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Abstrakty
The bis(4-tert-butylphenolato)dichlorotin(IV) complex of composition SnCl2(OC6H4But-4)2 (1) has been synthesized by the reaction of tin tetrachloride with bimolar amount of 4-t-butylphenol in benzene under reflux and characterized by elemental analyses, molar conductance measurements, molecular weight determination, IR, 1H, 13C NMR and FAB mass spectral techniques. Thermal behaviour of the complex has been investigated using TG-DTA technique. Lewis acid character of (1) has been explored by isolating its addition compounds with some nitrogeneous bases viz. diethylamine, triethylamine, imidazole, benzimidazole (L); 2,2'-bipyridyl, and 1,10-phenanthroline (B) of composition, SnCl2(OC6H4But-4)2×2L and SnCl2(OC6H4But-4)2×B, characterized by physicochemical and IR spectral studies.
Wydawca
Czasopismo
Rocznik
Tom
Strony
1537--1545
Opis fizyczny
Bibliogr. 29 poz., rys.
Twórcy
autor
autor
autor
autor
- Department of Chemistry, Himachal Pradesh University, Summer Hill, Shimla – 171005, India, scchaudhrychem@ya hoo.in
Bibliografia
- 1. Bradley D.C., Mehrotra R.C., Rothwell I.P. and Singh A., "Alkoxo andAryloxo Derivatives of Metals ", Academic Press, London, 445 (2001).
- 2. Malhotra K.C. and Martin R.L., J. Org. Met. Chem., 159, 239 (1982).
- 3. Deng M.Y., Yao Y.M., Shen Q. and Zhang Y, J. Chem. Soc, Dalton Trans., 944 (2004).
- 4. Fanwick A.E., Phomphrai K., Thorn M.G., Vilardo J.S., Trefun CA., Hanna B., Fanwick P.E. and Rothwell I.P., Organometallics, 23, 2146 (2004).
- 5. Yao YM. and Shen Q., Polyhedron, 17, 519 (1998).
- 6. Yao Y.M., Shen Q., Zhang Y. and Xue M.Q., Polyhedron, 20, 3201 (2001).
- 7. Ali M.A., Mirza A.H., Haneti M., Hamid S.A. and Bernhardt P.V., Polyhedron, 24, 383 (2005).
- 8. Yin H.D. and Chem S.W., Inorg. Chim. Acta, 359,3330 (2006); J. Org. Met. Chem., 691,3103 (2006).
- 9. Paman C, Kriza A., Pop V. and Wdrea S., J. Ind. Chem. Soc, 82, 71 (2005).
- 10. Aminabhavi T.M., Biradar N.S., Patil S.B., Radhabarangoudar V.L. and Rudzinski W.E., Inorg. Chim. Acta, 107, 231 (1985). 11. Gielen M., Lelieveld P., de Vos D. and Wilen R., "Metal Based Antitumour Drugs", Freund Publishing House (Belgium), Vol. 2, 95 (1992).
- 12. Smith G.D., Visciglio V.M., Fanwick P.E. and Rothwell LP., Organometallics, 11, 1064 (1992).
- 13. Smith G.D., Fanwick P.E. and Rothwell L.P., Inorg. Chem., 29, 3221 (1990).
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- 15. Taichi K., Teppei K., Shunsuke K. and Keiji M., Tetrahedron Lett., 47(6), 873 (2006).
- 16. Szymaskii H.A., "Interpreted Infrared Spectra", Plenum Press Data Division, New York, Vol. 3, 7 (1961) .
- 17. Socrates G., "Infrared Characteristic Group Frequencies", John Wiley, New York, 46 (1980).
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- 19. Sandhu G.K. and Boparoy N.S., J. Org. Met. Chem., 89,411 (1991).
- 20. Clark R.G., Nielson A.J. and Rickard C.E., Polyhedron, 6, 1765 (1987).
- 21. BeristeinH.J., Spectrochim. Acta, 18,16 (1962); Dyall L.K. and Kamp J.E., Spectrochim. Acta, 11,1076
- (1962) ; Stewant J.E., J. Chem. Phys., 30, 1259 (1959).
- 22. Biradar N.S. and Goudar T.R., J. Inorg. Nucl. Chem., 39, 358 (1977).
- 23. Morgan K.J., J. Chem. Soc, 2343 (1961); Harkins T.R., Walter J.L., Harris O.E. and Freiser H., J. Am. Chem. Soc, 78, 260 (1956).
- 24. Curran B.C., Sen D.N., Mizyshima S. and Qugaliano J.V, J. Am. Chem. Soc, 76, 429 (1956).
- 25. Goodgame D.M.L., Goodgame M., Hayward P.J. and Raymer-Canham G.W., Inorg. Chem., 7, 2447 (1968); Taylor CE. and Underhill A.E., J. Chem. Soc, 368 (1969); Cornilsen B. and Nakamoto K., J. Inorg. Nucl. Chem., 36, 2467 (1974).
- 26. Inskeep R.G., J. Inorg. Nucl. Chem., 24,763 (1962); Schilt A.S. and Taylor R.C., J. Inorg. Nucl. Chem., 9, 211 (1959); MalhotraK.C. and Krishan B., Ind. J. Chem., 14, 869 (1976).
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- 29. Sedaghat T. and Manati S., Inorg. Chem. Commun., 1, 760 (2004).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BUJ7-0015-0062