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Warianty tytułu
Neutronowa analiza aktywacyjna i jej wkład w nieorganiczną analizę śladową
Konferencja
Polish Conference on Analytical Chemistry / sympozjum (VI; 9-14 July, 2000; Gliwice, Poland)
Języki publikacji
Abstrakty
Theoretical principles of neutron activation analysis (NAA) are briefly described and the general schemes of instrumental (INAA) and radiochemical (RNAA) variants of the method are given. The unique merits of NAA which assure its high position among other methods of inorganic trace analysis are emphasized. Comparisons of NAA with some spectroscopic and other methods are presented. A short review of applications of NAA in various domains of science and technology is given and less common applications as molecular AA and derivative AA are mentioned. Unique properties of NAA i.e. practical absence of blank, the fact that this is a method based on nuclear properties of individual isotopes of an element and good accuracy at low concentration levels, are the reason why NAA is often used for verification of accuracy of other analytical methods and certification of the candidate reference materials. The decisive role of NAA in the certification of the candidate reference materials is emphasized.
Przedstawiono pokrótce teoretyczne podstawy neutronowej analizy aktywacyjnej (N AA) oraz zaprezentowano ogólny schemat N AA zarówno w wersji czysto instrumentalnej (INAA) jaki i radiochemicznej (RNAA). Podkreślono unikatowe zalety NAA, dzięki którym zajmuje ona wysoką pozycje, wśród innych metod nieorganicznej analizy śladowej. Porównano NAA z metodami spektroskopowymi i innymi. Dokonano krótkiego przeglądu zastosowań NAA w różnych dziedzinach nauki i techniki wspominając także mniej typowe zastosowania metody jak: molekularna AA i pochodna AA. Unikatowe własności NAA tj. praktyczny brak ślepej próby, fakt, że jest to metoda oparta na własnościach jądrowych poszczególnych izotopów danego pierwiastka, oraz dobra dokładność na niskim poziomie stężeń powodują, że NAA jest często używana do sprawdzania dokładności innych metod analitycznych i atestacji (certyfikacji) materiałów - kandydatów na materiały odniesienia. Podkreślono wyjątkowo ważną rolę NAA w procesie certyfikacji materiałów odniesienia.
Wydawca
Czasopismo
Rocznik
Tom
Strony
133--160
Opis fizyczny
Bibliogr. 116 poz.
Twórcy
autor
- Department of Analytical Chemistry, Institute of Nuclear Chemistry and Technology, 16 Dorodna Str., 03195 Warsaw, Poland
Bibliografia
- 1. Vandecasteele C., Activation Analysis with Charged Particles, E.Horwood Ltd., Chichester, 1988.
- 2. Segebade C., Weise H.P. and Lutz G.J., Photon Activation Analysis, W. de Gruyter, Berlin, 1988.
- 3. Dybczyński R., Chem. Anal. (Warsaw), 30, 749 (1985).
- 4. Guinn V.P. and Hoste J., Neutron Activation Analysis in: Elemental Analysis of Biological Materials, Technical Reports Series No. 197, IAEA, Vienna, 1980, pp. 105-140.
- 5. Heydorn K., Neutron Activation Analysis for Clinical Trace Element Research, Vol I and II, CRC Press, Boca Raton, 1984.
- 6. Parry S.J., Activation Spectrometry in Chemical Analysis, Wiley, New York (1991).
- 7. Girardi F., Guzzi G. and Pauly J., Anal. Chem., 37, 1085 (1965).
- 8. De Corte F., Simonits A., De Wispelaere A. and Hoste J., J. Radioanal. Nucl. Chem., 113, 145 (1987).
- 9. Moens L., De Corte F., De Wispelaere A., Hoste J., Simonits A., Elek. and Szabo E., J. Radioanal. Nucl. Chem., 82, 385 (1984).
- 10. Dybczyński R., Wasek M. and Maleszewska H., J. Radioanal. Nucl. Chem. (Articles), 130, 365 (1989).
- 11. Dybczyński R. and Danko B., J. Radioanal. Nucl. Chem., 181, 43 (1994).
- 12. Dybczyński R., J. Chromatogr., 600, 17 (1992).
- 13. Dams R., Robbins J.A., Rahn K.A. and Winchester J.W., Anal. Chem., 42, 861 (1970).
