New method of 2,4,6-trichloroaniline synthesis

• Autorzy: Gaca J. , Kędzierska M.

Warianty tytułu

PL

Nowa metoda otrzymywania 2,4,6-trichloroaniliny

• Języki publikacji: EN

Abstrakty

EN

The possibility of application of the system: peroxide chloride ion for the preparation of 2,4,6-trichloroaniline from sulfanilic acid has been demonstrated. The effect of various factors on the degree of sulfanilic acid conversion and on the 2,4,6-trichloroaniline yield has been studied.

Słowa kluczowe

EN

trichloroaniline; sulfanilic acid

PL

trichloroanilina; kwas sulfanilowy

• Wydawca: Centrum Materiałów Polimerowych i Węglowych PAN
• Czasopismo: Polish Journal of Applied Chemistry
• Rocznik: 2001
• Tom: Vol. 45, nr 3-4
• Strony: 85--89
• Opis fizyczny: Bibliogr. 10 poz., tabl. 2, rys.2

Twórcy

autor

Gaca J.

• Department of Chemistry and Chemical Engineering, University of Technology and Agriculture, Seminaryjna 3, 85-326 Bydgoszcz, Poland

autor

Kędzierska M.

• Department of Chemistry and Chemical Engineering, University of Technology and Agriculture, Seminaryjna 3, 85-326 Bydgoszcz, Poland

Bibliografia

• [1] J. GACA and S. ŻAK, Synth Commun., 27, 3291 (1997).
• [2] J. GACA and S. ŻAK, Pol. J. Appl. Chem., 3, 179 (1997).
• [3] J. GACA, M. K.ĘDZIERSKA and S. ŻAK, Congress PTCh i SITPCh, Poznań, S-5, D-54, (1996).
• [4] J. GACA and M. KĘDZIERSKA, Congress PTCh i SITPCh, Rzeszów, R-14, (1999).
• [5] H.CERFONTAIN, Mechanistic aspects in aromatic sulfonation and desulfonation, Wiley, Amsterdam 1968.
• [6] R.T. DATTA and J.C. BHOUMIK, J. Am. Chem. Soc., 43, 303 (1921).
• [7] G. OTTMANN and H. HOOKS,. J.Org. Chem., 30, 952 (1965).
• [8] Cal Y. MEYERS, J. Org. Chem., 26, 1046 (1961).
• [9] P. ŚVEC, Collection Czechoslov. Commun., 50, 1842,(1985).
• [10] B.R. EGGINS and P.K. ROBERTSON, J. Chem. Soc. Faraday Trans., 90 (15), 2249 (1994).