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Techniki spektroskopowe w sprzężeniu z rozdzielaniem chromatograficznym w zastosowaniach inżynierii i ochrony środowiska

Treść / Zawartość
Identyfikatory
Warianty tytułu
EN
Spectroscopic techniques combined with chromatographic of separation in the engineering and environmental protection application
Języki publikacji
PL
Abstrakty
PL
Przedstawiono zastosowania chromatograficznych technik rozdzielania w sprzężeniu z technikami spektroskopowymi do oznaczania priorytetowych zanieczyszczeń środowiska. Omówiono sprzężenia GC-MS oraz HPLC-MS wraz z tandemowymi odmianami spektrometrii mas a więc układami umożliwiającym wielokrotną fragmentację jonów (pułapki jonowe) oraz układy typu triple stage quadrupol. Przedstawiono zalety i wady każdej z technik na przykładach zastosowań w inżynierii i ochronie środowiska. Omówiono również technikę GC-AES (wraz z odmianą GC-AED) wykorzystywaną coraz chętniej do specjacyjnego oznaczania związków metaloorganicznych.
EN
The article presents the application of chromatographic techniques of separation combined with spectroscopic techniques for determination of major environmental pollutants. Combinations of GC-MS and/or HPLC-MS have been presented together with the tandem of mass spectroscopy - systems enabling multiple ion fragmentation (ion traps) and systems based on triple stage quadrupol. Advantages and disadvantages of each technique have been presented on the basis of application in the branch of environmental protection and engineering. We have also depicted in this article the GC-EAS technique (with GC-AED) which is more commonly applied for speciation of metal-organic compounds.
Rocznik
Tom
Strony
18--29
Opis fizyczny
Bibliogr. 37 poz., rys., tab.
Twórcy
autor
  • Katedra Podstaw Techniki, Wydział Podstaw Techniki, Politechnika Lubelska, 20-618 Lublin, ul. Nadbystrzycka 38
Bibliografia
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  • 2. Andersson J.T., 2002: Some unique properties of gas chromatography coupled with atomic emission detection, Anal. Bioanal. Chem., 373, 344-355.
  • 3. Athanasiadou M., Marsh G., Athanassiadis I., Asplund L., Bergman A., 2006: Gas chromatography and mass spectrometry of methoxylated polybrominated diphenyl ethers (MeO-PBDEs), J. Mass Spec., 41, 790-801.
  • 4. Becker G., Colmsjö A., 1998a: Gas chromatography-atomic emission detection for quantification of polycyclic aromatic sulfur heterocycles, Anal. Chim. Acta, 376, 265-272.
  • 5. Becker G., Nilsson U., Colmsjö A., Ostman C., 1998b: Determination of polycyclic aromatic sulfur heterocyclic compounds in airborne particulate by gas chromatography with atomic emission and mass spectrometric detection, J. Chromatogr. A, 826, 57-66.
  • 6. Björklund J., Tollbäck P., Östman C., 2003: Mass spectrometric characteristics of decabromodiphenyl ether and the application of isotopic dilution in the electron capture negative ionization mode for the analysis of polybrominated diphenyl ethers, J. Mass Spec.,38, 394-400.
  • 7. Buser H-R., Rappe C., 1991: Determination of polychlorodibenzotiophenes, the sulfur analogues of polychlorodibenzofurans, using various gas chromatographic/ mass spectrometric techniques, Anal. Chem., 63, 1210-1217.
  • 8. Cai Z., Ramanujam V.M.S., Gross M.L., Cristini A., Tucker R.K., 1994a: Levels of polychlorodibenzo-p-dioxins and dibenzofurans in crab tissues from Newark /Raritan Bay system, Environ. Sci. Technol., 28, 1528-1534.
  • 9. Cai Z., Giblin D.E., Ramanujam V.M.S., Gross M.L., Cristini A., 1994b: Mass-profile monitoring in trace analysis: Identification of polychlorodibenzothiophenes in crab tissues collected from the Newark/Raritan Bay system, Environ. Sci. Technol., 28, 1535-1538.
