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In this work, the electrochemical microcel technique bas been coupled with a Peltier heating stage to study the local electro-chemical behaviour of both phases of duplex stainless steels (UNS 31803 and UNS S32304) in 1.7M NaCl (pH=3) at 25°C and 80°C. The results (anodic and cathodic current densities, corrosion potential, pitting sites...) have been analysed consider-ing the microstructure and the mechanical state (determined by thermo-mechanical model) under the microcapillary. The results show a relationship between the corrosion potential and the stress distribution at the specimen surface. Moreover, the results derived from the corrosion tests seem to show that the microstructure and/or the mechanical stress have a significant role in pitting corrosion.
Wydawca
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Rocznik
Tom
Strony
98--107
Opis fizyczny
Bibliogr. 19 poz., rys., tab.
Twórcy
autor
autor
autor
autor
- LRRS, CNRS-Universite de Bourgogne, BP 47870,21078 Dijon Cedex, France
Bibliografia
- [1] Webb KG., Paik C.H. and Alkire R.C.: Local detection of dissolved sulphur species from inclusions in stainless steel using Ag microelectrode. Electrochemical and solid-state letters 4 (2001), pp. B15-B18.
- [2] Webb E.G. and Alkire RC: Pit initiation at single sulphide inclusions in stainless steel. Journal of the electrochemical society 149 (2002), pp. B286-B295.
- [3] Bahni H., Suter T. and Assi F: Micro-electrochemical techniques for studies of localized processes on metal surfaces in the nanometer range. Surface and coatings technology 130 (2000), pp 80-86.
- [4] Krawiec H., Vignal V., Finot E., Heintz O., Oltra R. and Olive J.M.: Local electrochemical studies after beat treatment of stainless steel. Role of induced metallurgical and modifications on pitting triggering. Metallurgical and materials transactions A: physical mettalurgy and materials science 35 (2004), pp. 3515-3521.
- [5] Perren R, Suter T., Uggowitzer P., Weber L., Magdowski R., Bahni H. and Speidel M.: Corrosion science 43 (2001), pp. 707 - 726.
- [6] Paik C.H., White H.S. and Alkire R.C.: Scanning electrochemical microscopy detection of dissolved sulphur species from inclusions in stainless steel. Journal of the electrochemical society 147 (2000), pp. 4120-4124.
- [7] Williams D.E. and Zhu Y.Y.: Explanation for initiations of pitting corrosion of stainless steels at sulphide inclusions. Journal of electrochemical society 147 (2000), pp. 1763-1766.
- [8] Akid R and Mills D.J.: A comparison between conventional macroscopic and novel microscopic scanning electrochemical methods to evaluate galvanic corrosion. Corrosion science 43 (2001), pp. 1203-1216.
- [9] Krawiec H., Vignal V.and Oltra R: Use of the electrochemical microcell technique and the SVET for monitoring pitting corrosion at MnS inclusions. Electrochemistry Communications 6 (2004), pp 655-660.
- [10] Vuillemin B., Philippe X., Oltra R., Vignal V., Coudreuse L, Dufour L.C. and Finot E. : SVET, AFM and AES study of pitting corrosion initiated on MnS inclusions by microinjection. Corrosion science 45 (2003), pp. 1143-1159.
- [11] Park J.O., Paik C. H., Huang Y.H and Alkire R.C: Influence of the Fe-Rich intermetallic inc1usions on pit initiation on aluminium alloys in aerated NaCl. Journal of electrochemical society 146 (1999), pp. 517-523.
- [12] Aldykiewicz A.J. and Isaacs H.S. : Dissolution characteristics of duplex stainless steels in acidic environments. Corrosion science 40 (1998), pp. 1627-1646.
- [13] Vignal V., Mary N., Valot c., Oltra R. and Coudreuse L.: Influence of elastic deformation on initiation of pits on duplex stainless steels. Electrochemical and solid-state letters 7(2004), C39-C42.
- [14] Vignal V., Favergeon J. and Oltra R.: Finite-element method for the determination of the surface stress field from the real microstructure of anisotropic materiais. Philosophical magazine letters 82 (2002), pp. 503-510.
- [15] Mary N., Vignal V., Oltra R and Coudreuse L.: Finite-element and XRD methods for the determination of the residual surface stress field and the elastic-plastic behaviour of duplex steels. Philosophical magazine 85 (2005), pp. 1227-1242.
- [16] Vignal V., Oltra R and Josse C.: Local analysis of the mechanical behaviour of inclusions containing stainless steels under straining conditions. Scripta materialia 49 (2003), pp. 779-784.
- [17] Mary N., Vignal V., Oltra R. and Coudreuse L.: Advances in local mechano-electrochemistry for detecting pitting corrosion in duplex steels. Journal of materials research 19 (2004), pp. 3688-3694.
- [18] Hauk V.: Structural and residual stress analysis by non-destructive methods (Elsevier, Amsterdam, 1997).
- [19] Vignal V., Oltra R., Mary N. and Peultier J.: A mechanical-electrochemical approach for the determination of precursor sites for pitting corrosion at microscale. Journal of the electrochemical society 153 (2006), B352-B357.
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Bibliografia
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