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Preparation of wastewater samples for GC-MS analysis of PAHs

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Standard EPA Method 8310 recommends the use of liquid chromatography with fluorescence detection for the determination of PAH compounds. Taking into consideration the advantages of gas chromatography - mass spectrometry (GC - MS) it is important to carry out investigations to optimise wastewater preparation for qualification and quantification of PAHs using this method. The aim of the investigation was to verify the procedure of wastewater preparation for PAHs analysis using GC-MS. The method was evaluated based on experimental recovery values of individual compounds. The experiments were carried out using both raw and biologically treated wastewaters collected from a municipal treatment plant.
Rocznik
Strony
259--264
Opis fizyczny
bibliogr. 17 poz., tab., wykr.
Twórcy
  • Department of Chemistry, Water and Wastewater Technology, Częstochowa University of Technology 69 Dąbrowskiego Str, 42-200 Częstochowa tel.034 32-50-919, fax:034 32 50 496, mwm@is.pcz.czest.pl
Bibliografia
  • [1] Barcelo D., Oubina A., Salau J.S., Perez S., 1998. Determination of PAHs in river water samples by EL1SA., Analytica Chimica Acta, 376, 49-53
  • [2] Clesceri L S., Greenberg A.E., Eaton A.D., 1998, Standard Methods for the Examination of Water and Wastewater, American Public Health Association, Washington
  • [3] Heleleh M.I. H., Al.-Omair A., Nisar A., Gevao B., 2005. Validation of various extraction techniques for the quantitative analysis of polycyclic aromatic hydrocarbons in sewage sludge using gas chromatography-ion trap mass spectrometry, Journal of Chromatography A., 1083, 163-160
  • [4] Lepri L., Bubba M.D., Masi F., Udisti R., Cini R., 2000. Particle size distribution of organic compounds in aqueous aerosols collected from above sewage aeration tanks, Aerosol Science and Technology, 32,404-420
  • [5] Maliszewska-Kordybach B., 1993. The effect of temperature on the rate of disappearance of polycyclic aromatic hydrocarbons from soils, Environmental Pollution, 79, 15-20
  • [6] Manoli E., Samara C, 1999. Occurrence and mass balance of polycyclic aromatic hydrocarbons in the sewage treatment plant, Journal of Environmental Quality, 28
  • [7] Manoli E.. Samara C, Konstantinou I., Albanis T., 2000. Polycyclic aromatic hydrocarbons in the bulk precipitation and surface waters of Northern Greece, Chemosphere, 41, 1845-1855
  • [8] Me Groddy S.E., Farrington J.W., Gschwend P.M., 1996. Comparison of the in situ and desorption sediment-water partitioning of Polycyclic Aromatic Hydrocarbons and Polychlorinated Biphenyls, Environmental Science and Technology, 30, 172-177
  • [9] Miege C, Bouzige M., Nicol S., Dugay J., Pichon V., Hennion M.C., 1999. Selective immunoclean-up followed by liquid or gas chromatography for the monitoring of polycyclic aromatic hydrocarbons in urban waste water and sewage sludges used for soil amendment., Journal of Chromatography A, 859, 29-39
  • [10] Miege C, Dugay J., Hennion M.C., 2003. Optimization, validation and comparison of various extraction techniques for the trace determination of polycyclic aromatic hydrocarbons in sewage sludge by liquid chromatography coupled to diode-array and fluorescence detection, Journal of Chromatography A., 995, 87-97
  • [11] Noordkamp E.R., Grotenhuis T.C., Rulkens W.H., 1997. Selection of an efficient extraction method for the determination of polycyclic aromatic hydrocarbons in contaminated soil and sediment, Chemosphere, 35, 9, 1907-1917
  • [12] Perez S., Guillamon M., Barcelo D., 2001. Quantitative analysis of polycyclic aromatic hydrocarbons in sewage sludge from wastewater treatment plants., Journal of Chromatography A, 938, 57-65
  • [13] Rogers H.R., 1996. Sources, behaviour and fate of organic contminants during sewage treatment and in sewage sludges, The Science of the Total Environmental, 185,3-26
  • [14] Włodarczyk-Makuła M., 2004. Analytical experiences with PAHs analysis in wastewater samples, Laboratorium, Aparatura, Badania LAB, 4, 9-12 (in Polish)
  • [15] Włodarczyk-Makula M., 2005. The Loads of PAHs in wastewater and sewage sludge of municipal Treatment Plant, Polycyclic Aromatic Compounds, 25, 183-194
  • [16] Wolska L., 2002. Miniaturised analytical procedure of determining polycyclic aromatic hydrocarbons and polychlorinated biphenyls in bottom sediments, Journal of Chromatography A., 959,173-180
  • [17] Wolska L., Rawa-Adkonis M., Namieśnik J., 2OO5.Determining PAHs and PCBs in aqueous samples: finding and evaluating sources of error, Analytical and Bioanalytical Chemistry, 6, 1389- 1397
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BUS5-0013-0045
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