Sonoelectroanalysis : a review

Banks, C. E.; Compton, R. G.

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Artykuł - szczegóły

Tytuł artykułu

Sonoelectroanalysis : a review

Autorzy

Banks C. E. , Compton R. G.

Wybrane pełne teksty z tego czasopisma

http://beta.chem.uw.edu.pl/chemanal/

Identyfikatory

Warianty tytułu

Elektroanaliza ultradźwiękowa : przegląd

Języki publikacji

Abstrakty

This review highlights recent advances made towards improving sonoelectroanalysis with an emphasis on applications where conventional electrochemical methodologies often fail. It is shown that: 1) the significantly increased mass transport regime under insonation very considerably enhances the sensitivity in comparison to what would be obtained under quiescent conditions and, in particular, 2) cavitational activity at the electrode solution interface provides depassivation in highly 'dirty' media or in the presence of undesirable surface active species and so can preserve quantitative electrode activity in complex, real world samples so removing the requirements for sample pretreatment which has hitherto limited the wider applications, for example, of stripping voltammetry.

W pracy przedstawiono ostatnie osiągnięcia w elektroanalizie z użyciem ultradźwięków. Szczególny nacisk położono na te zastosowania, w których tradycyjne postępowanie nie przynosi skutku. Pokazano, że: 1) napromieniowanie ultradźwiękami znacznie zwiększa szybkość transportu i czułość oznaczeń w porównaniu do spokojnych roztworów, i, w szczególności, 2) pojawiające się turbulencje dopasywują elektrody w bardzo „zabrudzonych" środowiskach i w obecności niechcianych związków powierzchniowych, a tym samym przedłużają aktywność elektrod w złożonych rzeczywistych próbkach. Można wówczas zrezygnować ze wstępnego kondycjonowania elektrod i rozszerzyć pole zastosowań, np. w analizie stripingowej.

Słowa kluczowe

sonoelectroanalysis ultrasounds electrochemistry

elektroanaliza ultradźwiękowa ultradźwięki elektrochemia

Wydawca

Komitet Chemii Analitycznej PAN

Czasopismo

Chemia Analityczna

Rocznik

2003

Tom

Vol. 48, No. 2

Strony

159--180

Opis fizyczny

Bibliogr. 105 poz.

Twórcy

autor

Banks C. E.

Physical and Theoretical Chemistry Laboratory, University of Oxford, South Parks Road, Oxford, OXI 3QZ, United Kingdom

autor

Compton R. G.

Richard.Compton@chemistry.ox.ac.uk

Physical and Theoretical Chemistry Laboratory, University of Oxford, South Parks Road, Oxford, OXI 3QZ, United Kingdom

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