- 14. Steiness E., in: Activation Analysis in Geochemistry and Cosmochemistry, [Brunfelt A.O., Steiness E., Eds], Universitetsforlaget, Oslo 1971, pp. 113-128.
- 15. Glascock M.D., Nuclear reaction chemical analysis: prompt and delayed measurements, in: Chemical Analysis by Nuclear Methods, [Z.B. Alfassi, Ed.], Wiley, New York 1994.
- 16. Bem H., Lowering of detection limit of selected elenments in neutron activation analysis (in Polish), Zeszyty Naukowe Politechniki Łódzkiej, Nr 524, Rozprawy Naukowe, z. 99, 1986, Wydawnictwo Politechniki Łódzkiej, Łódź 1987, (in Polish).
- 17. Dybczyński R., et.al., Geological Quartely, (in print).
- 18. Dybczyński R., et.al. Chem. Anal. (Warsaw), (in print).
- 19. Iraj Najafi S., Computerized analysis of gamma-ray spectra, in: Activation analysis, Vol I, [Z.B. Alfassi, Ed.], CRC Press, Boca Raton 1990.
- 20. Burgess D.D., Optimization of Instrumental Activation Analysis, in: Activation analysis, Vol. I, [Z.B. Alfassi, Ed.], CRC Press, Boca Raton 1990.
- 21. Grass F., Bichler M., Dorner J., Holzner H., Ritschel A., Ramadan A., Westphal G.P. and Gwozdz R., in: Nuclear Analytical Methods in the Life Sciences 1994, [J. Kucera, I. Obrusnik, E. Sabbioni, Eds.], Humana Press, Totowa, New Jersey 1994, pp. 33-46.
- 22. Minczewski J., Chwastowska J. and Dybczyński R., Separation and Preconcentration Methods in Inorganic Trace Analysis. Horwood, Chichester 1982.
- 23. Fardy J.J., Radiochemical Separations in Activation Analysis, in: Activation analysis, Vol I, [Z.B. Alfassi, Ed.], CRC Press, Boca Raton 1990, pp. 61-96.
- 24. Alfassi Z.B., Radiochemical neutron activation analysis, in: Determination of Trace Elements, [Z.B. Alfassi, Ed.], VCH Verlagsgesellschaft, Weinheim 1994, pp. 309-357.
- 25. Egorov E.V. and Makarova S.B., Ionnyi Obmien w Radiokhimii, Atomizdat, Moskva 1971 (in Russian).
- 26. Fołdzińska A. and Dybczyński R., J. Radioanal. Chem., 21, 507 (1974).
- 27. Kucera J., De Goeij J.J.M., J. Radioanal. Chem., 63,.23 (1981).
- 28. Dybczyński R. and Danko B., Biological Trace Element Research, 43/45, 615 (1994).
- 29. Dybczyński R. and Samczyński Z., J. Radioanal. Nucl. Chem. (Articles), 150, 143 (1991).
- 30. Danko B. and Dybczyński R., J. Radioanal. Nucl. Chem., 216, 51 (1997).
- 31. Samczyński Z. and Dybczyński R., Chem. Anal. (Warsaw), 41, 873 (1996).
- 32. Dybczyński R., Zh. Anal. Khim., 51,1328 (1996); J. Anal. Chem., (Moscow), 51, 1206 (1996).
- 33. Dybczyński R., Proc. Intern. Symposium on Harmonization of Health Related Environmental Measurements Using Nuclear and Isotopic Techniques, (IAEA-SM-344/16), Hyderabad, India 4-7 Nov., 1996, pp. 199-211.
- 34. Lyon W.S., J. Radioanal. Nucl. Chem. (Articles), 140, 205 (1990).
- 35. Braun T. and Zsindely S., Trends in AnaI. Chem., 9, 144 (1990).
- 36. Byrne A.R., Fresenius J. Anal. Chem., 345, 144 (1993).
- 37. Bode P., Overwater R.M.W. and De Goeij J.J.M., J. Radioanal. Nucl. Chem., 216, 5 (1997).
- 38. Matusiewicz H., Electrothermal vaporization sample introduction into plasma sources for analytical emission spectrometry, in: Advances in Atomic Spectroscopy, Vol. 2, JAI Press Inc., 1995, pp. 63-138.
