Gas chromatographic analysis of environmental sulphur compounds

Wardencki, W.

Artykuł - szczegóły

Tytuł artykułu

Gas chromatographic analysis of environmental sulphur compounds

Autorzy

Wardencki W.

Wybrane pełne teksty z tego czasopisma

http://beta.chem.uw.edu.pl/chemanal/

Identyfikatory

Warianty tytułu

Oznaczanie związków siarki w środowisku metodami chromatografii gazowej

Języki publikacji

Abstrakty

In this paper GC methods of determination of volatile sulphur compounds, established in the last two decades are reviewed. Techniques most frequently applied for their sampling from gas and liquid matrices are briefly presented. The problems encountered in chromatographic analysis of sulphur-containing compounds referred to chromatograpbic columns and detection systems are described: Tabulated examples of the typical columns and detectors most frequently employed in the analysis of sulphur compounds are included. Also, the examples of simple procedures of avoiding the losses and transformations of these compounds during storage, sampling and analysis are given.

W pracy dokonano przeglądu metod oznaczania lotnych związków siarki z wykorzystaniem chromatografü gazowej, opracowanych w ostatnich dwudziestu latach. Przedstawiono krótko techniki pobierania tych związków z gazowych i ciekłych matryc. Opisano również problemy najczęściej spotykane podczas ich chromatograficznej analizy, związane zarówno z kolumnami jak i detektorami. W tabelach zestawiono przykłady typowych kolumn i detektorów stosowanych w analizie związków siarki. Ponadto podano przykłady prostych procedur unikania strat związków siarki oraz ich przekształceń podczas przechowywania, pobierania i analizy.

Słowa kluczowe

oznaczanie siarka chromatografia gazowa

Wydawca

Komitet Chemii Analitycznej PAN

Czasopismo

Chemia Analityczna

Rocznik

1998

Tom

Vol. 43, No. 4

Strony

513--528

Opis fizyczny

Bibliogr. 156 poz.

Twórcy

autor

Wardencki W.

Analytical Chemistry Department, Chemical Faculty, Technical University of Gdańsk, 11/12 Narutowicz Str., 80-952 Gdańsk, Poland

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