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Analysis of intermetallic particles in AlSi1MgMn aluminium alloy

Wybrane pełne teksty z tego czasopisma
Identyfikatory
Warianty tytułu
Konferencja
12th International Scientific Conference CAM3S'2006, 27-30th November 2006, Gliwice-Zakopane
Języki publikacji
EN
Abstrakty
EN
Purpose: The main objective of this study was to analyze the morphology and composition of complex microstructure of the intermetallic phases in AlSi1Mg alloy. Design/methodology/approach: In this study, several methods were used such as: optical light microscopy (LM), transmission (TEM) and scanning (SEM) electron microscopy in combination with X-ray analysis (EDS) using polished sample, and X-ray diffraction (XRD) to identify intermetallics in AlSi1MgMn aluminium alloy. Findings: The results show that the as-cast microstructure of AlSi1MgMn alloy after slow solidification at a cooling rate 2 degrees centigrade/min, consisted a wide range of intermetallics phases. By using various instruments (LM, SEM, XRD) and techniques (imagine, EDS) the: alpha-A15FeSi, alpha-Al15(FeMn)3Si, A19Mn3Si, alpha-Al12Fe3Si, Mg2Si intermetallic phases were identified. Research limitations/implications: In order to complete and confirm obtained results it is recommended to perform further analysis of the 6000 series aluminium alloys. Therefore it is planned to include in a next study, microstructure analysis of the alloy by using transmission electron microscopy technique (TEM). Practical implications: Since the morphology, crystalography and chemical composition affect the intermetallic properties, what involves changes of alloy properties, from a practical point of view it is important to understand their formation conditions in order to control final constituents of the alloy microstructure. This paper has provided essential data about various intermetallic phases precipitating in 6000 series aluminium alloys. Originality/value: This paper proposes the best experimental techniques for analysis of the intermetallic phases occuring in the 6xxx series aluminium alloys, provide wide description of the intermetallics formation through all possible reactions and data about their chemical composition, morphology and crystallography.
Rocznik
Strony
155--158
Opis fizyczny
Bibliogr. 15 poz., fot., rys., tab.
Twórcy
  • Department of Materials Science, Rzeszów Univesity of Technology, ul. W. Pola 2, 35-959 Rzeszów, Poland, mrowka@prz.edu.pl
Bibliografia
  • [1] C.D. Marioara, S.J. Andersen, J. Jansen, H.W. Zandbergen, The influence of temperature and storage time at RT on nucleation of the β” phase in a 6082 Al-Mg-Si alloy, Acta Mater 51 (2003) 789-796.
  • [2] N.C.W. Kuijpers, W.H. Kool, P.T.G. Koenis, K.E. Nilsen, I. Todd, S. van der Zwaag, Assessment of different techniques for quantification of α-Al(FeMn)Si and β-AlFeSi intermetallics in AA 6xxx alloys, Materials Characterization 49 (2003) 409-420.
  • [3] Aluminium. Properties and Physical Metallurgy. Ed Hatch J.E., ASM Metals Park, Ohio 1984.
  • [4] S. Zajac, B. Bengtsson , Ch. Jönsson, Influence of cooling after homogenization and reheating to extrusion on extrudability and final properties of AA 6063 and AA 6082 alloys, Materials Science Forum, 396-402 (2002) 399-404.
  • [5] G. Mrówka-Nowotnik, J. Sieniawski, Influence of heat treatment on the micrustructure and mechanical properties of 6005 and 6082 aluminium alloys, Journal of Materials Processing Technology 162-163 (2005) 367-372.
  • [6] A.K. Gupta, P.H. Marois, D.J. Lloyd, Review of the techniques for the extraction of second-phase particles from aluminium alloys, Materials Characterization 37: 61-81 (1996) 61-80.
  • [7] R.A. Jeniski Jr, Effect of Cr addition the microstructure and mechanical behavior of 6061-T6 continuously cast and rolled redraw rod, Materials Science and Engineering A237 (1997) 52-64.
  • [8] M. Warmuzek, G. Mrówka, J. Sieniawski, Influence of the heat treatment on the precipitation of the intermetallic phases in commercial AlMn1FeSi alloy, Journal of Materials Processing Technology, 157-158 (2004) 624-632.
  • [9] Y.L.Liu, S.B. Kang, H.W.Kim, The complex microstructures in as-cast Al-Mg-Si alloy, Materials Letters 41 (1999) 267-272.
  • [10] L.F. Mondolfo, Aluminium Alloys, Structure and Properties. Butterworths, London-Boston, 1976.
  • [11] M. Warmuzek, K. Rabczak, J. Sieniawski, The course of the peritectic transformation in the Al-rich Al-Fe-Mn-Si alloys, Journal of Materials Processing Technology 162-163 (2005) 422-428.
  • [12] M. Warmuzek, J. Sieniawski, K. Wicher, G. Mrówka-Nowotnik, The study of distribution of the transition metals and Si during primary precipitation of the intermetallic phases in Al-Mn-Si alloys, Journal of Materials Processing Technology 175 1-3 (2006) 421-426.
  • [13] S.R. Claves, D.L. Elias, W.Z. Misiolek, Analysis of the Intermetallic Phase Transformation Occurring During Homogenization of 6xxx Aluminum Alloys. Mater. Sci. Forum 396-402 (2002) 667-674.
  • [14] M. Warmuzek et al, Influence of heat treatment on the precipitation of the intermetallic phases in AlMn1FeSi, Proc. Int. Conf. "Achievements in Mechanical & Materials Engineering" Gliwice-Zakopane (2002) 601-604.
  • [15] L.A. Dobrzański, W. Borek, R. Maniara, Influence of the crystallization condition on Al-Si-Cu casting alloys structure, Journal of Achievements in Materials and Manufacturing Engineering 18, 1-2 (2006) 211-214.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BOS5-0018-0028
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