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Synthesis and characterization of metastable CeO2-ZrO2 solid solution obtained by polymerized complex method

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The paper describes the preparation and characterization of nano-size metastable tetragonal CeO2–ZrO2 mixed oxides prepared by a polymerized complex method. A glycine–ethylene glycol solution containing Ce3+ and Zr4+ ions was polymerized at 80–110 °C to form a viscous transparent resin without any visible precipitation. After heat-treatment at relatively low temperature (ca 250 °C) on a hot plate in static air, the solid precursor ignited in part due to self-combustion, resulting in the formation of a nanocrystalline, compositionally-homogeneous solid solution. Its structure was confirmed using X-ray diffraction, HRTEM and Raman spectroscopy. The phase separation in CeO2–ZrO2 system on a subsequent heat-treatment in air and in a mixture of H2 and He was also investigated up to 1100 °C.
Wydawca
Rocznik
Strony
153--170
Opis fizyczny
Bibliogr. 65 poz.
Twórcy
autor
  • Institute of Low Temperature and Structure Research, Polish Academy of Sciences, P.O. Box 1410, 50-950 Wrocław 2, Poland
autor
  • Chemistry Department, Cambridge University, Cambridge CB2 1EW, UK
autor
  • Institute of Low Temperature and Structure Research, Polish Academy of Sciences, P.O. Box 1410, 50-950 Wrocław 2, Poland
autor
  • Institute of Low Temperature and Structure Research, Polish Academy of Sciences, P.O. Box 1410, 50-950 Wrocław 2, Poland
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Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPW7-0003-0017
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