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The strengthening of weight heavy alloys during heat treatment

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The results of studies of W-Ni-Co-Fe experimental alloy, with chemical composition assuring a possibility of producing Ni-based supersaturated solid solution are presented. The alloy was prepared from tungsten, nickel, cobalt and iron powders which were first mixed then melted in a ceramic crucible where they slowly solidified in hydrogen atmosphere. Next specimens were cut from the casting and heated at a temperature 950oC. After solution treatment the specimens were water quenched and then aged for 20 h at a temperature 300oC. The specimens were subjected to microhardness measurements and structure investigations. The latter included both conventional metallography and SEM observations. Moreover, for some specimens X-ray diffractometry studies and TEM investigations were conducted. It was concluded that quenching lead to an increase of tungsten concentration in nickel matrix which was confirmed by Ni lattice parameter increase. Aging of supersaturated solid solution caused strengthening of the Ni-based matrix, which was proved by hardness measurements. The TEM observation did not yield explicit proofs that the precipitation process could be responsible for strengthening of the alloy.
Rocznik
Strony
75--80
Opis fizyczny
Bibliogr. 13 poz., rys., tab., wykr.
Twórcy
autor
autor
autor
  • Institute of Mechanics and Printing, Faculty of Production Engineering, Warsaw University of Technology, ul. Narbutta 85, 02-524 Warszawa, Poland, mkaczoro@wip.pw.edu.pl
Bibliografia
  • [1] S. Pappu S., Kenedy C., Murr L. E., Magness L. S., Kapoor D.: Microstructure analysis and comparison of tungsten alloy rod and [001] oriented columnar-grained tungsten rod ballistic penetrators, Mat. Sci. Eng., A 262 (1999) p.115.
  • [2] He Z., Courtney T. H.: Crystallization and thermal stability of mechanically alloyed W-NiFe noncrystaline materials, Mat. Sci. Eng., A 315 (2001) p.166.
  • [3] Mudlle B. C., Edmonds D. W.: Acta Metall., 33 (1985)p. 2119.
  • [4] Edmonds D. W.: Structure/Property Realtionships in Sintered Heavy Alloys, Refractory Metals & Hard Materials, 10 (1991) p.15.
  • [5] Thomas G., Goringe M. J.: Transmission Electron Microscopy of Materials, A Willey-Interscience Publication, New York, 1979.
  • [6] Hirsch P. B., Howie A., Nicholson R. B., Pashley D. W., Whelan M. J.: Electron Microscopy of Thin Crystals, London, Butterworths, 1965.
  • [7] Amelinx S., Gevers R., Remaut G, Van Landuyt J.: Modern Diffraction and Imaging Techniques in Materials Science, North-Holland Publ. Co., Amsterdam, 1969.
  • [8] Dirnfeld S. F. Shechtman D.: Microstructure and crystallography of unidirectionally solidified Ni-W eutectic alloy, Metallurgical an Materials Transactions A, 16 (1985) pp. 1185-1193.
  • [9] Kaczorowski M., Skoczylas P., Nowak W.: The study of precipitation hardening of weight heavy alloys, Archives of Foundry Engineering, 2008, vol.8, Nr 1, pp. 167-174.
  • [10] Binary Phase Diagram, ed. T.B. Massalski 1990, ASM International.
  • [11] Terashima H., Ohta Y., Nakagawa Y.G.: \beta-Ni4W phase precipitation in nickel-based superalloy, Materials Science and Engineering, 88 (1987), pp. 15-18.
  • [12] Kingetsu T., Yamamoto M., Nenno S., Hindenori.: Field-Ion Microscope studies of Ni4W Type Ordering in the Near-Surface of Ni-16,6at % W Alloy, Jap. Journal of Applied Phys., 20 (1981) pp.1407-1411.
  • [13] Jones D. R. H., Benson J. P., Ison K. T.: Electron microscopy and electron diffraction study of ordering in Ni4W, J. Mat. Sci., 11(1974) pp. 1175-1179.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPZ7-0006-0039
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