressed that the mechanical properties of the PVD coatings obtained in this work are very encouraging and therefore their application for products manufactured at mass scale is possible in all cases where reliable, very hard and abrasion resistant coatings, deposited onto brass substrate are needed.
Rocznik
Strony
549--556
Opis fizyczny
Bibliogr. 25 poz., il., wykr.
Twórcy
  • Division of Materials Processing Technology, Management and Computer Techniques in Materials Science, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland, leszek.dobrzanski@polsl.pl
Bibliografia
  • [1] L. A. Dobrzański, K. Lukaszkowicz, D. Pakuła, J. Mikuła, Corrosion resistance of multilayer and gradient coatings deposited by PVD and CVD techniques, Archives of Materials Science and Engineering 28 (2007) 12-18.
  • [2] A. Erdemir, Review of engineering tribological interfaces for improved boundary lubrication, Tribology International 38 (2005) 249-256.
  • [3] M. Andritschky, Protective coatings on high temperature steel applied by PVD deposition techniques, Journal of Materials Processing Technology 53 (1995) 33-46.
  • [4] P. H. Mayrhofer, C. Mitterer, L. Hultman, H. Clemens, Microstructural design of hard coatings, Progress in Materials Science 51 (2006) 1032-1114.
  • [5] D. N. Allsopp, I. M. Hutchings, Micro-scale abrasion and scratch response of PVD coatings at elevated temperature, Wear 251 (2001) 1308-1314.
  • [6] R. Hoy, J. D. Kamminga, G. C. A. M. Janssen, Scratch resistance of CrN coatings on nitrided steel, Surface and Coatings Technology 200 (2006) 3856-3860.
  • [7] R. Jacobs, J. Meneve, G. Dyson, D. G. Teer, N. M. Jennett, P. Harris, J. von Stebut, C. Comte, P. Feuchter, A. Cavaleiro, H. Ronkainen, K. Holmberg, U. Beck, G. Reiners, C. D. Ingelbrecht, A certified material for the scratch test, Surface and Coatings Technology 174-175 (2003) 1008-1013.
  • [8] L. A. Dobrzański, K. Lukaszkowicz, Erosion resistance and tribological properties of coatings deposited by reactive magnetron sputtering method onto the brass substrate, Journal of Materials Processing Technology 157-158 (2004) 317-323.
  • [9] F. Ashrafizadeh, Adhesion evaluated of PVD coatings to aluminium substrate, Surface and Coatings Technology 130 (2000) 186-194.
  • [10] B. Navinsek, P. Panjan, M. Cekada, D. T. Quinto, Interface characterization of combination hard/solid lubricant coatings by specific methods, Surface and Coatings Technology 154 (2002) 194-203.
  • [11] K. Holmberg, A. Matthews, Coating Tribology, Elsevier, Amsterdam, 1994.
  • [12] K. Lukaszkowicz, L. A. Dobrzański, A. Zarychta, L. Cunha: Mechanical properties of multilayer coatings deposited by PVD techniques onto the brass substrate, Journal of Achievements in Materials and Manufacturing Engineering 15 (2006) 47-52.
  • [13] M. Koch, Use of ion beam etching for producing topographical microstructure, Practical Metallography 36 (1999) 233-249.
  • [14] J. Y. Robic, H. Leplan, Y. Pauleau, B. Rafin, Residual stress in silicon dioxide thin films produced by ion-assisted deposition, Thin Solid Films 290-291 (1996) 34-39.
  • [15] V. Teixeira, Residual stress and cracking in thin PVD coatings, Vacuum 64 (2002) 393-399.
  • [16] X. L. Peng, Y. Tsui, T. Clyne, Stiffness, residual stresses and interfacial fracture energy of diamond films on titanium, Diamond and Related Materials 6 (1997) 1612-1621.
  • [17] A. C. Vlasveld, S. G. Harris, E. D. Doyle, D. B. Lewis, W. D. Munz, Characterisation and performance of partially filtered arc TiAlN coatings, Surface and Coatings Technology 149 (2002) 217-224.
  • [18] L. A. Dobrzański, K. Lukaszkowicz, A. Zarychta, Mechanical properties of monolayer coatings deposited by PVD techniques, Journal of Achievements in Materials and Manufacturing Engineering 20 (2007) 423-426.
  • [19] C. Johnson, J. Ruud, R. Bruce, D. Wortman, Relationships between residual stress, microstructure and mechanical properties of electron beam-physical vapor deposition thermal barrier coatings, Surface and Coatings Technology 108/109 (1998) 80-85.
  • [20] W. Weng-Jin, H. Min-Hsiung, The effect of residual stress on adhesion of silicon-containing diamond-like carbon coatings, Thin Solid Films 345 (1999) 200-207.
  • [21] M. Larson, P. Hedenqvist, S. Hogmark, Deflection measurements as method to determine residual stress in thin hard coatings on tool materials, Surface Engineering 12 (1996) 43-48.
  • [22] A. O. Sergici, N. X. Randall, Scratch testing of coatings, Advanced Materials and Processes 4 (2006) 1-3.
  • [23] Y. He, I. Apachitei, J. Zhou, T. Walstock, J. Duszczyk, Effect of prior plasma nitriding applied to a hot-work tool steel on the scratch-resistant properties of PACVD TiBN and TiCN coatings, Surface and Coatings Technology 201 (2006) 2534-2539.
  • [24] J. Musil, H. Hruby, Superhard nanocomposite Ti1-xAlxN films prepared by magnetron sputtering, Thin Solid Films 365 (2000) 104-109.
  • [25] Z. Weiss, K. Marshall, Elemental depth profiling of coated and surface-modified materials by GD-OES: hard coatings on cutting tools, Thin Solid Films 308-309 (1997) 382-388.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BWAN-0001-0086
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