Synthesis and X-ray structural investigation of undoped borate glasses

Padlyak, B. V.; Mudry, S. I.; Kulyk, Y. O.; Drzewiecki, A.; Adamiv, V. T.; Burak, Y. V.; Teslyuk, I. M.

Artykuł - szczegóły

Tytuł artykułu

Synthesis and X-ray structural investigation of undoped borate glasses

Autorzy

Padlyak B. V. , Mudry S. I. , Kulyk Y. O. , Drzewiecki A. , Adamiv V. T. , Burak Y. V. , Teslyuk I. M.

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Języki publikacji

Abstrakty

A series of undoped borate glasses: Li2B4O7, LiKB4O7, LiB3O5, SrB4O7, and LiCaBO3 of high optical quality and chemical purity were obtained from the corresponding polycrystalline compounds using standard glass synthesis under technological conditions developed by the authors. The glasses were obtained by rapid cooling of molten crystalline material, which was heated to 100 K above the melting point to prevent crystallization and to exceed the glass transition point. The X-ray diffraction intensity profiles of the investigated glasses were typical of glassy compounds. The most typical intensity profile, consisting of almost symmetrical peaks, was observed in the case of Li2B4O7 and LiB3O5. Substitution and partial substitution of Li atoms by Sr and Ca atoms was accompanied by significant changes in the intensity profiles of the investigated glasses. Pair correlation functions and structural parameters (average interatomic distances and coordination number to oxygen) of the investigated glasses were evaluated and analyzed. Structural peculiarities of the investigated borate glasses are discussed in comparison with structural data available for their crystalline analogs.

Słowa kluczowe

borate glasses fabrication X-ray diffraction intensity curves pair correlation functions

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2012

Tom

Vol. 30, No. 3

Strony

264--273

Opis fizyczny

Bibliogr. 28 poz.

Twórcy

autor

Padlyak B. V.

autor

Mudry S. I.

autor

Kulyk Y. O.

autor

Drzewiecki A.

autor

Adamiv V. T.

autor

Burak Y. V.

autor

Teslyuk I. M.

Institute of Physical Optics, Dragomanova Str. 23, 79-005 Lviv, Ukraine

Bibliografia

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Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-article-BPW7-0023-0043