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Laser nitriding of the surface layer of Ti6Al4V titanium alloy

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Języki publikacji
PL
Abstrakty
EN
Purpose: The purpose of this paper is modification of the surface layer of the Ti6Al4V titanium alloy microstructure and properties by laser remelting in nitrogen atmosphere. Design/methodology/approach: Laser treatment was performed on the samples in stream of nitrogen. Microstructure of laser treated layer was investigated by using Epiphot 300 optical microscope and Novascan 30 scanning electron microscope. Phase composition was determined using X-ray diffractometry. The roughness of surface of treated material was examined using topography scanning system T 8000 made by Hommelwerke GMBH. The Vickers hardness under load of 1.96 N was measured on the cross sections of surface layer. The wear properties of alloyed zone were tested on the testing machine T 08M using ‘pin on disc’ test. Findings: Laser remelting process has produced a surface layer consists of hard ceramics particles of TiN and Ti2N phases spaced in martensitic matrix. The hardness of surface layer increases clearly in comparison with untreated alloy due to formation of TiN and Ti2N particles and depends on the volume fraction of nitrides. Their maximum value of the hardness (1500 HV 0.2) occurs on the surface of laser treated zone. Wear resistance of laser nitrided layer increases considerably in relation to base alloy. Research limitations/implications: Research range was limited to microstructure, phase composition, hardness, fractography and wear resistance investigations. To estimate the influence of the laser nitriding process on corrosion resistance of the layer additional examinations will be performed in future research. Practical implications: Laser remelting of titanium alloy in nitrogen atmosphere makes possible to obtain coatings composed of ceramic particles spaced in metallic matrix characterised by high hardness and wear resistance. Originality/value: The range of investigation included microstructure, phase composition, hardness as well as fractographic estimation and wear properties enables analysis of laser nitriding process efficienty.
Rocznik
Strony
25--28
Opis fizyczny
Bibliogr. 16 poz.
Twórcy
autor
  • Department of Materials Science, Rzeszów University of Technology, ul. W. Pola 2, 35-959 Rzeszów, Poland, ryfil@prz.edu.pl
Bibliografia
  • [1] L.A. Dobrzański, K. Labisz, A. Klimpel, J. Lelątko, Modelling of gradient layer properties of the 32CrMoV12-27 surface layer alloyed with WC powder, Journal of Achievements in Materials and Manufacturing Engineering 20 (2007) 343-346.
  • [2] M. Bonek, L.A. Dobrzański, M. Piec, E. Hajduczek, A.Klimpel, Crystallisation mechanism of laser alloyed gradient layer on tool steel, Journal of Achievements in Materials and Manufacturing Engineering 20 (2007) 411-414.
  • [3] L.A. Dobrzański, E. Jonda, A. Kriz, K. Lukaszkowicz, Mechanical and tribological properties of the surface layer of the hot work tool steel obtained by laser alloying, Archives of Materials Science and Engineering 28/7 (2007) 389-396.
  • [4] L.A. Dobrzański, E. Jonda, K Lukaszkowicz, A. Kriz, Structure and tribological behavior of structure layer of laser modified X40CrMoV5-1 steel, Journal of Achievements in Materials and Manufacturing Engineering 18 (2007) 343-346.
  • [5] M. Szkodo, Cavitation erosion behaviour of laser processed Fe-Cr-Mn and Fe-Cr-Co alloys, Journal of Achievements in Materials and Manufacturing Engineering 18 (2006) 239-242.
  • [6] W. Serbiński, B. Majkowska: Microstructure and corrosion properties f the laser treated SUPERSTON alloy, Journal of Achievements in Materials and Manufacturing Engineering 18 (2006) 415-418.
  • [7] A. Zieliński, M. Jażdżewska, A. Narożniak-Łuksza,W. Serbiński, Surface structure and properties of Ti6Al4V alloy laser melted at cryogenic conditions, Journal of Achievements in Materials and Manufacturing Engineering 18 (2006) 423-426.
  • [8] L.A. Dobrzański, E. Jonda, A. Polok, Comparison of the abrasion wear resistance of the X40CrMoV5-1 and 55NiCrMoV7 hot work tool steels with their surface layer enriched with the ceramic powders, Journal of Achievements in Materials and Manufacturing Engineering 15 (2006) 32-38.
  • [9] R. Filip, Alloying of surface layer of the Ti-6Al-4V titanium alloy through the laser treatment, Journal of Achievements in Materials and Manufacturing Engineering 15 (2006) 174-180.
  • [10] P. Jiang, X.L. He, X.X Li, L.G. Yu, H.M. Wang, Wear resistance of a laser surface alloyed Ti-6Al-4V alloy, Surface and Coatings Technology 130 (2000) 24-28.
  • [11] H.A. Wriedt, J.L. Murray, The N-Ti (nitrogenium-titanium) system, Bulletin of Alloy Phase Diagrams 4 (1987) 378-388.
  • [12] W. Lengauer, P. Ettmayer, The crystal structure of new phase in the Titanium – Nitrogen system, Journal of the Less Common Metals 120 (1986) 153-156.
  • [13] W. Lengauer, P. Ettmayer, The crystal structure of eta-Ti3N2-x; An additional new phase in the Ti– N system, Journal of the Less Common Metals 125 (1986) 55-58.
  • [14] H.W Bergmann, S. Lee, Properties of laser gas alloyed titanium, Proceedings of the 3rd Conference Lasers in Manufacturing, Paris, 1986, 221-232.
  • [15] J.L. Murray, Phase Diagrams of Binary Titanium Alloys,ASM, Metals Park, OH, 1987.
  • [16] C. Hu, H. Xin, L.M. Watson, T.N. Baker, Analysis of the phases developed by laser nidriding Ti-6Al-4V alloys, Acta Materialia 10 (1997) 4311-4322.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BSL9-0030-0005
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