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The method of obtaining hydroxyapatite by thermal treatment of deproteinised and defatted bone pulp called bone sludge was presented. The products of the calcining process were characterized with X-ray diffraction (XRD) and Fourier transformed infrared spectroscopy (FT-IR). The calcium content was determined with titration, whereas the contents of total phosphorus - with a spectrophotomertric method. X-ray investigations confirmed that hydroxyapatite was the main component of the calcining products in the calcining process. The FT-IR spectra confirmed that all organic substances were removed during the calcining process. On the basis of the research into physiological liquids the propensity to resorption of hydroxyapatite bioceramic was evaluated.
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37--43
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Bibliogr. 8 poz., rys.
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- Institute of Inorganic Chemistry and Technology, Cracow University of Technology, ul. Warszawska 24, 31-155 Kraków, asobczak@chemia.pk.edu.pl
Bibliografia
- 1. Święcicki, Z. (1992). Bioceramics for orthopedics Instytut Podstawowych Problemów Techniki PAN, Wyd. Spółdzielcze Sp. z.o.o., Warszwa (in Polish).
- 2. Knychalska-Karwan, Z. & Ślósarczyk, A. (1994). Hydroxyapatite in stomatology Krakmedia, Kraków (in Polish).
- 3. Ślósarczyk, A. (1997). Hydroxyapatite bioceramics Biuletyn Ceramiczny nr 13 Ceramika 51, Polskie Towarzystwo Ceramiczne, Kraków (in Polish).
- 4. Shin, H., Jo, S. & Mikos, A.G. (2003). Biomimetic materials for tissue engineering. Biomaterials 24, 4353 - 4364.
- 5. Vallet-Regi, M. & Gonzales-Calbert J. (2004). Calcium phosphates as substitution of bone tissues. Prog. Solid St. Chem. 32, 1 - 31. Received 1 December 2003; received in revised form 1 June 2004; accepted 15 July 2004, from Science Direct database on the World Wide Web: www.elsevier.nl/locate/pssc. DOI:10.1016/j.progsolidstchem.2004.07.001. www.elsevier.nl/locate/pssc
- 6. Alpert, N.L., Kaiser, W.E. & Szymański H.A. (1973). Infrared spectroscopy - theory & practice PWN Warszawa (in Polish).
- 7. Rapacz-Kmita, A., Paluszkiewicz, C., Ślósarczyk, A. & Paszkiewicz Z. (2005). FTIR and XRD investigations on the thermal stability of hydroxyapatite during hot pressing and pressure less sintering processes, J. Mol. Struc. 744 - 747, 653 - 656. Received 10 November 2004; accepted 30 November 2004 Available online 11 January 2005, from Science Direct database on the World Wide Web: www.elsevier.com/locate/molstruc. DOI:10.1016/j.molstruc.2004.11.070. www.elsevier.com/locate/molstruc
- 8. Ślósarczyk, A., Paszkiewicz, Z. & Paluszkiewicz C. (2005). FTIR and XRD evaluation of carbonated hydroxyapatite powders synthesized by wet methods, J. Mol. Struc 744 - 747, 657 - 661. Received 10 November 2004; accepted 30 November 2004 Available online 11 January 2005, from Science Direct database on the World Wide Web: www.elsevier.com/locate/molstruc. DOI: 10.1016/j.molstruc.2004.11.078. www.elsevier.com/locate/molstruc
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Bibliografia
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bwmeta1.element.baztech-article-BPS2-0050-0067