Instrumental neutron activation analysis (INAA) for steel analysis and certification

• Autorzy: Polkowska-Motrenko H. , Chajduk E. , Danko B.
• Języki publikacji: EN

Abstrakty

EN

Instrumental neutron activation analysis (INAA) procedure of elemental steel analysis has been elaborated. The reliability of results obtained by the described procedure has been proved in the frame of different proficiency testing/interlaboratory comparison (PT/ILC) programmes, in which the Institute of Nuclear Chemistry and Technology (INCT, Warsaw) took part since 2005. This work summarizes participation of INCT in these exercises and demonstrates the usefulness of INAA to the certification of steel reference materials.

Słowa kluczowe

EN

steel analysis; neutron activation analysis (NAA); proficiency testing/interlaboratory comparison (PT/ILC); certification of steel reference materials

• Wydawca: Institute of Nuclear Chemistry and Technology
• Czasopismo: Nukleonika
• Rocznik: 2011
• Tom: Vol. 56, No. 4
• Strony: 311--315
• Opis fizyczny: Bibliogr. 17 poz., rys.

Twórcy

autor

Polkowska-Motrenko H.

autor

Chajduk E.

autor

Danko B.

• Laboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, 16 Dorodna Str., 03-195 Warsaw, Poland, Tel.: [phone], Fax: [phone],

Bibliografia

• 1. Cincu E, Craciun L, Manera-Grigore I et al. (2009) Application of the INAA technique for elemental analysis of metallic biomaterials used in dentistry. Appl Radiat Isot 67:2133–2136
• 2. Cincu E, Manera I, Manu V et al. (2007) Comparative performance of INAA and other spectroscopy techniques in the elemental analysis of stainless steel materials. J Radioanal Nucl Chem 274:199–205
• 3. European Committee for Iron and Steel Standardization (2002) Certificate of chemical analysis EURONORM-CRM no. 298-1 Duplex Stainless Steel. Swedish Institute for Metals Research, Stockholm
• 4. Gervasio APG, Luca GC, Menegario AA, Reis BF, Filho HB (2000) On-line electrolytic dissolution of alloys in flow injection analysis: determination of iron, tungsten, molybdenum, vanadium and chromium in tool steels by inductively coupled plasma atomic emission spectrometry. Anal Chim Acta 405:213–219
• 5. Granfors M, Gustavsson I (2001) Determination of trace and ultra-trace elements in wet-digested steel using inductively coupled plasma time of flight mass spectrometry (ICP-TOFMS). J Anal At Spectrom 16:1439–1941
• 6. Ida H, Kawai J (2005) An X-ray fluorescence spectrometer with X-ray generator and a secondary target for the determination of Cr in steel. Spectrochim Acta B 60:89–93
• 7. Kimura A, Toh Y, Oshima M, Hatsukawa Y, Goto J (2007) Determination of As and Sb in iron and steel by neutron activation analysis with multiple gamma-ray detection. J Radioanal Nucl Chem 271:323–327
• 8. Liu H, Jiang SJ (2003) Dynamic reaction cell inductively coupled plasma mass spectrometry for determination of silicon in steel. Spectrochim Acta Part B 58:153–157
• 9. Mackey EA, Becker DA, Spatz RO et al. (2004) Certification of NIST Standard Reference Material 1575a Pine Needles and Results of an International Laboratory Comparison. NIST Special Publication 260-156. NIST, Washington
• 10. Moreira EG, Vasconcellos MBA, Saiki M (2005) Instrumental neutron activation analysis applied to the determination of the chemical composition of metallic materials with study of interferences. J Radioanal Nucl Chem 264:45–50
• 11. Oss Giacomelli MB, Borba da Silva JB, Curtius AJ (1998) Determination of Mo and Bi in steels by electrothermal atomic absorption spectrometry after complexation and sorption on activated carbon. Talanta 47:877–881
• 12. Polkowska-Motrenko H, Dybczyński RS, Chajduk E (2010) Certification of reference materials for inorganic trace analysis: the INCT approach. Accredit Qual Assur 15:245–250
• 13. SIMR (2005) Report on Interlaboratory Comparison of elemental composition in Stainless Steel SS1 determined by laboratories from Belgium, Hungary, Poland and Romania using the INAA analytical technique on the Stainless Steel SS1 received from SIMR within the PT Exercise 2004–2005. Swedish Institute for Corrosion and Metals Research, Stockholm
• 14. Tian W, Ni B, Wang P, Cao L, Zhang Y (2001) Metrological role of neutron activation analysis. IA. Inherent characteristics of relative INAA as a primary ratio method of measurement. Accredit Qual Assur 6:488–492
• 15. Tian W, Ni B, Wang P, Cao L, Zhang Y (2002) Metrological role of neutron activation analysis. IB. Inherent characteristics of relative INAA as a primary ratio method of measurement. Accredit Qual Assur 7:7–12
• 16. Zeisler R, Greenberg RR, Mackey EA, Murphy KE, Spatz RO, Tomlin BE (2009) Challenges and success in the use of neutron activation analysis procedures for value assignment of animal serum and bovine liver Standard Reference Materials. J Radioanal Nucl Chem 281:11–15
• 17. Zeisler R, Lindstrom RM, Greenberg RR (2005) Instrumental neutron activation analysis: a valuable link in chemical metrology. J Radioanal Nucl Chem 263:315–319