  • 10. Covaci A., Voorspoels S., de Boer J., 2003: Determination of brominated flame retardants, with emphasis on polybrominated diphenyl ethers (PBDEs) in environmental and human samples: a review. Environ. Internat., 29, 735-756.
  • 11. Echarri I., Nerin C., Wells D.E., Domeńo C., Cacho J., 1998: Multivariate analysis applied to the study of the distribution of chlorobiphenyls (CBs), including the nonortho-CBs, in fish and sea mammals, Analyst,. 123, 421-427.
  • 12. Eljarrat E., Lacorte S., Barceló D., 2002: Optimization of congener-specific analysis of 40 polybrominated diphenyl ethers by gas chromatography/mass spectrometry, J. Mass Spec., 37, 76-84.
  • 13. Fabrellas B., Sanz P., Abad E., Rivera J., Larrazabal D., 2004: Analysis of dioxins and furans in environmental samples by GC-ion-trap MS/MS, Chemosphere, 55, 1469-1475.
  • 14. Focant J-F., Eppe G., De Pauw E., 2001: Optimisation and use of tandem-in-time mass spectrometry in comparison with immunoassay and HRGC/HRMS for PCDD/F screening, Chemosphere, 43, 417-424.
  • 15. Focant J-F., Pirard C., De Pauw E., 2004: Automated sample preparation-fractionation for the measurement of dioxins and related compounds in biological matrices: a review, Talanta, 63, 1101-1113.
  • 16. Focant J-F., Eppe G., Scippo M-L., Massart A-C., Pirard C., Maghuin-Rogister G., DePauw E., 2005: Comprehensive two-dimensional gas chromatography with isotope dilution time-of-flight mass spectrometry for the measurement of dioxins and polychlorinated biphenyls in foodstuffs. Comparison with other methods, J. Chromatogr. A, 1086, 45-60.
  • 17. Frenich-Garrido A., Gonzalez-Romero R., Vidal-Martinez J.L., Bolanos-Plaza P., Rodriguez-Cuadros L., Abdo-Herrera M.A., 2006: Characterization of recovery profiles using gas chromatography-triple quadrupole mass spectrometry for determination of pesticide residues in meat samples, J. Chromatogr. A, 1133, 315-321.
  • 18. Go´mara B., Garci´a-Ruiz C., Gonza´lez M.J., Marina M.L., 2006a: Fractionation of chlorinated and brominated persistent organic pollutants in several food samples by pyrenyl-silica liquid chromatography prior to GC-MS determination, Anal. Chim. Acta, 565, 208-213.
  • 19. Gómara B., Herrero L., Bordajandi L.R., González M.J., 2006b: Quantitative analysis of polybrominated diphenyl ethers in adipose tissue, human serum and foodstuff samples by gas chromatography with ion trap tandem mass spectrometry and isotope dilution, Rapid Comm. Mass Spec., 20, 69-74.
  • 20. Harrad S., Wijesekera R., Hunter S., Halliwell C., Baker R., 2004: Preliminary Assessment of U.K. Human Dietary and Inhalation Exposure to Polybrominated Diphenyl Ethers, Environ. Sci. Tech., 38, 2345-2350.
  • 21. Helen C., Lemasle M., Laplanche A., Genin E., 2001: Determination of polychlorodibenzo-p-dioxins and polychlorodibenzofurans by gas chromatography/tandem mass spectrometry and gas chromatography/ triple mass spectrometry in a quadrupole ion trap, J. Mass Spectrom., 36, 546-554.
  • 22. Hites R.A., Foran J.A., Schwager S.J., Knuth B.A., Hamilton M.C., Carpenter D.O., 2004: Global Assessment of Polybrominated Diphenyl Ethers in Farmed and Wild Salmon, Environ. Sci. Tech., 38, 4945-4949.
