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Purpose: Ultrafine reinforcement particles are formed as product of reaction between reactive components. Those kinds of materials have good mechanical properties (higher yield stress and creep resistance). Via in situ reaction between liquid metal and reacting substance (solid or gas) is possible to obtain aluminium matrix composites similar to SAP composites by casting methods. Presented results of researches concerning possibilities of obtaining ultrafine aluminium nitride particles via in situ reaction between aluminium alloys (with addition of Mg) and nitrogen. Design/methodology/approach: The experiments were performed in a reaction chamber, heated in a sylite furnace where the 0.3 MPa pressure of nitrogene were obtained and autoclave furnace at gas pressure of 1 MPa. Samples were heated at 1000°C and held at that temperature for 1 hour at the suitable gas pressure. Findings: The research has shown, that vaporization of Mg and indirect nitridation depend on gas pressure in reaction chamber. At high pressure (1 MPa) of N2 in situ reaction procced in limited scope. Practical implications: Using the in situ reaction in order to form AlN dispersion reinforcement in the aluminium alloy matrix seems possible but the control of the reaction is difficult. Originality/value: During the liquid-phase process, the following factors determine the possibility of controlling the process of the dispersion reinforcement phases’ formation: the matrix alloy composition, the temperature, the reactive gas pressure and the time of synthesis.
Wydawca
Rocznik
Tom
Strony
17--20
Opis fizyczny
Bibliogr. 15 poz.
Twórcy
autor
autor
- Department of Alloys and Composite Materials Technology, Faculty of Materials Science and Metallurgy, Silesian University of Technology, ul. Krasińskiego 8, 40-019 Katowice, Poland, maciej.dyzia@polsl.pl
Bibliografia
- [1] S.C. Tjong, Z.Y. Ma1, Microstructural and mechanical characteristics of in situ metal matrix composites, Materials Science and Engineering 29 (2000) 49-113.
- [2] Y.J. Kim, H. Chung, S.J.L Kang, In situ formation of titanium carbide in titanium powder compacts by gas-solid reaction, Composites A32 (2001) 731-738.
- [3] E. Fra , A. Janas, A. Kolbus, M. Górny, Synthesis of the "in situ" Al-TiC and Cu-Ti composites by using the reactive gas, Materials Engineering 2 (2000) 48-55.
- [4] J. Śleziona, B. Formanek, A. Olszówka-Myalska, Obtaining of aluminium alloys matrix composites reinforced with fine dispersed ceramic and intermetallic particles, Materials Engineering 3 (2002) 122-128.
- [5] J. Śleziona , M. Dyzia, J. Myalski, J. Wieczorek, The structure and properties of sinters produced from composite powders Al-Al2O3-Al3Fe-Al3Ti, Journal of Materials Processing Technology 162-163 (2005) 127-130.
- [6] A. Dolata-Grosz, J. Śleziona, B. Formanek, J. Wieczorek: Al-FeAl-TiAl-Al2O3 composite with hybrid reinforcement, Journal of Materials Processing Technology 162-163 (2005) 33-38.
- [7] M.K. Prekumar, M.G. Chu, Al-TiC particulate composite produced by a liquid state in situ process, Materials Science and Engineering A202 (1995) 172-178.
- [8] J.G. Lee, H.A. Ma, X.L. Lee, Y.J. Zheng, G.H. Zuo, X. Jia, Preparation and characterization of Al/AlN composites sintered under high pressure, Journal of Materials Science 42 (2007) 9460-9464.
- [9] J. Vicens, M. Chedru, J.L. Chermant, New Al-AlN composites fabricated by squeeze casting: interfacial phenomena, Composites A33 (2002) 1421-1423.
- [10] Y. Kameshima, M. Irie, A. Yasumori, K. Okada, Mechanochemical effect on low temperature synthesis of AlN by direct nitridation metod, Solid State Ionics 172 (2004) 185-190.
- [11] J. Cintas , F.G. Cuevas, J.M. Montes, E.J. Herrera, Highstrength PM aluminium by milling inammonia gas and sintering, Scripta Materialia 53 (2005) 1165-170.
- [12] Q. Hou, R. Muthharasan, M. Koczak, Feasibility of aluminium nitride formation in aluminium alloys, Materials Science and Engineering A195 (1995) 121-129.
- [13] Y. Huashun, J.D. Kim, S.B. Kang, The formation of AlN and TiN particles during nitrogen bearing gas injection into Al-Mg-Ti melt, Materials Science Engineering A386 (2004) 318-325.
- [14] H. Scholz, P. Greil, Nitridation reactions of molten Al-(Mg, Si) alloys, Journal of Materials Science 26 (1991) 669-677.
- [15] T.B. Sercombe, G.B. Schaffer, On the role of magnesium and nitrogen in the infiltration of aluminium by aluminium for rapid prototyping applications, Acta Materialia 52 (2004) 3019-3025.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BSL8-0028-0004