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A chemiresistive sensor was fabricated by the chemical modification of multi-walled carbon nanotubes (MWNTs) and chemical oxidation of polyaniline (PANI). The resistances of the sensing film samples against 100, 250, 500, 1000 ppm explosives (picric acid (PA), 2,6-dinitrotoluene (2,6-DNT) and 2,4,6-trinitrotoluene(TNT)) agents were investigated. The MWNTs with various wt. % PANI agents were characterized by TGA, SEM, FTIR and Raman spectroscopy, respectively. The experimental results showed that 1wt. % MWNTs and 10, 5, 1wt. % PANI sensor samples provided high sensitivity, excellent selectivity and good reproducibility to PA and 2,6-DNT vapours. In addition, principal component analysis (PCA) was applied to distinguish the performance of PA, 2,6-DNT and TNT agents. Our results indicate that the electric detection of explosive agents is possible with simply fabricated MWNTs-PANI devices.
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Tom
Strony
509--520
Opis fizyczny
Bibliogr. 18 poz.
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autor
autor
autor
autor
- Graduate School of Defense Science, Chung Cheng Institute of Technology, National Defense University, Tao-Yuan, Taiwan 335, ROC
Bibliografia
- [1] SENESAC L., THUNDAT T.G., Mater. Today, 11 (2008), 28.
- [2] BYALL E.B., Explosives report 1998–2001detection and characterization of explosives and explosive residue. A review, 13th INTERPOL Forensic Science Symposium, Lyon, France, October 2001, pp. 16–19.
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- [4] PINNADUWAGEA L.A., THUNDATA T., GEHLA A., WILSONA S.D., HEDDENA D.L., LAREAUB R.T., Ultramicr., 100 (2004), 211.
- [5] DOHN S., KJELSTRUP-HANSEN J., MADSEN D.N., MOLHAVE K., BOGGILD P., Ultramicr., 105 (2005), 209.
- [6] TOMCHENKO A.A., HARMER G.P., MARQUIS B.T., Sens. Actuators B., 108 (2005), 41.
- [7] QU F., YANG M., JIANG J., SHEN G.AND YU R., Anal. Biochem., 344 (2005), 108.
- [8] SHIMANO J.Y., MACDIARMID A.G., Synth. Met., 123 (2001), 251.
- [9] DHAWAN S.K., KUMAR D., RAM M.K., CHANDRA S., TRIVEDI D.C., Sens. Actuators B., 40 (1997), 99.
- [10] GOSPODINOVA N., TERLEMEZYAN L., Prog. Polym. Sci., 23 (1998), 1443.
- [11] LEEA D.-S., JUNGA H.-Y., LIMA J.-W., LEEB M., BANB S.-W., HUHC J.-S., LEE D.-D., Sens. Actuators B., 71 (2000), 90.
- [12] BAIBARAC M., BALTOG I., LEFRANT S., MEVELLER J.Y., CHAUVER G., Chem Mater., 15 (2003), 4149.
- [13] FREDERICH J..HARRIS P., Carbon Nanotubes and Related Structures. New Materials for the TwentyFirst Century, Cambridge University Press, Cambridge, 1999.
- [14] MATSUGUCHI M., UMEDA S., SADAOKA Y., SAKAI Y., Sens. Actuators B., 49 (1998), 179.
- [15] BLAU W.J., PANHUIS M., MAITI A., DALTON A.B., VAN DEN NOORT A., COLEMAN J.N., MCCARTHY B., J. Phys. Chem. B., 107 (2003), 478.
- [16] WEI C., Nano Lett., 6 (2006), 1627.
- [17] VALENTINI L., BAVASTRELLO V., STURA E., ARMENTANO I., NICOLINI C., KENNY J.M., Chem. Phys.Lett., 383 (2004), 617.
- [18] CHOI N.-J., KWAK J.-H., LIM Y.-T., BAHN T.-H., YUN K.-Y., KIM J.-CH., HUHD J.-S., LEE D.-D., Sens. Actuators B., 108 (2005), 298.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPW7-0011-0107