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Katalizatory niklowe i rutenowo-niklowe na nośnikach zawierających zeolit ZSM-5 i tlenek glinu. Wybrane właściwości fizykochemiczne i katalityczne

Autorzy
Masalska A.
Wybrane pełne teksty z tego czasopisma
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Warianty tytułu
EN
Nickel catalysts and ruthenium-nickel catalysts supported on AI2O3+ZSM-5: Physicochemical and catalytic properties
Języki publikacji
PL
Abstrakty
PL
Przedstawiono wyniki prac dotyczących charakterystyki właściwości fizykochemicznych zeoli-tów, układów dwuskładnikowych ZSM-5+Al203 oraz katalizatorów niklowych i rutenowo-niklo-wych zawierających jako nośnik układ dwuskładnikowy w powiązaniu ze składem chemicznym, sposobem otrzymywania i ich właściwościami katalitycznymi. Określono wpływ sposobu łączenia zeolitu z wodorotlenkiem glinu na teksturę i właściwości kwasowe układów ZSM-5+Al203 oraz wpływ metody preparatyki katalizatorów niklowych na oddziaływania metal-nośnik i ich aktywność w krakingu oraz selektywnym krakingu węglowodorów parafinowych o łańcuchu normalnym (oraz ich monometylowych izomerów). Ustalono zależność między składem chemicznym, sposobem otrzymywania katalizatorów niklowych i rutenowo-niklowych a ich aktywnością uwodorniającą w konwersji węglowodorów aromatycznych. Określono korelację pomiędzy stosunkiem liczby centrów metalicznych do liczby centrów kwasowych w katalizatorach niklowych a ich selektywnością w reakcji uwodornienia toluenu. Udokumentowano wpływ warunków obróbki termicznej i sposobu wprowadzania niklu na oddziaływania metal-nośnik oraz wpływ ilości rutenu, rodzaju prekursora rutenu i sposobu preparatyki katalizatorów niklowych na oddziaływania metal-metal (Ru-Ni) i metal-nośnik oraz właściwości uwodorniające katalizatorów w konwersji 1 -metylonaftalenu. Opracowano formułę katalizatora umożliwiającego otrzymanie zadowalających ilości produktów w dwóch przeciwstawnych reakcjach (uwodornienie-reakcja egzotermiczna, kraking-reakcja endo-termiczna); w optymalnej temperaturze reakcji podczas przemiany frakcji oleju napędowego otrzymano produkty o korzystnych właściwościach niskotemperaturowych przy jednoczesnym ponad 50-procentowym stopniu odaromatyzowania surowca. Opisano zależność pomiędzy składem chemicznym i właściwościami fizykochemicznymi katalizatorów a stopniem ich zakoksowania oraz charakterem depozytów węglowych, ze szczególnym uwzględnieniem podatności koksu na utlenienie.
EN
ZSM-5 zeolites, two-component ZSM-5+Al203 systems, nickel catalysts and nickel-ruthenium catalysts supported on the ZSM-5+Al203 were analyzed for physicochemical and catalytic properties, which were related to the preparation method used, as well as to the chemical composition. Consideration was given to the problem of how the method of combining the zeolite with aluminium hydroxide affects the texture and acid properties of ZSM-5+Al203 systems, and how the method of nickel catalyst preparation influences metal-support interactions and catalyst activity in cracking and selective cracking (dewaxing) straight-chain paraffin hydrocarbons and their monomethyl isomers. For nickel and nickel-ruthenium catalysts, a correlation was found to occur between chemical composition, preparation method and hydrogenating activity in aromatics conversion. For nickel catalysts, a correlation was established between the metal to acid ratio and selectivity in toluene hydrogénation. It has been demonstrated that the method of nickel incorporation and the conditions of thermal treatment influence the nickel-support interactions, and that the quantity of ruthenium, the type of ruthenium precursor and the method of nickel catalyst preparation impact on the metal-metal (Ru-Ni) and metal-support interactions, as well as on the hydrogenating properties of the catalysts in the conversion of 1-methyl-naphthalene. A catalyst formula was derived for obtaining the desired quantity of products which form during conversion of the diesel oil fraction in two 'opposite' reactions (exothermic hydrogénation reaction and en-dothermic cracking reaction). The products attained at optimal temperature displayed sufficiently good cold-flow properties, and the dearomatization of the feed exceeded 50%. The chemical composition and physicochemical properties of the catalysts were related to the degree of coking and to the character of the carbonaceous deposits, particular consideration being given to the oxidability of the coke.
Słowa kluczowe
PL
EN
Wydawca
Oficyna Wydawnicza Politechniki Wrocławskiej
Czasopismo
Prace Naukowe Wydziału Chemicznego Politechniki Wrocławskiej. Monografie
Rocznik
2010
Tom
Nr 7, nr 7
Strony
190--190
Opis fizyczny
s., bibliogr. 298 poz.
Twórcy
autor
Masalska A.
  • Wydział Chemiczny Politechniki Wrocławskiej, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław.
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