Synthesis and characterization of metastable CeO2-ZrO2 solid solution obtained by polymerized complex method

Miśta, W.; Rayment, T.; Hanuza, J.; Macalik, L.

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Tytuł artykułu

Synthesis and characterization of metastable CeO2-ZrO2 solid solution obtained by polymerized complex method

Autorzy

Miśta W. , Rayment T. , Hanuza J. , Macalik L.

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Języki publikacji

Abstrakty

The paper describes the preparation and characterization of nano-size metastable tetragonal CeO2–ZrO2 mixed oxides prepared by a polymerized complex method. A glycine–ethylene glycol solution containing Ce3+ and Zr4+ ions was polymerized at 80–110 °C to form a viscous transparent resin without any visible precipitation. After heat-treatment at relatively low temperature (ca 250 °C) on a hot plate in static air, the solid precursor ignited in part due to self-combustion, resulting in the formation of a nanocrystalline, compositionally-homogeneous solid solution. Its structure was confirmed using X-ray diffraction, HRTEM and Raman spectroscopy. The phase separation in CeO2–ZrO2 system on a subsequent heat-treatment in air and in a mixture of H2 and He was also investigated up to 1100 °C.

Słowa kluczowe

ceria-zirconia polymerized complex method Raman spectroscopy X-ray diffraction

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2004

Tom

Vol. 22, No. 2

Strony

153--170

Opis fizyczny

Bibliogr. 65 poz.

Twórcy

autor

Miśta W.

mista@int.pan.wroc.pl

Institute of Low Temperature and Structure Research, Polish Academy of Sciences, P.O. Box 1410, 50-950 Wrocław 2, Poland

autor

Rayment T.

Chemistry Department, Cambridge University, Cambridge CB2 1EW, UK

autor

Hanuza J.

Institute of Low Temperature and Structure Research, Polish Academy of Sciences, P.O. Box 1410, 50-950 Wrocław 2, Poland

autor

Macalik L.

Institute of Low Temperature and Structure Research, Polish Academy of Sciences, P.O. Box 1410, 50-950 Wrocław 2, Poland

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Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-article-BPW7-0003-0017