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Heterocyclic derivatives of aminomethylphosphonic acid were obtained in a one-pot procedure, by treatment of the corresponding heterocyclic aldimines with a mixture of trimethyl phosphite and bromotrimethylsilane (BrTMS). A reagent for phosphorylation of the imines in this case was the tris(trimethylsilyl)phosphite, formed in situ in a reaction mixture. The silylated esters formed were hydrolyzed to the final aminophosphonic acids.
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Tom
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1271--1275
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- Institute of Organic Chemistry, Biochemistry and Biotechnology, Wroclaw University of Technology, 50-370 Wroc3aw, Poland
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Bibliografia
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bwmeta1.element.baztech-article-BUJ1-0019-0034