  • 23. de Hoffmann J., 1996: Tandem mass spectrometry: a primer, J. Mass Spectrom., 31, 129-137.
  • 24. Kemmochi Y., Tsutsumi K., 2001: Rapid PCDD/PCDF screening method for fly ash with ion trap MS/MS, Chemosphere, 43, 433-437.
  • 25. Kemmochi Y., Tsutsumi K., Futami K., 2002: Optimization of the ionization conditions for the trace analysis PCDD/PCDF with ion trap MS/MS, Chemosphere, 46, 1451-1455.
  • 26. Larrazábal D., Martínez M.A., Eljarrat E., Barceló D., Fabrellas B., 2004: Optimization of quadrupole ion storage mass spectrometric conditions for the analysis of selected polybrominated diphenyl ethers. Comparative approach with negative chemical ionization and electron impact mass spectrometry, J. Mass Spec., 39, 1168-1175.
  • 27. March R.E., Splendore M., Reiner E.J., Mercer R.S., Plomley J.B., Waddell D.S., Mac Pherson K.A., 2000a: Erratum to A comparison of three mass spectrometric methods for the determination of dioxins/furans, International Journal of Mass Spectrometry, 197, 283-297.
  • 28. March R.E., Splendore M., Reiner E.J., Mercer R.S., Plomley J.B., Waddell D.S., MacPherson K.A., 2000b: A comparison of three mass spectrometric methods for the determination of dioxins/furans, International Journal of Mass Spectrometry, 194, 235-246.
  • 29. Nćrt C., De Sćger S., Van Peteghem C., 2004: Development of a gas chromatography/ion trap mass spectrometry based method for the quantification of polybrominated diphenyl ethers and polychlorinated biphenyls in adipose tissue, Rapid Comm. Mass Spec., 18, 2317-2322.
  • 30. North K.D, 2004: Tracking polybrominated diphenyl ether releases in a wastewater treatment plant effluent, Palo Alto, California. Environ. Sci. Tech., 38, 4484-4488.
  • 31. Santos F.J., Galceran M.T., (2003), Modern developments in gas chromatography mass spectrometry-based environmental analysis, J. Chromatogr. A, 1000, 125-151.
  • 32. Sinkkonen S., Paasivirta J., Lahtiperä M., 2001: Chlorinated and methylated dibenzothiophenes in sediment samples from a river contaminated by organochlorine wastes, J. Soils & Sediments, 1, 9-14.
  • 33. Sjödin A., Carlsson H., Thuresson K., Sjölin S., Bergman A., Östman C., 2001: Flame Retardants in Indoor Air at an Electronics Recycling Plant and at Other Work Environments, Environ. Sci. Tech., 35, 448-454.
  • 34. Wang D., Cai Z., Jiang G., Wong M.H., Wong W.K., 2005: Gas chromatography/ion trap mass spectrometry applied for the determination of polybrominated diphenyl ethers in soil, Rapid Comm. Mass Spec., 19, 83-89.
  • 35. Wiedmann T., Schimmel H., Ballschmiter, K-H., 1998: Ion trap MS/MS of polychlorinated dibenzo-p-dioxins and dibenzofurans: confirming the concept of the molar response, Fresenius J. Anal. Chem., 360, 117-119.
  • 36. Worrall K., Robinson C., Wood D., Harrington P., 2001: Optimization of a HRGC-HRMS method for the analysis of PCDD/Fs in salmon and spinach using PTV and/or splitless injection coupled with thin film capillary GC, DIOXIN 2001, 9-14th September, KYONGJU, KOREA, www.micromass.co.uk
  • 37. Zhu L., Ma B., Liang X., 2008: Quantitative analysis of polybrominated diphenyl ethers in earthworms and soil by gas chromatography coupled to ion-trap tandem mass spectrometry, Rapid Comm. Mass Spec., 22, 394-400.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPL2-0020-0034
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