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Continuous heating from as-quenched state in a new hot-work steel

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: This work contains a detailed description of the kinetics of phase transformations during tempering of a new hot-work steel. Moreover, the differences in hardness and microstructure of samples of the investigated steel in relationship to the heat treatment were evaluated. Design/methodology/approach: CHT diagram, illustrating the kinetics of phase transformations during continuous heating (tempering) from as-quenched state of investigated steel, was elaborated using a DT 1000 dilatometer of a French company Adamel. In the case of investigations of the microstructural changes, quenched samples were heated with a heating rate of 0.05°C/s to the temperatures of 150, 280 and 650°C. The microstructure of investigated steel were examined using light microscope Axiovert 200 MAT, scanning electron microscope Stereoscan 120 and transmission JEM200CX microscope. The measurements of hardness were performed with the Vickers HPO250 apparatus. Findings: Heating of the investigated steel from the as-quenched state resulted in the occurrence of 4 primary transformations: precipitation of ε carbide, M3C precipitation, transformation of retained austenite and precipitation of alloy carbides of MC and M2C type, nucleating independently. TEM investigations, focused on the determination of a degree of phase transformations during continuous tempering, showed compatibility of the microstructure with the CHT diagram for tested steel. Research limitations/implications: Description of the kinetics of phase transformations during tempering of a new hot working steel. Practical implications: This results may be used to design new technologies of tempering of this steel and new designed hot-work steels. Originality/value: Characterization of kinetics phase transformations during continuous heating from asquenched state in new hot-work steel. Moreover it was shown, that the heating rate from asquenched state has a strong influence on a hardness after tempering.
Rocznik
Strony
517--524
Opis fizyczny
Bibliogr. 17 poz., il., wykr.
Twórcy
autor
autor
autor
  • Faculty of Metals Engineering and Industrial Computer Science, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059 Kraków, Poland, pbala@agh.edu.pl
Bibliografia
  • [1] J. Pacyna, Design the chemical composition of steels, AGH University of Science and Technology, Cracow 1997 (in Polish).
  • [2] J. R. Davis et al., ASM Handbook. Vol. 4. Heat Treating. ASM international 1991.
  • [3] C. R. Brookes, Principles of the heat treatment of plan carbon and low alloy steels. Materials Park: ASM International, 1999.
  • [4] A. K. Sinha, Physical metallurgy handbook, The McGraw-Hill Companies, Inc., 2003.
  • [5] R. Dąbrowski, The effect of vanadium on the structure and properties of quenched and tempered model alloy steels. PhD thesis, AGH University of Science and Technology, Cracow 2002, (in Polish).
  • [6] J. Pacyna, A. Jędrzejewska-Strach, M. Strach, The effect of manganese and silicon on the kinetics of phase transformations during tempering-Continuous Heating Transformation (CHT) curves. Proceedings of the 4th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME’95, Gliwice-Wisła, 1995, 259-262.
  • [7] S. Murphy, J. A. Whiteman, The precipitation of epsilon-carbide in twinned martensite, Metallurgical Transaction 1 (1970) 843-848.
  • [8] Y. Ohmori, I. Tamura, Epsilon carbide precipitation during tempering of plain carbon martensite, Metallurgical Transaction 23A (1992) 2737-2751.
  • [9] D. E. Kaputkin, Reversible martensitic transformation, ageing and low-temperature tempering of iron-carbon martensite, Materials Science and Engineering A 438-440 (2006) 207-211.
  • [10] A. Kokosza, J. Pacyna, Evaluation of retained austenite stability in heat treated cold work tool steel, Proceedings of the 13th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME’2005, Gliwice-Wisła, 2005, 315-318.
  • [11] J. Pacyna, A. Kokosza, Stabilizations of retained austenite in the new steel for working rolls, Proceedings of the 4th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME’95, Gliwice-Wisła, 1995, 263-266.
  • [12] S. Nagakura, Y. Hirotsu, M. Kosunoki, T. Suzuki, Y. Nakamura, Crystallographic Study of the Tempering of Martensitic Carbon Steel by Electron Microscopy and Diffraction, Metallurgical Transaction 14A (1983) 1025-1031.
  • [13] L. Xu, J. Xing, S. Wei, Y. Zhang, R. Long, Study on relative wear resistance and wear stability of high-speed steel with high vanadium content, Wear 262 (2007) 253-261.
  • [14] L. A. Dobrzański, M. Ligraski, Role of Ti in the W-Mo-V high-speed steels, Proceedings of the 4th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME’95, Gliwice-Wisła, 1995, 87-90.
  • [15] L. A. Dobrzański, W. Kasprzak, J. Mazurkiewicz, The structure and properties W-Mo-V-Co high-speed steel of the type 11-2-2-5 after heat treatment, Proceedings of the 4th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME’95, Gliwice-Wisła, 1995, 83-86 (in Polish).
  • [16] P. Bała, The kinetics of phase transformations during tempering and its influence on the mechanical properties, PhD thesis, AGH University of Science and Technology, Cracow 2007.
  • [17] P. Bała, J. Pacyna, J. Krawczyk, The kinetics of phase transformations during tempering in the new hot working steel, Journal of Achievements in Materials and Manufacturing Engineering 22/2 (2007) 15-18.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BWAN-0001-0082
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