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Barium strontium titanate (BST) was prepared via the simple sol-gel method by using tetrabutyl titanate, ethanol, citric acid and ethylene glycol as starting materials. Thermogravimetry and differential thermal analysis were used to examine the behaviour of the xerogel. The particle size of BST was approximately 21 nm, as calculated by the X-ray diffraction and confirmed by transition electron microscopy for the calcination temperature of 750 °C. It was found that the particles of BST powders calcined at 750 °C were smaller and more homogeneous and uniform than those obtained at 800 °C.
Słowa kluczowe
Wydawca
Czasopismo
Rocznik
Tom
Strony
421--426
Opis fizyczny
Bibliogr. 13 poz.
Twórcy
autor
autor
autor
- Ceramic Engineering Department School of Materials Science and Engineering Sharif University of Technology Azadi Street, Tehran Iran
Bibliografia
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- [2] WANG J.Y., YAO X., ZHANG L.Y., Ceram. Int., 30 (2004), 1749.
- [3] JANG H.M., JUN Y.H., Ferroelectrics., 193 (1997), 125.
- [4] MAO C., DONG X., ZENG T., Matter. Lett., 61 (2007), 1633.
- [5] SUASMORO S., PRATAPA S., HARTANTO D., SETYOKO D., DANI U.M., J. Eur. Ceram. Soc., 20 (2000), 309.
- [6] KAO C.F., YANG W.D., Appl. Organometal. Chem., 13 (1999), 383.
- [7] SHIIBASHI H., MATSUDA H., KUWABARA M., J. Sol-Gel Sci. Techn., 16 (1999), 129.
- [8] KOMAROV A.V., PARKIN I.P., ODLYHA M., J. Mater. Sci., 31 (1996), 5033.426 M. GOLMOHAMMAD et al.
- [9] ROEDER R.K., SLAMOVICH E.B., J. Am. Ceram. Soc., 82 (1999), 1665.
- [10] TSAY J.D., FANG T.T., GUBIOTTI T.A., YING J.Y., J. Mater. Sci., 33 (1998), 3721.
- [11] BELLAMY L.J., The Infra-Red Spectra of Complex Molecules, Methuen Co. Ltd., London, 1958.
- [12] DURA N.P., CAPEL F., GUTIERREZ D., TARTAJ J., BANARES M.A., MOURE C., J. Mater. Chem.,11 (2001), 1828.
- [13] TIAN H.Y., QI J.Q., WANG Y., WANG J., CHAN H.L.W., CHOY C.L., Nanotech., 16 (2005), 47.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPW7-0013-0023