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Nowe azometiny i poliazometiny o budowie liniowej, gwiaździstej i dendrytowej: synteza, przejścia fazowe i wybrane właściwości optoelektryczne

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EN
New azomethines and polyazomethines with linear, star-shaped and dendrimer structure: synthesis, phase transitions and selected optoelectrical properties
Języki publikacji
PL
Abstrakty
PL
Celem naukowym przedstawionej dysertacji było poszerzenie wiedzy o termotropowych związkach organicznych zawierających wiązania iminowe oraz zbadanie możliwości ich zastosowań w optoelektronice. W ramach pracy przebadano 93 związki organiczne zarówno o budowie liniowej (związki małocząsteczkowe i polimery) jak i związki rozgałęzione oraz dendrymery. W pracy przedstawiono azometiny symetryczne i niesymetryczne typu pręta sztywnego oraz azometiny typu bananowego. Polimery zawierały grupy azometinowe w łańcuchu głównym. Dendrymery z wiązaniami iminowymi badano biorąc pod uwagę zarówno generację, rodzaj rdzenia i grup końcowych. W celu porównania wybranych właściwości fizykochemicznych w tym ciekłokrystalicznych azometin i poliazometin, otrzymano diimidy, poliimidy, azyny i bistiazole zawierające te same ugrupowania chemiczne, co azometiny i poliazometiny. Właściwości ciekłokrystaliczne otrzymanych związków zostały zbadane poprzez zastosowanie skaningowej kalorymetrii różnicowej (DSC) i polaryzacyjnego mikroskopu optycznego (POM). Dodatkowo właściwości ciekłokrystaliczne wybranych związków zostały potwierdzone za pomocą spektroskopii absorpcyjnej w zakresie UV-vis i podczerwieni (IR) i metody dyfrakcji promieniowania rentgenowskiego (WAXS/SAXS). Wykonano także wstępne badania spektroskopii impedancyjnej oraz wykreślono krzywe Nyquist'a. Dla wybranych związków wykonano badania absorpcji w zakresie UV-vis oraz badania fotoluminescencyjne. Na podstawie przeprowadzonych badań ustalono wpływ budowy i rodzaju otrzymanych związków na ich właściwości ciekłokrystaliczne i optoelektryczne. W pracy pokazano przykłady potencjalnego wykorzystania otrzymanych związków w fotowoltaice, jako warstwy aktywnej ogniw słonecznych oraz jako związki wykazujące właściwości termoluminescencyjne.
EN
In this work, 93 liquid crystalline [LC] imines and polyazomethines having different shapes [linear, star, dendrimers] and symmetries (symmetrical and asymmetrical) were investigated as liquid crystalline materials for potential optoelectronic and photovoltaic applications. The geometrical analyses included rod, bent and disc-shaped azomethines. Thermotropic polyazomethines having an imine band in the main chain were characterized. Among star-shaped compounds, thiophosphoryl and cyclotriphosphasene dendrimers with different generations ranging from 0 to 5 were investigated as liquid crystalline materials. Additionally, diimides, bisthiazolothiazoles, azines and polyimides were synthesized and their performances as liquid crystalline materials were compared with those of azomethines and polyazomethines. The thermotropic liquid crystalline behavior of different compounds was examined by the differential scanning calorimetry (DSC) and polarizing optical microscopy (POM). LC properties of selected compounds were detected by X-ray diffraction (WAXS/SAXS). Optical properties of obtained compounds, including UV-vis absorption and photoluminescence (PL), were studied in solution. UV-vis properties of selected compounds in the form of thin films were investigated on a quartz substrate. Some compounds were irradiated with a test dose of 1 or 2 Gy Co-60 gamma-rays to detect their thermoluminescence properties in the temperature range 25-200°C. In order to assess electrical performance, these materials were characterized by impedance spectroscopy at different temperatures. Additionally, the films were characterized by AFM technique and roughness (Ra, RMS) along with skew and kurtosis. Finally, the photovoltaic properties of bulk heterojunction (BHJ) and monolayer devices were investigated in the dark and during irradiation with xenon lamp under STC conditions (AM1,5G, 1000 W/m2 at room temperature 25°C).
Rocznik
Tom
Strony
1--157
Opis fizyczny
Bibliogr. 332 poz., rys., tab.
Twórcy
autor
  • Instytut Elektrotechniki, Oddział Technologii i Materiałoznawstwa Elektrotechnicznego we Wrocławiu
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