- 39. Krivan V., Angewandte Chemie, Int. Ed., 18, 123 (1979).
- 40. Moens L. and Dams R., J. Radioanal. Nucl. Chem. (Articles), 192, 29 (1995).
- 41. Elemental Analysis of Biological Materials, Technical Reports Series No. 197, IAEA, Vienna 1980.
- 42. Parr R.M., Report No. 2, Intercomparison of Minor and Trace Elements in IAEA Animal Muscle [H-4], IAEA/RI/91, IAEA, Vienna, October 1980.
- 43. Dybczyński R., Relative accuracy, precision and frequency of use of neutron activation analysis and other techniques as revealed by the results of some recent IAEA intercomparisons, in: Quality Assurance in Biomedical Neutron Activation Analysis, IAEA-TECDOC-323, IAEA, Vienna, 1984, pp. 39-51.
- 44. Dybczyński R., Fresenius J. Anal. Chem., 352, 120 (1995).
- 45. Dybczyński R., J. Radioanal. Chem., 60, 45 (1980).
- 46. Pszonicki L., Veglia A., Dybczyński R. and Suschny 0., Report on Intercomparison V-8 of the Determination of Trace Elements in Rye Flour, IAEA/RL/91, Vienna, January, 1982.
- 47. Greenberg R.R., Proc. Intern. Symposium on Harmonization of Health Related Environmental Measurements Using Nuclear and Isotopic Techniques, (IAEA-SM-344/18), Hyderabad, India 4-7 Nov. 1996, pp. 137-144.
- 48. Greenberg R.R., J. Radioanal. Nucl. Chem. (Articles), 113, 233 (1987).
- 49. Thompson D., Parry S.J., Benzing R., Williams J.G. and Jarvis K.E., J. Radioanal. Nucl. Chem., 233, 63 (1998).
- 50. Becker D.A., Fresenius J. Anal. Chem., 345, 298 (1993).
- 51. Karpov Yu.J. and Alimarin I.P., Zh. Anal. Khim., 34, 1402 (1979).
- 52. Hoste J., J. Radioanal. Chem., 19, 7 (1974).
- 53. May S., Piccot D. and Pinte G., J. Radioanal. Chem., 17, 153 (1973).
- 54. Niese S., J. Radioanal. Chem., 38, 37 (1977).
- 55. Zaidi J.H., Waheed S. and Ahmed S., J. Radioanal. Nucl. Chem., 242, 259 (1999).
- 56. Zaidi J.H., Arif M., Fatima I., Ahmed S. and Qureshi I.H., J. Radioanal. Nucl. Chem., 241, 123 (1999).
- 57. Ordogh M., Szabo E. and Hegedus O., Radiochemical Methods of Analysis, Vol. I, IAEA, Vienna, 1965, p. 175.
- 58. Verheike M., Instrumental Neutron Activation Analysis Developed for Silicon Integrated Circuit Technology, Ph.D. Thesis, Eindhoven University of Technology, 1992.
- 59. Tomura K. and Tomuro H., J. Radioanal. Nucl. Chem., 242, 147 (1999).
- 60. McGuire S.C., Hossain T.Z., Golkowski., Kemess N.D. and Sulcer J.D., J. Radioanal. Nucl. Chem. (Articles), 192, 65 (1995).
- 61. Maleszewska H. and Dybczyński R., J. Radioanal. Chem., 31, 177 (1976).
- 62. Hoffman E.L. and Ernst P.C., J. Radioanal. Chem., 71, 447 (1982).
- 63. Meloni S., Odone M., Cecchi A. and Poli G., J. Radioanal. Chem., 71, 429 (1982).
- 64. Yui M., Kikawada Y., Oi T., Honda T. and Nozaki T., J. Radioanal. Nucl. Chem., 238, 3 (1998).
- 65. Morrison G.H., Gerard J.T., Travesi A., Currie R.L., Peterson S.F. and Potter N.M., Anal. Chem., 41, 1633 (1969).
- 66. Joron J.L., Treuil M. and Raimbault L., J. Radioanal. Nucl. Chem., 216, 229 (1997).
- 67. Fong B.B. and Chatt A., J. Radioanal. Nucl. Chem., 110, 135 (1987).
- 68. Miller G.E., J. Radioanal. Nucl. Chem., 114, 351 (1987).
