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This paper presents the results of metallographic, X-ray, and TEM examinations of the microstructure and the sub-structure of the diffusion layer that underlies the TiN + Ti2N layer produced by glow discharge nitriding of the Ti6Al2Cr2Mo alloy. The metallographic examinations show that a two-phase zone α + β - its thick-ness increasing with the increasing process temperature - can be observed underneath the nitride layer after half an hour of nitriding at 940ºC, when the core of the sample has an α - phase structure. The presence of the glow discharge assisting the nitrid-ing process accelerated the thickening of both the nitride zone and the diffusion layer. Morphology of α - phase grains changed as well. The grain lengh-to-thickness ratio decreased. X-ray examinations revealed the presence in the substrate structure of two kinds of solid solution with the α titanium matrix. TEM analysis showed a state of certain ordering of the crystalline lattice and, locally, a tweed-type structure of the β phase.
Wydawca
Czasopismo
Rocznik
Tom
Strony
28--34
Opis fizyczny
Bibliogr. 15 poz., rys., tab.
Twórcy
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, Warsaw, Poland
autor
- Institute of Metallurgy and Materials Science, Polish Academy of Scinces, Cracow, Poland
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, Warsaw, Poland
autor
- Warsaw University of Technology, Faculty of Materials Science and Engineering, Warsaw, Poland
Bibliografia
- 1. A. Fleszar, T. Wierzchoń, Sun Kym Kim, J.R. Sobiecki: Surface and Coatings Technology, 131 (2000), 62.
- 2. E.I. Meletis: Surface and Coatings Technology, 149 (2002) 95.
- 3. E. Roliński, G. Sharp, D.F. Cowgill, D.J. Peterman.: Journal of Nuclear Materials, 252 (1998) 2000.
- 4. E. Foi, C. Deramaix.: Surface Engineering. Vol. 16, no. 3 (2000) 205.
- 5. A. Raveh, A. Bussiba et al.: Surface and Coating Technoogy 57 (1993) 19.
- 6. K. Wilsdorf, H.J. Spies: Gas and plasma nitriding of the (α+β)Ti alloy in various gas mixture and the influence of a subsequent age-hardening treatment on mechanical properties. Proc. of 11th Congress of IFHT SE, AIM, Florence, Italy, 1 (1998) 351.
- 7. B. Major, M. Gołębiewski, T. Wierzchoń: Journal of Mat. Sci. Lett., 21(2002)1289.
- 8. T. Wierzchoń, A. Fleszar.: Surface and Coatings Technology, 96 (1997) 205.
- 9. T.W. Duering, J. Albrecht, I. Richter, P. Tischer.: Acta Metall., 2, 30(1982)2161.
- 10. A.A. Popow.: Phys. Met. Metallov., 76 (1993) 5, 147.
- 11. R.W. Cahn and P. Haasen (Eds): Physical Metallurgy, vol. 2, North-Holland Phys. Publishing, (1983) 345.
- 12. T. Hemejims, G. Lutjering S. Weissmenn.: Metall. Trans., 11, (1972) 3.
- 13. G.H. Narayan, T.T. Archbold.: Metall. Trans., 8(1970)1, 2281.
- 14. J. Wood and P. A. Russo.: Industrial Heating, 4 (1997)51.
- 15. W.A. Bieloglasov, A.A. Popw.: Rus. Metall., 2(1987)63.
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Bibliografia
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bwmeta1.element.baztech-article-BPG5-0015-0035