Uncommon applications of statistical methods of the design of experiments in chemical technology and environment protection

• Autorzy: Lewandowski G. , Ćwirko J.
• Języki publikacji: EN

Abstrakty

EN

The review of literature related to the applications of statistic methods of design of experiments in chemical technology and environment protection was presented in the work. The research that consists of two stages: a stage of choosing the best variables describing an experimental object and a stage of proper experimental investigation, seems particularly interesting. An interesting example of an application of statistical strategies in environmental protection is the optimization of photoactivity of TiO2/SiO2 mixture, received by a sol-gel technique. TiO2, due to its specific feature, was applied in the photocatalytic methods of removing toxic compounds from water and air. In the experiments there were used two designs - the fractional factorial design 2^5-1 (as the elimination one) and the central composite design (as the proper one). Following the data analysis from the elimination plan two variables were eliminated, which helped to simplify the research object. Among other uncommon applications of the design of experiments: the optimization of the conditions for the extraction of natural pigments used in dyeing food, the production of fatty acid methyl esters used as diesel oil substitutes (biodiesel) and the optimization of a supercritical fluid extraction methodology for the analysis of castor oil, should be mentioned.

Słowa kluczowe

EN

design of experiments; optimization; central composite designs; dyes; esterification; TiO2 photoactivity; biodiesel

PL

planowanie doświadczeń; optymalizacja; plany kompozycyjne centralne; barwniki; estryfikacja; fotoaktywność TiO2

• Wydawca: West Pomeranian University of Technology. Publishing House
• Czasopismo: Polish Journal of Chemical Technology
• Rocznik: 2007
• Tom: Vol. 9, nr 4
• Strony: 63--67
• Opis fizyczny: Bibliogr. 9 poz., rys., tab.

Twórcy

autor

Lewandowski G.

autor

Ćwirko J.

• Institute of Organic Chemical Technology, Szczecin University of Technology, ul. Pułaskiego 10, 70-322 Szczecin,

Bibliografia

• 1. Hendershot R. J., Rogers W. B., Snively Ch. M., Ogunnaike B. A., Lauterbach J.: Catal. Today, 2004, 98, 375 - 385.
• 2. He Y, Bao Y. D.: Renewable Energy, 2005, 30, 805 - 813.
• 3. van Ginkel S., Sung S., Lay J. -J.: Environ. Sci. Technol., 2001, 35, 4726 - 4730.
• 4. Cole D. C., Pagano N., Kelly M. F., Ellingboe J.: J. Comb. Chem., 2004, 6, 78 - 82.
• 5. Gooding O. W., Vo L., Bhattacharyya S., Labadie J.: J. Comb. Chem., 2002, 4, 576 - 583.
• 6. Lung-Chuan Chen, Chao-Ming Huang: Application of statistical strategies to process optimization of sol-gel derived SiO2 modification of TiO2, Ind. Eng. Chem. Res., 2004, 43, 6446 - 6452.
• 7. Gonzales M., Mendes J., Carnero A., Lobo M. G., Afonso A.: Optimizing conditions for the extraction of pigments in cochineals (Dactylopius coccus Costa) using response surface methodology, J. Agric. Food Chem., 2002, 50, 6968 - 6974.
• 8. Turner Ch., Whitehand L. C., Nguyen T., McKeon T.: Optimization of a supercritical fluid extraction/reaction methodology for the analysis of castor oil using experimental design, J. Agric. Food Chem., 2004, 52, 26 - 32.
• 9. Vicente G., Coteron A., Martinez M., Aracil J.: Application of the factorial design of experiments and response surface methodology to optimize biodiesel production, Ind. Crops and Products, 1988, 8, 29 - 35.