- 69. Sun J.X. and Jervis R.E., J. Radioanal. Nucl. Chem., 89, 553 (1985).
- 70. Laul J.C., Atomic Energy Rev., 17, 603 (1979).
- 71. Cohen D.R., Hoffman E.L. and Nichol I., J. Geochem. Explor., 29, 49 (1987).
- 72. Lipschutz M.E., Wolf S.F., Vogt S., Michlovich E., Lindstrom M.M., Zolensky M.M., Mittlefehldt D.W., Satterwhite C., Schultz L., Loeken T., Scherer P., Dodd R.T., Sears D.G.W., Benoit P.H., Wacker J.F., Burns R.G. and Fissher D.S., Meteoritics, 28, 528 (1993).
- 73. Zipfel J., Palme H., Kennedy A.K., Hutcheon I.D., Geochim. Cosmochim. Acta, 59, 3607 (1995).
- 74. Xiao X. and Lipschutz M.E., Geochim. Cosmochim. Acta, 55, 3407 (1991).
- 75. Warren P.H. and Kallemeyn G.W., Meteoritics & Planetary Science, 31, 97(1996).
- 76. Landstrom O., Samsahl K. and Wenner C.G., 1968 Int. Conf. on Modern Trends in Activation Analysis, NBS Special Publication 312, Vol. I, Washington 1969, p. 353.
- 77. Hogdahl O., in: Activation Analysis in Geochemistry and Cosmochemistry, [A.O. Brunfelt, E. Steiness, Eds.], Universitetsforlaget, Oslo 1971, p. 301.
- 78. Guinn V.P., Ann. Rev. Nucl. Sci., 24, 561 (1974).
- 79. Jervis R.E., in: Nuclear Activation techniques in the Life Sciences 1967, IAEA, Vienna 1967, p. 645.
- 80. Moauro A., Carconi P.L. and Casadio S., J. Radioanal. Nucl. Chem., 216, 171 (1997).
- 81. Dybczyński R. and Boboli K., J. Radioanal. Chem., 31, 267 (1976).
- 82. Cornelis R., Speecke A. and Hoste J., Anal. Chim. Acta., 78, 317 (1975).
- 83. Reddy S.J., Mauerhofer E., Porte N., Damodar J. and Denschlag H.O., J. Radioanal. Nucl. Chem., 238, 83 (1998).
- 84. Woittiez J.R.W., van Kamp G.J. and Das H.A., J. Radioanal. Chem., 70, 239 (1982).
- 85. Saiki M., Vasconcellos M.B.A., de Arauz L.J. and Fulfaro R., J. Radioanal. Nucl. Chem., 236, 25 (1998).
- 86. Białkowska M., Hoser A., Szostak W.B., Dybczyński R., Sterliński Sl., Nowicka G., Majchrzak J., Kaczorowski J. and Danko B., Ann. Nutr. Metabol., 31, 327 (1987).
- 87. Zaichick V.Ye., Sviridova T.V. and Zaichick S.V., J. Radioanal. Nucl. Chem., 217, 157 (1997).
- 88. Versieck J., in: Nuclear Analytical Methods in the Life Sciences 1994, [J. Kucera, I. Obrusnik, E. Sabbioni Eds.], Humana Press, Totowa, New Jersey 1994, pp. 407-413.
- 89. Vasconcellos M.B.A., Saiki M., Paletti G., Catharino M.G.M., Baruzzi R.B. and Cuten D.J., in: Proc. Intern. Symposium on Harmonization of Health Related Environmental Measurements Using Nuclear and Isotopic Techniques, (IAEA-SM-344/58), Hyderabad, India 4-7 Nov. 1996, pp. 371-376.
- 90. Pietra R., Sabbioni E., Gallorini M. and Orvini E.J., J. Radioanal. Nucl. Chem., 102, 69 (1986).
- 91. Grimanis A.P., Vassilaki-Grimani M., Alexion D. and Papadatos C., in: Nuclear Activation Techniques in the Life Sciences 1978, IAEA, Vienna 1978, p. 241.
- 92. Wainerdi R.E. and Melon M.P., Nuclear Activation Techniques in the Life Sciences 1967, IAEA, Vienna 1967, p. 33.
- 93. DeGoeij J.J.M., Houtman J.P.N., Tjioe P.S. and Koeman J.H., Nuclear Activation Techniques in the Life Sciences 1972, IAEA, Vienna 1972, p. 295.
