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Structure of TiBN coatings deposited onto cemented carbides and sialon tool ceramics

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Języki publikacji
PL
Abstrakty
EN
Purpose: The aim of this paper was investigated structure of sintered carbides WC-Co type and sialon tool ceramics with wear resistance ternary coatings TiBN type deposited by cathodes arc evaporation process (CAE-PVD). Design/methodology/approach: Observation of fracture and topography studied coatings were done by scanning electron microscope. Chemical composition was determine by energy dispersive spectrometry (EDS) method. Thin foils of substrates and coatings by transmission electron microscopy (TEM) was done. Phases composition analysis carried out by XRD and GIXRD method. Findings: The investigated PVD gradient coatings deposited by CAE-PVD method are demonstrating fine-grained structure. The TiN, TiB and TiB2 phases were found in coatings and Β-Si3N4 phase was found in sialon tool ceramics. Coating onto sialon tool ceramics reveal shallow pinhole while coating onto cemented carbide is without discontinuity. Research limitations/implications: In the future investigations will progress for mechanical properties, e.g. roughness, microhardness, adhesion strength and operating properties. Originality/value: In this work the influence of parameters deposited coatings by CAE-PVD technique on structure and phases composition the ternary TiBN gradient coatings were investigated.
Rocznik
Strony
48--54
Opis fizyczny
Bibliogr. 20 poz.
Twórcy
autor
autor
autor
autor
  • Division of Materials Processing Technology, Management and Computer Techniques in Materials Science, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland, leszek.dobrzanski@polsl.pl
Bibliografia
  • [1]H. Holzschuh, Deposition of Ti–B–N (single and multilayer) and Zr–B–N coatings by chemical vapor deposition techniques on cutting tools, Thin Solid Films 469–470 (2004) 92–98.
  • [2]L.A. Dobrzański, M. Staszuk, M. Pawlyta, W. Kwaśny, M. Pancielejko, Characteristic of Ti(C,N) and (Ti,Zr)N gradient PVD coatings deposited onto sintered tool materials, Journal of Achievements in Materials and Manufacturing Engineerting, 31/2 (2008) 629-634.
  • [3]L.A. Dobrzański, K. Gołombek, Structure and properties compound coatings TiN+gradient or multi (Ti,Al,Si)N+TiN types deposited onto cermet tools, Proceedings of the Scientific Conference “Materials, Mechanical and Manufacturing Engineering”, M3E 2005 133-140. [4]K. Lukaszkowicz, L.A. Dobrzański, M. Staszuk, M. Pancielejko, Comparison of the PVD gradient coatings deposited onto X40CrMoV5-1 and HS6-5-2 tool steel substrate, Journal of Achievements in Materials and Manufacturing Engineerting, 27/1 (2008) 79-82.
  • [5]L.A. Dobrzański M. Staszuk, J. Konieczny, J. Lelątko, Structure of gradient coatings deposited by CAE-PVD techniques, Journal of Achievements in Materials and Manufacturing Engineerting, 24/2 (2007) 55-58.
  • [6]P. Cichorz, Cutting tools, WNT, Warszawa 2006 (in Polish).
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  • [9]M. Sopińska-Lizer, Sialon ceramic obtained from a powder by carbothermic reaction – physical-chemical production bases and properties, Scientific books, Silesian University of Technology Publishing House, Gliwice 2000.
  • [10]S. Hampshire, Silicon nitride ceramics – review of structure, processing and properties, Journal of Achievements in Materials and Manufacturing Engineering 24/1 (2007) 43-50. [11]K.H. Jack, Review: SiAlONs and related nitrogen ceramics, Journal of Materials Science 11 (1976) 1135-1157.
  • [12]L.A. Dobrzański, Engineering materials and materials design. Fundamentals of materials science and physical metallurgy, WNT, Warsaw-Gliwice, 2006 (in Polish).
  • [13]Y. He, I. Apachitei, J. Jhou, W. Walstock, J. Duszczyk, Effect of prior plasma nitriding applied to a hot-work tool steel on the scratch-resistant properties of PACVD TiBN and TiCN coatings, Surface & Coatings Technology 201 (2006) 2534–2539.
  • [14]T.P. Mollart, J. Haupt, R. Gilmore, W. Gissler, Tribological behaviour of homogeneous Ti-B-N, Ti-B-N-C and TiN/h-BN/TiB2 multilayer coatings, Surface and Coatings Technology 86-87 (1996) 231-236.
  • [15]W. Gissler, P.N. Gibson, Titanium implantation into born nitride films and ion-beam mixing of titanium born nitride multilayers, Ceramics International 22 (1996) 335-340. [16]Y.H. Lu, Z.F. Zhou, P. Sit, Y.G. Shen, K.Y. Li, Haydn Chen, X-Ray photoelectron spectroscopy characterization of reactively sputtered Ti–B–N thin films, Surface & Coatings Technology 187 (2004) 98– 105.
  • [17]Z. Werner, J. Stanisławski, J. Piekoszewski, E.A. Levashov, W. Szymczyk, New types of multi-component hard coatings deposited by ARC PVD on steel pre-treated by pulsed plasma beams, Vacuum 70 (2003) 263–267.
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  • [19]K. Gołombek, J. Mikuła, D. Pakuła, L.W. Żukowska, L.A. Dobrzański, Sintered tool materials with multi - component PVD gradient coatings, Journal of Achievements in Materials and Manufacturing Engineerting 31/1 (2008) 15-22.
  • [20]L.A. Dobrzański, K. Gołombek, Gradient coatings deposited by Cathodic Arc Evaporation: characteristic of structure and properties, Journal of Achievements in Materials and Manufacturing Engineerting, 14 (2006) 48-53.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BSL9-0031-0007
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