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Proceedings of the All-Polish Seminar on Mössbauer Spectroscopy OSSM'06, June 18-21, 2006, Koszęcin, Poland
Języki publikacji
Abstrakty
Arrays of Fe3O4 nanowires embedded in mesoporous ordered silica were obtained in two ways: dissolving Fe3+ ions in an aqueous medium and their adsorption on internal and external surfaces, with the use of a Fe-EDTA complex. Magnetite polycrystalline nanowires were characterized by means of X-ray diffraction and 57Fe Mössbauer spectroscopy (MS). The average length of these nanowires is about 70 nm and their diameter is about 3 nm. Mössbauer studies evidenced that the composites consist of very small Fe3O4 particles. Almost 80% of particles exist in a paramagnetic state.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
33--36
Opis fizyczny
Bibliogr. 10 poz., rys.
Twórcy
autor
autor
autor
autor
autor
autor
- Institute of Physics, M. Curie-Skłodowska University, 1 M. Curie-Skłodowska Sq., 20-031 Lublin, Poland, Tel.: +48 81 5376220, Fax: +48 81 5376191, zsurowie@tytan.umcs.lublin.pl
Bibliografia
- 1. Grün M, Unger KK, Schueth F, Lauer I (1997) Characterization of porous solids IV. In: McEnaney B, Mays JT, Rouquerol J et al. (eds) Ordered microporous/mesoporous MCM-41 type absorbents: novel routes in synthesis, product characterization and specification. The Royal Society of Chemistry, pp 81−89
- 2. Kresge CT, Leonowicz ME, Roth WJ, Vartuli JC, Beck JS (1992) Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism. Nature 359:710−712
- 3. Mørup S (1983) Magnetic hyperfine splitting in Mössbauer spectra of microcrystals. J Magn Magn Mater 37:39−50
- 4. Nuzaihan M, Hashim U, Halim NHA, Bajuri SNM (2006) Nanowire formation for single electron transistor using SEM based electron beam lithography (EBL) technique: positive tone vs. negative tone e-beam resist. Nanotechnology 3:266–269
- 5. Wawryszczuk J, Goworek, J, Zaleski R, Goworek T(2003) Positron lifetime in mesoporous silica of MCM-41 type. Langmuir 19:2599−2605
- 6. Xue DS, Li FS (2004) 57Fe Mössbauer study of magnetic nanowires. Hyperfine Interact 156/157:31−40
- 7. 7. Xue DS, Zhang LY, Li FS (2004) Synthesis and Mössbauer study of maghemite nanowire arrays. Hyperfine Interact 156/157:41−46
- 8. Yang SG, Zhu H, Yu DL, Jin ZQ, Tang SL, Du YW (2000) Preparation and magnetic property of Fe nanowire array. J Magn Magn Mater 222:97−100
- 9. Zaleski R, Wawryszczuk J, Goworek J, Borówka A, Goworek T (2003) Vacuum removal of the template in MCM-41 silica studied by the positron annihilation method. Journal Colloid Interface Sci 262:466−473
- 10. Zhou P, Xue D, Luo H, Shi H (2002) Temperature dependence of the Mössbauer effect on prussian blue nanowires. Hyperfine Interact 142:601−606
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BUJ6-0011-0045