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A new series of nitrate transition metal complexes containing diethyl(pyridin-3-ylmethyl)phosphonate (3-pmpe) as a ligand, having a general formula [M(3-pmpe)2(H2O)2](NO3)2 (M = Cu, Co and Ni) and [Zn(3-pmpe)2](NO3)2 were prepared. The complexes were identified and characterized by the elemental analysis, spectroscopic and magnetic studies. Ligands containing two donor atoms, heterocyclic nitrogen and phosphoryl oxygen atoms bind in a bidentate bridging manner via the pyridine nitrogen and the phosphoryl oxygen atoms. The magnetic behaviour in the temperature range 1.8-300 K) of the Cu(II), Ni(II), Co(II) complexes as well as their spectroscopic properties suggest polymeric structure of all complexes and the existence of a weak antiferromagnetic exchange coupling between paramagnetic centres inside the dibridged linear chains [M(3-pmpe)2M]n.
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Tom
Strony
999--1007
Opis fizyczny
Bibliogr. 38 poz.
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autor
autor
autor
- Faculty of Chemistry University of Wroclaw Joliot-Curie 14 50-383 Wrocław, Poland
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPW7-0012-0007