Neutron activation analysis and its contribution to inorganic trace analysis

Dybczyński, R.

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Tytuł artykułu

Neutron activation analysis and its contribution to inorganic trace analysis

Autorzy

Dybczyński R.

Wybrane pełne teksty z tego czasopisma

http://beta.chem.uw.edu.pl/chemanal/

Identyfikatory

Warianty tytułu

Neutronowa analiza aktywacyjna i jej wkład w nieorganiczną analizę śladową

Konferencja

Polish Conference on Analytical Chemistry / sympozjum (VI; 9-14 July, 2000; Gliwice, Poland)

Języki publikacji

Abstrakty

Theoretical principles of neutron activation analysis (NAA) are briefly described and the general schemes of instrumental (INAA) and radiochemical (RNAA) variants of the method are given. The unique merits of NAA which assure its high position among other methods of inorganic trace analysis are emphasized. Comparisons of NAA with some spectroscopic and other methods are presented. A short review of applications of NAA in various domains of science and technology is given and less common applications as molecular AA and derivative AA are mentioned. Unique properties of NAA i.e. practical absence of blank, the fact that this is a method based on nuclear properties of individual isotopes of an element and good accuracy at low concentration levels, are the reason why NAA is often used for verification of accuracy of other analytical methods and certification of the candidate reference materials. The decisive role of NAA in the certification of the candidate reference materials is emphasized.

Przedstawiono pokrótce teoretyczne podstawy neutronowej analizy aktywacyjnej (N AA) oraz zaprezentowano ogólny schemat N AA zarówno w wersji czysto instrumentalnej (INAA) jaki i radiochemicznej (RNAA). Podkreślono unikatowe zalety NAA, dzięki którym zajmuje ona wysoką pozycje, wśród innych metod nieorganicznej analizy śladowej. Porównano NAA z metodami spektroskopowymi i innymi. Dokonano krótkiego przeglądu zastosowań NAA w różnych dziedzinach nauki i techniki wspominając także mniej typowe zastosowania metody jak: molekularna AA i pochodna AA. Unikatowe własności NAA tj. praktyczny brak ślepej próby, fakt, że jest to metoda oparta na własnościach jądrowych poszczególnych izotopów danego pierwiastka, oraz dobra dokładność na niskim poziomie stężeń powodują, że NAA jest często używana do sprawdzania dokładności innych metod analitycznych i atestacji (certyfikacji) materiałów - kandydatów na materiały odniesienia. Podkreślono wyjątkowo ważną rolę NAA w procesie certyfikacji materiałów odniesienia.

Słowa kluczowe

neutron activation analysis trace analysis reference materials

analiza neutronowa aktywacyjna analiza śladowa odnośnik

Wydawca

Komitet Chemii Analitycznej PAN

Czasopismo

Chemia Analityczna

Rocznik

2001

Tom

Vol. 46, No. 2

Strony

133--160

Opis fizyczny

Bibliogr. 116 poz.

Twórcy

autor

Dybczyński R.

Department of Analytical Chemistry, Institute of Nuclear Chemistry and Technology, 16 Dorodna Str., 03195 Warsaw, Poland

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