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Abstrakty
2,l,3-Benzoselenadiazole-5-carbaldehyde 5 has been prepared in 53% overall yield from 5-methyl-2,l,3-benzoselenadiazole 1, by a four-step synthesis. Compounds 1-5 and 2,1,3-benzo-selenadiazole 8 have been analysed by 1H, 13C, 15N and 77Se NMR spectroscopy, and structural implications are discussed. Some imines and diimines were prepared from 5, but low solubility in organic solvents made these compounds of little interest for further studies.
Rocznik
Tom
Strony
47--56
Opis fizyczny
Bibliogr. 13 poz.
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autor
autor
autor
autor
- Department of Chemistry, NTNU, Trondheim, Norway (EHM)
Bibliografia
Typ dokumentu
Bibliografia
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bwmeta1.element.baztech-article-BPP1-0014-0005