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The study is concerned with the nitrided layers produced on 'medical' steel of the 316L (00H17N14M2) grade at a temperature of 450°C. The results of the microstructural observations performed by TEM and of the phase analysis of the layers are presented and discussed. The examinations were conducted in the regions extending from the surface down to a depth of about 25 um. The nearsurface zone appeared to contain nitrogen austenite and fine precipitates. There were also certain phases in the lamellar form. Because of the applicative aspect of the glow discharge nitriding of 316 steel, the examinations also included its mechanical strength, in particular the static tensile strength and the lowcycle fatigue strength. The static tensile tests showed no significant differences in the yield stress between the samples in the starting state and those subjected to the low-temperature glow discharge assisted nitriding. The low-cycle fatigue tests (which, in view of the differences between the properties of the untreated material and the nitrided layers, can be classified among the most severe mechanical tests) either, indicated no essential differences in the fatigue properties of the samples subjected to the surface treatments conducted under various conditions.
Wydawca
Czasopismo
Rocznik
Tom
Strony
38--48
Opis fizyczny
Bibliogr. 15 poz., rys., fot., tab.
Twórcy
autor
autor
autor
autor
autor
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, Warsaw
Bibliografia
- 1. W.Liang, S.Juncai, X. Xiaolei „Low pressure plasma arc source ion nitriding compared with glow-discharge plasma nitriding of stainless steel", Surface and Coatings Technology 145 (2001) 31 – 37.
- 2. J. R. Sobiecki, T. Borowski, H. Matysiak, K. J. Kurzydłowski, T. Wierzchoń, Increase of durability of stainless steel using the glow discharge treatment, Proc. of 2nd. Inter. Conf. Heat Treat. and Surf. Eng. in Automotive Applications, Riva del Garda, Italy 2005, CD-Rom.
- 3. E. Menthe, K.-T. Rie "Further investigation of the structure and properties of austenitic stainless steel after plasma nitriding", Surface and Coatings Technology 116 - 119 (1999) 1999 – 204.
- 4. T. Czerwiec ,N. Renevier, H. Michel “Low - temperature plasma - assisted nitriding”, Surface and Coatings Technology 131 (2000) 267 – 277.
- 5. S. Leigh, M. Samandi, G.A. Collins, K.T. Short, P. Martin, L. Wielunaki "The influence of ion energy on the nitriding behaviour of austenitic stainless steel" ,Surface and Coatings Technology 85 (1996) 37 – 43.
- 6. J. Erneman ,M. Schwind, P. Liu, J. - O. Nilsson, H. - O.. Andrén, J.Ågren „Precipitation reactions caused by nitrogen uptake during service at high temperatures of a niobium stabilized austenitic stainless steel", Act Materialia 52 (2004) 4337 – 4350.
- 7. W. Liang, X. Xiaolei „ XTEM and XPS studies of plasma nitrocarburising layers on 0.45% C steel", Surface and Coatings Technology 126 (2000) 288 – 293.
- 8. D.R.G. Mitchell, D.J. Attard, G.A. Collins, K.T. Short „ Characterisation of PP and RF plasma nitrided austenitic stainless steels using plan and cross - sectional TEM techniques", Surface and Coatings Technology 165 (2003) 107 – 118.
- 9. M.K. Lei, Z.L. Zhang „ Plasma source ion nitriding of pure iron : formation of an iron nitride layer and hardened diffusion layer at low temperature", Surface and Coatings Technology 91 (1997) 25 – 31.
- 10. X.L. Xu, L. Wang, Z.W. Yu , Z.K. Hei „ Microstructural characterization of plasma nitrided austenitic stainless steel", Surface and Coatings Technology 132 (2000) 270 – 274.
- 11. X. Xiaolei, W. Liang, Y. Zhiwei ,H. Zukun „ A comparative study on microstructure of the plasma - nitrided layers on austenitic stainless steel and pure Fe", Surface and Coatings Technology 192 (2005) 220 – 224.
- 12. M.P. Fewell, D.R.G. Mitchell, J.M. Priest, K.T. Short, G.A.Collins „ The nature of expanded austenite", Surface and Coatings Technology 131 (2000) 300 – 306.
- 13. J.P. Riviere, P. Meheust, J.P. Villain, C. Templier, M. Cahoreau, G. Abrasonis, L. Pranevicius „High current density nitrogen implantation of an austenitic stainless steel", Surface and Coatings Technology 158 - 159 (2002) 99 – 104.
- 14. Z.Q. Liu, D.X. Li, Z.K. Hei, H. Hashimoto “Electron diffraction study on superstructure in the compound layer of ion - nitrided pure iron", Scripta Materialia 46 (2002) 179 – 185.
- 15. T. Christiansen, M. A. J. Somers, On the crystallographic structure of S-phase, Scripta Materialia 50 (2004) 35-37.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BPG8-0018-0026