Bis(3-methyl-1-propene) ether and 3-(3-methyl-1-propene)-3-methyl-1,2-epoxypropane ether synthesis during the epoxidation of 1-butene-3-ol with hydrogen peroxide over the TS-2 catalyst

• Autorzy: Wróblewska A. , Wójtowicz G.
• Języki publikacji: EN

Abstrakty

EN

The influence of technological parameters on the transformation of 1-butene-3-ol (1B3O) to bis(3-methyl- 1-propene) ether (2x1B3O ether) and 3-(3-methyl-1-propene)-3-methyl-1,2-epoxypropane ether (1B3Ox1,2EB3O ether) over the TS-2 catalyst was presented. The reaction was performed in a glass reactor at atmospheric pressure and in methanol medium (protic solvent). The optimum conditions of 2x1B3O ether and 1B3Ox1,2EB3O ether obtaining were established by the mathematical method of experiments design (rotatable-uniform design) and after the analyses of the layer drawings.

Słowa kluczowe

EN

bis(3-methyl-1-propene) ether; 3-(3-methyl-1-propene)-3-methyl-1,2-epoxypropane ether; TS-2; hydrogen peroxide; epoxidation in liquid phase

PL

bis(3-methyl-1-propen)eter; 3-(3-metylo-1-propen) eter-3-metylo-1 ,2-epoksypropan; TS-2; nadtlenek wodoru; epoksydowanie w fazie ciekłej

• Wydawca: West Pomeranian University of Technology. Publishing House
• Czasopismo: Polish Journal of Chemical Technology
• Rocznik: 2010
• Tom: Vol. 12, nr 3
• Strony: 66--71
• Opis fizyczny: Bibliogr. 19 poz., rys., tab.

Twórcy

autor

Wróblewska A.

autor

Wójtowicz G.

• West Pomeranian University of Technology, Szczecin, Institute of Organic Chemical Technology, ul. Pułaskiego 10, 70-322 Szczecin, Poland,

Bibliografia

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