- 94. Asubiojo O.J. and Iskander F.Y., J. Radioanal. Nucl. Chem., 125, 265 (1988).
- 95. Salmon L. and Cawse P.A., Instrumental Neutron Activation Analysis in: Soil Analysis, [K.A. Smith, Ed.], Dekker, New York, pp. 299-353.
- 96. Winchester J.W., J. Radioanal. Chem., 19, 311 (1974).
- 97. Lee K.-Y., Shim S.-K., Yoon Y.-Y., Chung Y.-S. and Lee G.-H., J. Radioanal. Nucl. Chem., 241, 129 (1999).
- 98. Frontasyeva M.V. and Steinnes E., in: Proc. Intern. Symposium on Harmonization of Health Related Environmental Measurements Using Nuclear and Isotopic Techniques, (IAEA-SM-344/28), Hyderabad, India 4-7 Nov. 1996, pp. 301-311.
- 99. Zeisler R., Haselberger N., Makarewicz M., Ogris R., Parr R.M., Stone S.F., Valkovic O., Valkovic V. and Wehrstein E., J. Radioanal. Nucl. Chem., 217, 5 (1997).
- 100. Landsberger S., Buchholz B., Chichester D., Kaminski M., Cerbus J. and Larson S., in: Proc. Intern. Symposium on Harmonization of Health Related Environmental Measurements Using Nuclear and Isotopic Techniques, (IAEA-SM-344/20), Hyderabad, India 4-7 Nov. 1996, pp. 547-565.
- 101. Jervis R.E., in: Nuclear Analytical Methods in the Life Sciences 1994, [J. Kucera, I. Obrusnik, E. Sabbioni, Eds.], Humana Press, Totowa, New Jersey 1994, pp. 159-167.
- 102. Mello E., Lusuardi S., Meloni S. and Odone M., J. Radioanal. Chem., 69, 259 (1982).
- 103. Peltz C., Schmid P. and Bichler M., J. Radioanal. Nucl. Chem., 242, 361 (1999).
- 104. Schubiger P.A., Muller O. and Gentner W., J. Radioanal. Chem., 39, 99 (1977).
- 105. Neef H. and Glascock M.D., J. Radioanal. Nucl. Chem. (Articles), 196, 275 (1995).
- 106. Whitehead J.K., Hossain T.Z. and Silverman A., J. Radioanal. Nucl. Chem. (Articles), 196, 235 (1995).
- 107. Carlson S.B. and James W.D., J. Radioanal. Nucl. Chem. (Articles), 196, 207 (1995).
- 108. Lux F., Braunstein L. and Strauss R., in: Modern Trends in Activation Analysis, NBS Special Publication 312, Vol. 1, Washington 1969, p. 216.
- 109. Pańczyk E., Ligęza M. and Waliś L., Nukleonika, 37, 29 (1992).
- 110. Houtman J.P. and Turkstra J., in: Radiochemical Methods of Analysis, Vol. I, IAEA, Vienna 1965, p. 85.
- 111. Pańczyk E., Ligęza M. and Waliś L., Czech. J. Phys., 49/S1, 401 (1999).
- 112. Dybczyński R., Reference materials and their role in quality assurance in inorganic trace analysis, chapter in collective work: Quality problems in trace analysis in environmental studies (in Polish), [A. Kabata-Pendias, B. Szteke, Eds.], Second enlarged edition, Wydawnictwo Edukacyjne Zofii Dobkowskiej, Warszawa, 1998.
- 113. Kucera J. and Byrne A.R., in: Proc. Intern. Symposium on Harmonization of Health Related Environmental Measurements Using Nuclear and Isotopic Techniques, (IAEA-SM-344/27), Hyderabad, India 4-7 Nov. 1996, pp. 349-359.
- 114. Chai C.F., Kong P., Mao X.Y. and Ma S.L., J. Radioanal. Nucl. Chem. (Articles), 192, 101 (1995).
- 115. Hou X., J. Radioanal. Nucl. Chem., 242, 49 (1999).
- 116. Ehmann W.D., Utilization of chemical derivatives in activation analysis, in: Activation analysis, Vol. I, [Z.B. Alfassi, Ed.], CRC Press, Boca Raton 1990.
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