Synthesis of inorganic oxide composites with the use of postgalvanic waste solutions of copper(II) sulfate

• Autorzy: Modrzejewska-Sikorska A. , Ciesielczyk F. , Jesionowski T.
• Języki publikacji: EN

Abstrakty

EN

The study was undertaken to obtain an oxide composite (inorganic colourful pigment) in the method based on the use of postgalvanic waste solution of copper(II) sulfate. The conditions of the process of precipitation of synthetic CuOźSiO 2 were optimised by checking the effect of the concentration and the volume ratio of the reagents and the temperature on the physico-chemical parameters of the final product. The oxide composite obtained in the optimum conditions was characterised by high refinement of particles and large specific surface area BET of 326 m2/g.

Słowa kluczowe

EN

oxide composite CuO.SiO2; waste solution of copper(II) sulfate; precipitation; particle size distribution; surface area; colorimetric characteristics

PL

powierzchnia; tlenek złożonych CuO.SiO2; rozkład wielkości cząsteczek; powierzchnia właściwa; właściwości kalorymetryczne; opady

• Wydawca: West Pomeranian University of Technology. Publishing House
• Czasopismo: Polish Journal of Chemical Technology
• Rocznik: 2010
• Tom: Vol. 12, nr 2
• Strony: 46--51
• Opis fizyczny: Bibliogr. 11 poz., rys., tab.

Twórcy

autor

Modrzejewska-Sikorska A.

autor

Ciesielczyk F.

autor

Jesionowski T.

• Poznan University of Technology, Institute of Chemical Technology and Engineering, M. Sklodowskiej-Curie 2 Sq., 60-965 Poznan, Poland,

Bibliografia

• 1. Shu, C., Mingxia, X., Cailou, Z. & Jiaqi, T. (2002). Fabrication of cordierite powder for magnesium-aluminum hydroxide and sodium silicate: Its characteristic and sintering, Mater. Res. Bull. 37, 1333 – 1340. DOI:10.1016/S0025-5408(02)00759-6.
• 2. Varghese, S. & Karger-Kocsis, J. (2003). Natural rubber-based nanocomposites by latex compounding with layered silicates, Polymer 44, 4921 – 4927. DOI:10.1016/S0032-3861(03)00480-4.
• 3. Arroyo, M., López-Manchado, M.A. & Herrero, B. (2003). Organo-montmorillonite as substitute of carbon black in natural rubber compounds, Polymer 44, 2447 – 2453. DOI:10.1016/S0032-3861(03)00090-9.
• 4. Hedicke-Höchstötter, K., Lim, G.T., Altstädt, V. (2009). Novel polyamide nanocomposites based on silicate nanotubes of the mineral halloysite, Compos. Sci. Technol. 69, 330 – 334. DOI:10.1016/j.compscitech.2008.10.011.
• 5. Jo, B., Park, S. & Kim, D. (2008). Mechanical properties of nano-MMT reinforced polymer composite and polymer concrete, Constr. Build. Mater. 22, 14 – 20. DOI:10.1016/j.conbuildmat.2007.02.009.
• 6. Wieczorek, M., Krysztafkiewicz, A. & Jesionowski, T. (2004). Influence of modification by N-2-(aminoethyl)-3-aminopropyltrimethoxysilane on physicochemical properties of bentonite, J. Phys. Chem. Solids 65, 447 – 452. DOI:10.1016/j.jpcs.2003.09.016.
• 7. Krysztafkiewicz, A., Michalska, I. & Jesionowski, T. (2001). Zinc, chromium and iron silicates as fillers and inorganic colour pigments, Compos. Interfaces 8, 257 – 262. DOI: 10.1163/15685540152594730.
• 8. Zanetti, M. & Costa, L. (2004). Preparation and combustion behaviour of polymer/layered silicate nanocomposites based upon PE and EVA, Polymer 45, 4367 – 4373. DOI:10.1016/j.polymer.2004.04.043.
• 9. Upadhyay, R.D. & Kale, D.D. (2001). Properties of polypropylene filled with synthetic sodium aluminum silicate, J. Appl. Polym. Sci. 81, 2297 – 2303. DOI: 10.1002/app.1670.
• 10. Ozyilmaz, G., Tukel, S.S. & Alptekin, O. (2005). Activity and storage stability of immobilized glucose oxidase onto magnesium silicate, J. Mol. Cat. B 35, 154 – 160. DOI:10.1016/j.molcatb.2005.07.001.
• 11. Buczydło, E. (1972). Pickling and galvanizing plants waste utilization (in Polish), Wydanie 1, Wydawnictwo Śląsk, Katowice.