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For the first time the 31P solid-state NMR CP/MAS technique was applied to determine the amount of C-P forms in the total phosphorus in sea anemones. Signals of phosphonates (ca 20 ppm) and phosphates (ca 0 ppm) are well resolved and the phosphonate/ phosphate ratios were easily calculated. Sea anemones Anemonia sulcata from the Adriatic Sea contain 41-54% of phosphorus as phosphonates (P-C). 31PNMRanalysis of lipids was also performed.
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Tom
Strony
573--581
Opis fizyczny
Bibliogr. poz. 15, rys.
Twórcy
autor
- Department of Chemistry, Technical University of Łódź, Żeromskiego 116, 90-924 Łódź, Poland
Bibliografia
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- 2.Mastalerz P. and Kafarski P., Naturally Occurring Aminophosphonic and Aminophosphinic Acids, In: Aminophosphonic and Aminophosphinic Acids, Kukhar V.P., Hudson H. R., (Eds.), Wiley, 2000, pp. 1-31.
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- 6.Glonek T., 31 P NMR in the Analysis of Extracted Tissue of Phospholipids, In: Phosphorus-31 NMR Spectral Properties in Compound Characterization and Structural Analysis, Quin L.D., Verkade J.G., (Eds.), VCH Publishers, Inc., New York, 1999, pp. 283-294.
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- 9. Kittredge J.S., Isbell A.F. and Hughes R.R., Biochemistry, 6, 289 (1967).
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- 11.Clark L.L., Ingall E.D. and Benner R., Nature, 393, 426 (1998).
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- 15.Hägele G., Szakâcs Z., Ollig J., Hermens S. and Pfaff C., Heteroatom Chem., 11, 562 (2000).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BUJ3-0002-0053