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Structure and adhesion of thin coatings deposited by PVD technology on the X6CrNiMoTi17-12-2 and X40CrMoV5-1 steel substrates

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Języki publikacji
PL
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Purpose: The main aim of the research was the investigation of the structure and adhesion of AlTiCrN, CrAlSiN and TiAlSiN coatings deposited by physical vapour deposition technology on the X40CrMoV5-1 hot work tool steel and the X6CrNiMoTi17-12-2 austenitic stainless steel substrate. Design/methodology/approach: Observations of surface and microstructure of the deposited coatings were carried out on cross sections in the SUPRA 35 scanning electron microscope. The microhardness tests of coatings were made with the SHIMADZU DUH 202 ultra-microhardness tester. The cohesion and adhesion properties of the coatings were made using the scratch test on the CSEM REVETEST device. Findings: It was found that the coatings present a compact structure, without any visible delaminations or defects. The morphology of the fracture of coatings is characterized by a dense structure, in some cases there is a columnar structure. The coatings demonstrated good adhesion to the substrate. The critical load LC2 lies within the range of 39-47 N, depending on the coating and substrate type. The coatings demonstrate a high hardness (~40 GPa). Practical implications: The process of covering steels with the thin PVD coatings is currently the most commonly method used to extend their life. Investigations of those coatings determining their scratchresistant properties and structure enable to pick out the optimum coatings for given industrial applications. Originality/value: The results of the investigation provide useful information on microstructure and scratch-resistant properties of the quaternary coatings deposited on the hot work tool steels and austenitic stainless steels.
Słowa kluczowe
Rocznik
Strony
40--47
Opis fizyczny
Bibliogr. 20 poz.
Twórcy
autor
autor
  • Division of Materials Processing Technology, Management and Computer Techniques in Materials Science, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland, krzysztof.lukaszkowicz@polsl.pl
Bibliografia
  • [1] K. Lukaszkowicz, L.A. Dobrzański, A. Zarychta, Structure, chemical and phase compositions of coatings deposited by reactive magnetron sputtering onto the brass substrate, Journal of Materials Processing Technology 157-158 (2004) 380-387.
  • [2] L.A. Dobrzański, K. Lukaszkowicz, A. Kriz, Properties of the multi-layer Ti/CrN and Ti/TiAlN coatings deposited with the PVD technique onto the brass substrate, Journal of Materials Processing Technology 143-144 (2003) 832-837.
  • [3] D. Pakuła, L.A. Dobrzański, K. Gołombek, M. Pancielejko, A. Křiž, Structure and properties of the Si3N4 nitride ceramics with hard wear resistant coatings, Journal of Materials Processing Technology 157-158 (2004) 388-393.
  • [4] D. Pakuła, L.A. Dobrzański, A. Križ, M. Staszuk, Investigation of PVD coatings deposited on the Si3N4 and sialon tool ceramics, Archives of Materials Science and Engineering 46/1 (2010) 53-60.
  • [5] L.A. Dobrzański, M. Staszuk, J. Konieczny, W. Kwaśny, M. Pawlyta, Structure of TiBN coatings deposited onto cemented carbides and sialon tool ceramics, Archives of Materials Science and Engineering 38/1 (2009) 48-54.
  • [6] K. Lukaszkowicz, J. Szewczenko, M. Pancielejko, Structure, mechanical properties and corrosion resistance of PVD gradient coatings deposited onto the X40CrMoV5-1 hot work tool steel substrate, International Journal of Materials and Product Technology 39 (2010) 148-158.
  • [7] L.A. Dobrzański, K. Lukaszkowicz, K. Labisz, Structure, texture and chemical composition of coatings deposited by PVD techniques, Archives of Materials Science and Engineering 37/1 (2009) 45-52.
  • [8] L.A. Dobrzański, K. Lukaszkowicz, Erosion resistance and tribological properties of coatings deposited by reactive magnetron sputtering method onto the brass substrate, Journal of Materials Processing Technology 157-158 (2004) 317-323.
  • [9] L.A. Dobrzański, D. Pakuła, Structure and properties of the wear resistant coatings obtained in the PVD and CVD processes on tool ceramics, Materials Science Forum 513 (2006) 119-133.
  • [10] M. Drak, L.A. Dobrzański, Corrosion of Nd-Fe-B permanent magnets, Journal of Achievements in Materials and Manufacturing Engineering 20 (2007) 239-241.
  • [11] L.A. Dobrzański, D. Pakuła, Comparison of the structure and properties of the PVD and CVD coatings deposited on nitride tool ceramics, Journal of Materials Processing Technology 164-165 (2005) 832-842.
  • [12] L.A. Dobrzański, D. Pakuła, A. Křiž, M. Soković, J. Kopač, Tribological properties of the PVD and CVD coatings deposited onto the nitride tool ceramics, Journal of Materials Processing Technology 175 (2006) 179-185.
  • [13] K. Lukaszkowicz, J. Sondor, A. Kriz, M. Pancielejko, Structure, mechanical properties and corrosion resistance of nanocomposite coatings deposited by PVD technology onto the X6CrNiMoTi17-12-2 and X40CrMoV5-1 steel substrates, Journal of Materials Science 45/6 (2010) 1629-1637.
  • [14] Y. He, I. Apachitei, J. Zhou, T. Walstock, J. Duszczyk, Effect of prior plasma nitriding applied to a hot-work tool steel on the scratch-resistant properties of PACVD TiBN and TiCN coatings, Surface and Coatings Technology 201 (2006) 2534-2539.
  • [15] S.J. Bull, Failure mode maps in the thin film scratch adhesion test, Tribology International 30/7 (1997) 491-498.
  • [16] K. Lukaszkowicz, A. Czyżniewski, W. Kwaśny, M. Pancielejko, Structure and mechanical properties of PVD coatings deposited onto the X40CrMoV5-1 hot work tool steel substrate, Vacuum (2011) doi:10.1016/j.vacuum.2011.10.031
  • [17] S. Veprek, M.J.G. Veprek-Heijman, Industrial applications of superhard nanocomposite coatings, Surface and Coatings Technology 202 (2008) 5063-5073.
  • [18] J. Soldan, J. Neidhardt, B. Sartory, R. Kaindl, R. Cerstvy, P.H. Mayrhofer, R. Tessadri, P. Polcik, M. Lechthaler, C. Mitterer, Structure-property relations of arc-evaporation Al-Cr-Si-N coatings, Surface and Coatings Technology 202 (2008) 3555-3562.
  • [19] G.S. Fox-Rabinovich, K. Yamomoto, S.C. Veldhuis, A.I. Kovalev, G.K. Dosbaeva, Tribological adaptability of TiAlCrN PVD coatings under high performance dry machining conditions, Surface and Coatings Technology 200 (2005) 1804-1813.
  • [20] P. Burnett, D. Rickerby, The relationship between hardness and scratch adhesion, Thin Solid Films 154 (1987) 403-416.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BSL9-0053-0005
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