Epoxidation of methallyl alcohol over Ti-Beta catalyst

• Autorzy: Wróblewska A. , Milchert E.
• Języki publikacji: EN

Abstrakty

EN

The epoxidation of methallyl alcohol (MAA) to 2-methylglycidol was carried out with 30 wt% hydrogen peroxide in an autoclave. The titanium silicalite catalyst Ti-Beta was used as a catalyst and methanol as a solvent. The effect of temperature (20- 120°C), the molar ratio MAA/H2O2 (1:1 - 5:1), methanol concentration (5 - 80 wt%), Ti-Beta concentration (0.1 - 2.0 wt%) and reaction time (0.5 - 5.0h) were studied. The optimum parameters were: temperature 100"C, the molar ratio MAA/H2O2 = 1:1, methanol concentration 5 wt%, Ti-Beta concentration 0.1 wt% and reaction time 0.5h.

Słowa kluczowe

EN

Ti-Beta; epoxidation; 2-methylglycidol

PL

Ti-Beta; epoksydacja; 2-metyloglicydol

• Wydawca: West Pomeranian University of Technology. Publishing House
• Czasopismo: Polish Journal of Chemical Technology
• Rocznik: 2006
• Tom: Vol. 8, nr 2
• Strony: 73--75
• Opis fizyczny: Bibliogr. 6 poz., rys., tab.

Twórcy

autor

Wróblewska A.

autor

Milchert E.

• Institute of Organic Chemical Technology, Szczecin University of Technology, ul. Pułaskiego 10, 70-322 Szczecin,

Bibliografia

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