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Nanoalumina obtained by pyrosol method

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Ceramic materials are interesting due to their properties such as chemical and thermal stability, corrosion resistance, biocompatibility, piezoelectricity, high dielectricity. Also, nano-sized materials may have properties different from the micro scale materials. Pyrosol method is an alternative method to obtain nanoscale particles. In this study alumina particles were prepared by pyrosol method using AlCl3 (0.1 M and 0.05 M) as precursor solutions. The particles were obtained by maintaining the temperature of 400 °C in the pyrolysis furnace. Then, the powders were heat treated at 1000 °C for 2 hours. The X-ray diffraction analyses indicated that the obtained nanoparticles were identified as a mixture of a and g crystalline alumina. Scanning electron microscopy images showed that the prepared Al2O3 nanoparticles obtained from the concentration of 0.05 M had smaller dimensions than those obtained from the concentration of 0.1 M. Images of transmission electron microscopy showed spherical particles with the median diameter approximately of 150 nm, using as precursor AlCl3 solution (0.05 M).
Słowa kluczowe
Wydawca
Rocznik
Strony
368--374
Opis fizyczny
Bibliogr. 11 poz., rys.
Twórcy
autor
autor
autor
  • National Institute of Rehabilitation, Physical Medicine and Balneoclimatology, Bucharest, Romania
Bibliografia
  • [1] DAVIS K., Material Review: Alumina (Al2O3), School of Doctoral Studies (European Union) Journal, 2010.
  • [2] PICONI C. MACCAURO G., MURATORI F., BRACH DEL PREVER E., J. Appl. Biomater. Biomech., 1(1), (2003),19.
  • [3] GRANADO S., RAGEL V., J. Mater. Chem., 7(8), (1997),1581.
  • [4] LI JI-GUANG, SUN XU-DONG, ZHANG MIN, LI XIAODONG, RU HONG-QIANG, Journal of Inorganic Materials, 6, (1998).
  • [5] DUMINICA F.D., MAURY F., ABISSET S., Thin Solid Films, 515, (2007), 7732.
  • [6] VASILE B.S., VASILE O.R., GHITULICA C.D., ANDRONESCU E., DOBRANIS R., DINU E., TRUSCA R., Phys. Status Solidi (a), 207 (11), (2010), 2499.374 R. ROGOJAN et al.
  • [7] THONGSUWAN W., AUKKARAVITTAYAPUN S., PISITH S., Key Engineering Materials, 353, (2007), 2175.
  • [8] VALLET-REGI M., NICOLOPOULOS S., ROMAN J., MARTINEZ J.L., GONZALES-CALBET J.M., J. Mater. Chem., 7(6), (1997), 1017.
  • [9] ESPARZA-PONCE H.E., REYES-ROJAS A., ANTUNEZFLORES W., MIKI-YOSHIDA M., Materials Science and Engineering, A 343, (2003), 82.
  • [10] DINU E., SIEBERT E., ANDRONESCU E., DJURADO E., DESSEMOND L., GHITULICA C.D., Phys. Status Solidi (a), 205/6, (2008), 1488.
  • [11] International Centre for Diffraction Data (ICDD): aAl2O3 – [83-2080], g-Al2O3 – [48-0367].
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPW7-0025-0023
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