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New [N,N'-bis-(salicylaldehydene)-1,2-bis-(m-aminophenoxy)eth ane] (MAS) and a common tetra dentate ligand N,N'-ethylenebis(salicylideneimine) (AS) for this study have been prepared, and the new ligand was characterized on the basis of microanalytical data, elemental analysis, UV-visible, IR, 1H NMR and 13C NMR spectra. Selective extraction of Cu(II) from aqueous solution by using N,N'-bis-(salicylalde hydene)-1,2-bis-(m-aminophenoxy)ethane and N,N'-ethylenebis(salicylideneimine) was studied. Separation of Cu(II) from other metal ions such as Cd(II), Pb(II), Ni(II), Co(II) in aqueous solutions of various pH values and complexing reagents (MAS, AS) was described. The separation factors for these metals using these reagents were reported and efficient methods for the separation of Cu(II) from other metal ions were proposed. From the loaded organic phase, Cu(II) stripping was carried out in one stage with different mineral acid solutions. The stripping efficiency was found to be quantitative in case of H2SO4 for MAS and HNO3, H2SO4, HCl for AS.
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Rocznik
Tom
Strony
1591--1600
Opis fizyczny
Bibliogr. 29 poz., rys.
Twórcy
autor
autor
autor
autor
- University of Dicle, Faculty of Sci ence and Art, Chemistry Department, TR 21280, Diyarbakir, Turkey, iaydin@dicle.edu.tr
Bibliografia
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- 11. Sasayama K., Umetani S. and Matsui M., Anal. Chim. Acta, 149, 253 (1983).
- 12. Kara D. and Alkan M., Talanta, 55(2), 415 (2001).
- 13. Kara D. and Alkan M., J. Trace Microprobe Technol, 21(3), 479 (2003).
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- 20. Kara D., Alkan M. and Cakir U., Turk. J. Chem., 25, 293 (2001).
- 21. Kara D., Alkan M. and Gucer S., Anal. Lett., 35(15), 2577 (2002).
- 22. Kara D. and Alkan M., Instrum. Sci. Technol., 32(3), 291 (2004).
- 23. Aydin H., Ziyadanogullari B. and Temel H., Russ. J. Phys. Chem., 79(1), 114 (2005).
- 24. Temel H., Ziyadanogullari B., Alp H., Aydin I., Aydin F. and Ilhan S., Russ. J. Coord. Chem., 32(4), 282 (2006).
- 25. Ziyadanogullari B., Cevizici D., Temel H. and Guzel R, Ann. Chim. (Soc. Chim. Italiana), 97, 287 (2007).
- 26. Ziyadanogullari B., Cevizici D., Temel H. and Ziyadanogullari R.,J. Hazard. Mater., 150,285 (2008).
- 27. Soliman M.E., Mahmoud E.M. and Ahmed A.S., Talanta, 2, 243 (2001).
- 28. (a) Temel H., Taskin T. and Sekerci M., Russ. J. Inorg. Chem., 49(3), 347 (2004); (b) Temel H., Cakir U. and Ugras H.I., Russ. J. Inorg. Chem., 51(2), 274 (2005); (c) Tasker P.-A. and Fleischer E.B., J. Am. Chem. Soc, 92, 7072 (1970); (d) Jaunin R. and Holl R, Helv. Chim. Acta, 192, 1783 (1958); (e) Biernat J-F. and Luboch E., Tetrahedron, 40, 1927 (1984); (f) Cope C, J. Am. Chem. Soc, 57, 572 (1935); (g) Baliah V. and Aparajithan K., J. Indian Chem. Soc, 69, 255 (1992); (h) Bradshaw J.-S., Koyama H., Dalley N.-K. and Izatt R.-M., J. Heterocyclic Chem., 24, 1077 (1987); (i) Biernat J.F., Jerecsek E. and Bujewski A., Polish J. Chem., 53, 2351 (1979); (k) King A.P. and Krespan C.G., J. Org. Chem., 39, 1315 (1974).
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Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BUJ7-0015-0068