Analiza doświadczalna własciwości termomechanicznych stopów TiNi oraz poliuretanu z pamięcią ksztaltu

Pieczyska, E.

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Analiza doświadczalna własciwości termomechanicznych stopów TiNi oraz poliuretanu z pamięcią ksztaltu

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Pieczyska E.

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Warianty tytułu

Experimental analysis of thermomechanical properties of TiNi SMA and shape memory polyurethane

Języki publikacji

Abstrakty

Niniejsza rozprawa przedstawia wyniki badan sprz^zen termodynamicznych zachodz^cych podczas indukowanej napr^zeniami przemiany fazowej w stopach TiNi z pami^ciq, ksztaltu (SMA) oraz termomechaniczne wlasciwosci poliuretanu z pami^ci^ ksztaltu (SMP), przeprowadzonych w IPPT PAN oraz w AIT w Japonii. W ramach pracy przeprowadzono na maszynach wytrzymalosciowych badania zmian parametrow mechanicznych oraz, za pomocq, kamery termowizyjnej, obserwacje zmian temperatury probek tych materialow w procesie jednoosiowego rozci^gania, prostego scinania oraz odksztalcen cyklicznych realizowanych z roznymi pr^dkosciami odksztalcania. Wykazano, ze przemiana martenzytyczna wprost i odwrotna, zachodz^ca podczas pseudospr^zystego odksztalcania stopow z pami^ci^ ksztaltu, moze miec charakter niejednorodny, niezaleznie od rodzaju, pr§dkosci czy sposobu sterowania odksztalceniem probki. Makroskopowo rozwija si? ona w zlokalizowanych cienkich pasmach, podobnych do pasm Ludersa, w dwoch prawie prostopadlych kierunkach. Niejednorodnosci przemiany martenzytycznej udokumentowano w technice badan w podczerwieni oraz fotografuj^c relief na powierzchni probki. Wykazano, ze istnieje mozliwosc oddzialywania na przebieg zainicjowanych juz przemian fazowych w stopie z pami^ciq, ksztaltu. Zbadano efekty termomechaniczne zwi^zane z inicjacj^, rozwojem i zanikiem przemiany w warunkach wprowadzanych przystankow w gal?ziach obci^zania i odci^zania p?tli pseudospr?zystosci. Wykorzystuj^c wyznaczone doswiadczalnie parametry badanego stopu TiNi oraz stosuj^c termodynamicznq. teori? przemiany fazowej stopow z pami^ci^ ksztaltu, przeprowadzono energetyczny bilans przemiany indukowanej napr^zeniem dla przypadku jednoosiowego rozciqgania dla roznych pr^dkosci odksztalcania. Wyznaczono zmiany napr^zenia i temperatury podczas rozci^gania i prostego scinania poliuretanu z pami^ci^ ksztaltu oraz zbadano stopien odzyskiwania ksztaltu i wlasciwosci po odksztalcaniu i wygrzaniu powyzej jego temperatury zeszklenia.

The thesis presents results of experimental investigations of thermomechanical couplings related to stress-induced martensite transformation in TiNi shape memory alloy (SMA) and thermomechanical properties of shape memory polyurethane (SMP) carried out at IFTR PAS and Aichi Institute of Technology in Japan. The investigations of mechanical properties of the SMA and SMP specimens subjected to uniaxial tension, simple shear, as well as cyclic loadings, have been carried out on testing machines with various strain rates. Also the temperaturę changes have been recorded with use of an thermovision camera. It has been demonstrated that the forward and reverse martensitic transformation, related to the SMA pseudoelastic behavior, can occur in inhomogeneous way in Liiders-like bands developing in two almost perpendicular directions, for both stress- and strain-controlled tension tests, at various strain rates. The martensite transformation heterogeneity has been confirmed by infrared techniąue and by photographs of the SMA specimen surface relief. It has been proved that it is possible to control the process of martensite transformation not only by the temperaturę but also by the stress changes, due to the thermomechanical couplings. The effects of thermomechanical couplings related to the nucleation, development and vanishing of the stress-induced martensite transformation have been studied in terms of the introduced breaks in loading and unloading branches of the SMA pseudoelastic loop. Basing on the thermodynamic theory, complemented by the estimated material parameters of TiNi and uding the stress-and temperature-strain characteristics found during tension tests, an energy balance for the stress-induced forward and reverse martensite transformation for various strain rates has been calculated. Mechanical and temperature characteristics of a shape memory polyurethane subjected to tension and simple shear processes have been found. Shape recovery of defects introduced in the glass state and removed during the subsequent heating above the polymer glass transition temperature has been studied.

Słowa kluczowe

stop wytrzymałość materiałów zmęczenie materiału nikiel tytan

mechanics of materials alloy nickel titanium

Wydawca

Instytut Podstawowych Problemów Techniki PAN

Czasopismo

Prace Instytutu Podstawowych Problemów Techniki PAN

Rocznik

2008

Tom

nr 3

Strony

1--214

Opis fizyczny

Bibliogr. 157 poz.

Twórcy

autor

Pieczyska E.

Instytut Podstawowych Problemów Techniki Polskiej Akademii Nauk

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