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Resolution-enhanced H NMR spectra of six single diastereomers of fused-ring sulfur-containing lactams have been recorded and interpreted. In joint analysis of derived couplings Ť/HH> performed with use of the Karplus-Conroy type relationship and results of static MM calculations, it was possible to determine the configuration of title compounds and the conformation elucidation of their six-membered rings. Simultaneously, the stereochemistry of the observed ring-closure reaction was determined. The application of TNDO/2 method for the prediction of n JHH values is also briefly discussed.
Rocznik
Tom
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17--25
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Bibliogr. 22 poz.
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autor
- Department of Organic Chemistry, University of Łódź, Narutowicza 68, 90-136 Łódź 1, P.O. Box 376, Poland (RBN) (Katedra Chemii Organicznej, Uniwersytet Łódzki), rynaz@chemul.uni.lodz.pl
Bibliografia
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Bibliografia
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bwmeta1.element.baztech-article-BPP1-0014-0002